CN102908379A - Multi-index quality-control based fresh platycodon grandiflorum medicinal slice processing method - Google Patents
Multi-index quality-control based fresh platycodon grandiflorum medicinal slice processing method Download PDFInfo
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Abstract
The invention discloses a multi-index quality-control based fresh platycodon grandiflorum medicinal slice processing method and sets up a quality comprehensive-quality evaluating system taking platycodon grandiflorum total saponin, platycodon grandiflorum polysaccharide and platycodon grandiflorum saponin D as indexes. In the multi-index quality-control based fresh platycodon grandiflorum medicinal slice processing method, multiple indexes are included, combination of total effective part and single effect ingredient is featured, internal quality of the platycodon grandiflorum can be comprehensively reflected, so that harvesting of the platycodon grandiflorum is more reasonable and scientific, production-place processing of the platycodon grandiflorum is standardized, and quality of platycodon grandiflorum medicinal slices is improved. Further, the multi-index quality-control based fresh platycodon grandiflorum medicinal slice processing method provides reference for standard harvesting, production-place processing, medicinal technique and the like of the platycodon grandiflorum in Bozhou.
Description
Technical field
The present invention relates to a kind of Radix Platycodonis decoction pieces and gather, processing, concocting method.
Background technology
Chinese medicine is mainly derived from plant, and traditional processing mode of tcm and herbal slice is reprocessed into decoction pieces for taking first medical material.The prepared slices of Chinese crude drugs are material bases of tcm clinical practice medication, yet traditional concocting method process is comparatively loaded down with trivial details, and work consuming is consuming time, can cause the uneven of product quality, and prepared slice quality is unstable, and these factors have seriously restricted the development of the industrialization of modern Chinese medicine decoction pieces.
Chinese crude drug at source directly is processed into decoction pieces, namely at source with fresh medical material after certain dried, carry out again dry method after cutting into decoction pieces.Not only can shorten processing link, energy savings, and also decoction pieces can also keep preferably color and luster abnormal smells from the patient.But relevant fresh medical material processing in production place concocted technology is less both at home and abroad, most of decoction pieces processing rest on medicinal herb grower's empirical operation and small-scale production, do not set up its processing in production place and quality control procedure both at home and abroad, About The Quality of Sliced Herbal Medicine is also unstable, decoction pieces market is comparatively chaotic, and urgency is treated the production technology that the bright medicine in the place of production of development parameter is directly processed decoction pieces.
Summary of the invention
The present invention discloses a kind of Radix Platycodonis decoction pieces, the present invention also aims to disclose gathering of a kind of Radix Platycodonis decoction pieces, processing, processing procedure.The objective of the invention is to realize by following technology.
This paper has set up the method for quality control take Radix Platycodi total saponins, platycodon root polysaccharide, Platycodin D as index, the method is with many indexs, total effective parts and single active ingredient are integrated as characteristics, the inherent quality that can comprehensively reflect Radix Platycodonis uses this quality control appraisement system to optimize the gathering of Radix Platycodonis, processing in production place, decoction pieces technique.
The optimum process condition of optimizing is: the Radix Platycodonis of the life in 2 years of gathering October, choose the bright Radix Platycodonis medical material of diameter about 2cm, clean silt, remove reed head and bifurcated, fibrous root, afterbody, scrape off crust, put 60 ℃ of forced air drying 7-9h (the Radix Platycodonis water content reaches 35～40%) in the baking oven, take out, cut into the thick disk of 2-3mm, get final product at 60 ℃ of baking 6～7h.
Following experimental example and embodiment are used for further specifying
Embodiment 1
Taked the bright Radix Platycodonis medical material of life in 2 years October, choose the bright Radix Platycodonis medical material of diameter about 2cm, clean silt, remove reed head and bifurcated, fibrous root, afterbody, drop in the cylinder stripping machine, clean silt, scrape off crust, put in the self-control drying room, 65 ℃ of (the interior temperature of drying room is actual to be 60 ℃) dry 7-9h when reaching 35～40% to the Radix Platycodonis water content, take out, cut into the thick disk of 2-3mm at reciprocating medicine cutter, put into the self-control drying room, smoke 8-9h for 65 ℃, take out, cool, pack with plastic bag sealing.
Drink at random 3 in sheet sample, sample 1, sample 2, sample 3.Sample 1, sample 2, the decoction pieces sheet type of sample 3 is all complete; Color is faint yellow.Sample 1, sample 2, the time of sample 3 dryings is respectively 8.5h, 8h, 9h.
The Radix Platycodonis decoction pieces is compared with the Radix Platycodonis decoction pieces thin layer chromatography of control medicinal material, differentiated a lower thin layer chromatography according to 2005 editions one middle Radix Platycodonis, measure the speckle of aobvious same color.
According to 2005 editions " appendix IXH one method of Chinese Pharmacopoeia 2005 version " aquametry " is measured, sample 1, sample 2, the water content of sample 3 is respectively 12.8%, 12.0%, 11.9%, all less than 13%, surpasses the regulation of pharmacopeia.Meet the pharmacopeia requirement.
According to 2005 editions " high performance liquid chromatography of Chinese pharmacopoeia (appendix VID) mensuration.Sample 1, sample 2, the content of the Radix Platycodi total saponins of sample 3 is respectively 4.03%, 4.1%, and 4.64%.All be higher than 1.7%, meet the requirement of pharmacopeia.
According to 2005 editions " high performance liquid chromatography of Chinese pharmacopoeia (appendix VID) mensuration.Sample 1, sample 2, the Platycodin D of sample 3 is respectively 0.1903%, 0.1827%, and 0.1853%.All be higher than 0.1%.
