CN102876539A - Method for improving anthocyanin content in red bayberry wine - Google Patents
Method for improving anthocyanin content in red bayberry wine Download PDFInfo
- Publication number
- CN102876539A CN102876539A CN201210392290XA CN201210392290A CN102876539A CN 102876539 A CN102876539 A CN 102876539A CN 201210392290X A CN201210392290X A CN 201210392290XA CN 201210392290 A CN201210392290 A CN 201210392290A CN 102876539 A CN102876539 A CN 102876539A
- Authority
- CN
- China
- Prior art keywords
- red bayberry
- juice
- fermentation
- waxberry
- anthocyanidin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 244000132436 Myrica rubra Species 0.000 title claims abstract description 62
- 235000014101 wine Nutrition 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims abstract description 32
- 150000004636 anthocyanins Chemical class 0.000 title abstract 10
- 229930002877 anthocyanin Natural products 0.000 title abstract 9
- 235000010208 anthocyanin Nutrition 0.000 title abstract 9
- 239000004410 anthocyanin Substances 0.000 title abstract 9
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 75
- 238000000855 fermentation Methods 0.000 claims abstract description 49
- 230000004151 fermentation Effects 0.000 claims abstract description 49
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000011347 resin Substances 0.000 claims abstract description 26
- 229920005989 resin Polymers 0.000 claims abstract description 26
- 235000019990 fruit wine Nutrition 0.000 claims abstract description 14
- 238000005352 clarification Methods 0.000 claims abstract description 13
- 230000032683 aging Effects 0.000 claims abstract description 9
- 238000004519 manufacturing process Methods 0.000 claims abstract description 6
- 238000005516 engineering process Methods 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 239000002253 acid Substances 0.000 claims abstract 4
- 150000001452 anthocyanidin derivatives Chemical class 0.000 claims description 62
- 229930014669 anthocyanidin Natural products 0.000 claims description 61
- 235000008758 anthocyanidins Nutrition 0.000 claims description 61
- 235000009134 Myrica cerifera Nutrition 0.000 claims description 41
- 244000269152 Myrica pensylvanica Species 0.000 claims description 41
- 240000001717 Vaccinium macrocarpon Species 0.000 claims description 38
- 235000012545 Vaccinium macrocarpon Nutrition 0.000 claims description 38
- 235000002118 Vaccinium oxycoccus Nutrition 0.000 claims description 38
- 235000004634 cranberry Nutrition 0.000 claims description 38
- 235000007270 Gaultheria hispida Nutrition 0.000 claims description 25
- 235000012851 Myrica pensylvanica Nutrition 0.000 claims description 25
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 17
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 14
- 238000003483 aging Methods 0.000 claims description 8
- 239000003292 glue Substances 0.000 claims description 7
- 239000000049 pigment Substances 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 7
- 238000011081 inoculation Methods 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 6
- 235000007652 Arbutus Nutrition 0.000 claims description 3
- 240000008327 Arbutus unedo Species 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 229940126670 AB-836 Drugs 0.000 claims description 2
- 230000000274 adsorptive effect Effects 0.000 claims description 2
- 238000010828 elution Methods 0.000 claims description 2
- 230000001954 sterilising effect Effects 0.000 claims description 2
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- 235000008694 Humulus lupulus Nutrition 0.000 claims 9
- 229920002678 cellulose Polymers 0.000 claims 9
- 239000001913 cellulose Substances 0.000 claims 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 3
- 150000001914 cyanidin Chemical class 0.000 claims 1
- 238000012545 processing Methods 0.000 abstract description 13
- 235000013399 edible fruits Nutrition 0.000 abstract description 8
- 238000001179 sorption measurement Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 238000013124 brewing process Methods 0.000 abstract 1
- 238000005119 centrifugation Methods 0.000 abstract 1
- 235000010987 pectin Nutrition 0.000 abstract 1
- 229920001277 pectin Polymers 0.000 abstract 1
- 239000001814 pectin Substances 0.000 abstract 1
- VEVZSMAEJFVWIL-UHFFFAOYSA-O cyanidin cation Chemical compound [O+]=1C2=CC(O)=CC(O)=C2C=C(O)C=1C1=CC=C(O)C(O)=C1 VEVZSMAEJFVWIL-UHFFFAOYSA-O 0.000 description 22
- 239000000047 product Substances 0.000 description 16
- 235000007336 cyanidin Nutrition 0.000 description 11
- 239000002932 luster Substances 0.000 description 8
- 239000000203 mixture Substances 0.000 description 7
- 238000011010 flushing procedure Methods 0.000 description 6
- 235000000346 sugar Nutrition 0.000 description 6
- 229930006000 Sucrose Natural products 0.000 description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 5
- 239000004575 stone Substances 0.000 description 5
- 239000005720 sucrose Substances 0.000 description 5
- 238000000605 extraction Methods 0.000 description 4
- 239000012467 final product Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 239000008399 tap water Substances 0.000 description 4
- 235000020679 tap water Nutrition 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 235000008375 Decussocarpus nagi Nutrition 0.000 description 3
- 235000014631 Myrica rubra Nutrition 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 229940072056 alginate Drugs 0.000 description 2
- 235000010443 alginic acid Nutrition 0.000 description 2
- 229920000615 alginic acid Polymers 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 238000010009 beating Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000009923 sugaring Methods 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 235000003283 Pachira macrocarpa Nutrition 0.000 description 1
- 244000171263 Ribes grossularia Species 0.000 description 1
- 235000002357 Ribes grossularia Nutrition 0.000 description 1
- 240000001085 Trapa natans Species 0.000 description 1
- 235000014364 Trapa natans Nutrition 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- -1 aluminum ion Chemical class 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 235000021028 berry Nutrition 0.000 description 1
- 102000006995 beta-Glucosidase Human genes 0.000 description 1
- 108010047754 beta-Glucosidase Proteins 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
- 239000000989 food dye Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- 229960002737 fructose Drugs 0.000 description 1
- 230000004345 fruit ripening Effects 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000002207 metabolite Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000001603 reducing effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000009165 saligot Nutrition 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Images
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention belongs to the fields of fruit deep processing and fruit wine processing and relates to a method for improving the anthocyanin content in red bayberry wine. According to the characteristic that the anthocyanin in the red bayberry wine brewing process can be easily degraded, and the anthocyanin in the red bayberry juice is firstly separated and is added after the fermentation completion of the anthocyanin separated red bayberry juice, so the anthocyanin content in the red bayberry wine products can be obviously improved. After the juice of fresh red bayberries is taken, filtration and centrifugation are carried out, clean red bayberry juice is obtained, a macroporous adsorption resin column is adopted for adsorption, the anthocyanin is adsorbed onto the resin column, and decolored red bayberry juice flows out from the column, so the red bayberry juice are separated into two parts including the anthocyanin part and the decolored red bayberry juice part, the decolored red bayberry juice is fermented according to the conventional fruit wine brewing technology, substances including red bayberry anthocyanin and the like adsorbed onto the resin column are eluted by acid edible alcohol and are added after the fermentation completion of the decolored red bayberry juice, and then, the subsequent treatment including pectin adding, clarification, ageing and the like is carried out according to the conventional fruit wine production process, so the anthocyanin content in red bayberry wine is improved.
Description
Technical field
The invention belongs to food processing field, relate to deep processing of red bayberry, be specifically related to improve the production method of red hayberry wine anthocyanidin content.
Background technology
Red bayberry (Myrica rubra Sieb et Zucc) is the Myruca ceas red bayberry spp.ing plant, originate in China southeast, on