According to 2005 editions Chinese Pharmacopoeia determination of polysaccharide, sample 1, sample 2, the platycodon root polysaccharide 23.83%, 24.13%, 22.8% of sample 3.All be not less than 22.8%, meet the pharmacopeia requirement.
Take the bright Radix Platycodonis medical material of life in 2 years the example 2:10 month, chosen the bright Radix Platycodonis medical material of diameter about 2cm, cleaned silt, remove reed head and bifurcated, fibrous root, afterbody, drop into and clean silt in the cylinder stripping machine, scrape off crust, put in the self-control drying room, 60 ℃ of dry 7-9h are when reaching 35～40% to the Radix Platycodonis water content, take out, cut into the thick disk of 2-3mm at reciprocating medicine cutter, put into low temp dryer, smoke 6-7h for 60 ℃, take out, cool, pack with plastic bag sealing.
Drink at random 3 in sheet sample, sample 4, sample 5, sample 6.Decoction pieces sheet type is all complete; Color is white slightly yellow.Sample 4, sample 5, sample 6 respectively dry time be 6.5h, 6.2h, 7.0h.
The Radix Platycodonis decoction pieces is compared with the Radix Platycodonis decoction pieces thin layer chromatography of control medicinal material, differentiated a lower thin layer chromatography according to 2005 editions one middle Radix Platycodonis, measure the speckle of aobvious same color.
According to 2005 editions " appendix IXH one method of Chinese Pharmacopoeia 2005 version " aquametry " is measured, sample 4, sample 5, the water content of sample 6 is respectively, 11.7%, 10.8%, 12.0%, all less than 13%,
According to 2005 editions " high performance liquid chromatography of Chinese pharmacopoeia (appendix VID) mensuration.Sample 4, sample 5, the content of the Radix Platycodi total saponins of sample 6 is respectively 4.69%, 4.52%, and 4.71%.All be higher than 1.7%, meet the requirement of pharmacopeia.
According to 2005 editions " high performance liquid chromatography of Chinese pharmacopoeia (appendix VID) mensuration.Sample 4, sample 5, the Platycodin D of sample 6 is respectively 0.1801%, 0.1914%, and 0.1839%.All be higher than 0.1%.
According to 2005 editions Chinese Pharmacopoeia determination of polysaccharide, sample 4, sample 5, the platycodon root polysaccharide 25.76%, 26.15%, 25.46% of sample 6.All be higher than 22.8%, meet the pharmacopeia requirement.
Claims (3)
1. the Radix Platycodonis decoction pieces based on the Quality Control of many indexs is taken advantage of bright processing technique, by setting up many indexs, the quality evaluation system that total effective parts combines with single active ingredient, gather below having chosen, processing and concocting method: choose bright Radix Platycodonis medical material, put forced air drying in the baking oven, take out, cut into disk, be positioned over forced air drying in the baking oven.
2. take advantage of bright processing technique according to claims 1 described Radix Platycodonis decoction pieces, the gather October Radix Platycodonis of life in 2 years, choose the bright Radix Platycodonis medical material of diameter about 2cm, clean silt, remove reed head and bifurcated, fibrous root, afterbody, scrape off crust, be positioned over forced air drying in the baking oven, take out, cut into disk, be positioned over forced air drying in the baking oven.
3. take advantage of bright processing technique according to claims 1,2 described Radix Platycodonis decoction pieces, choose bright Radix Platycodonis medical material, clean silt, remove reed head and bifurcated, fibrous root, afterbody, scrape off crust.Put 60 ℃ of forced air drying 7-9h (the Radix Platycodonis water content reaches 35～40%) in the baking oven, take out, cut into the thick disk of 2-3mm, get final product at 60 ℃ of baking 6～7h.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103583766A (en) * | 2013-10-31 | 2014-02-19 | 巫溪县瑞雪药材种植有限责任公司 | Making method for preserved platycodon grandiflorum fruit |
| CN104126795A (en) * | 2014-07-01 | 2014-11-05 | 安顺天元生物资源开发有限公司 | Platycodon grandiflorum rough processing method |
| CN105193895A (en) * | 2015-09-23 | 2015-12-30 | 成都艾比科生物科技有限公司 | Comprehensive extraction method for extracting saponin and polysaccharide from platycodon grandiflorum |
Citations (2)
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| CN102000119A (en) * | 2009-09-01 | 2011-04-06 | 杭州海善制药设备有限公司 | Fresh processing technology of traditional Chinese plant medicine at producing site |
| CN102370680A (en) * | 2010-08-25 | 2012-03-14 | 中国中医科学院中药研究所 | Processing method for decoction pieces of Ligusticum wallichii in producing area |
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2012
- 2012-10-15 CN CN2012103888970A patent/CN102908379A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102000119A (en) * | 2009-09-01 | 2011-04-06 | 杭州海善制药设备有限公司 | Fresh processing technology of traditional Chinese plant medicine at producing site |
| CN102370680A (en) * | 2010-08-25 | 2012-03-14 | 中国中医科学院中药研究所 | Processing method for decoction pieces of Ligusticum wallichii in producing area |
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| 章承林等: "《药用植物栽培技术》", 31 August 2009, 中国农业大学出版社 * |
| 金传山等: "桔梗双飞片产业化生产工艺研究", 《中药材》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103583766A (en) * | 2013-10-31 | 2014-02-19 | 巫溪县瑞雪药材种植有限责任公司 | Making method for preserved platycodon grandiflorum fruit |
| CN104126795A (en) * | 2014-07-01 | 2014-11-05 | 安顺天元生物资源开发有限公司 | Platycodon grandiflorum rough processing method |
| CN105193895A (en) * | 2015-09-23 | 2015-12-30 | 成都艾比科生物科技有限公司 | Comprehensive extraction method for extracting saponin and polysaccharide from platycodon grandiflorum |
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Application publication date: 20130206 |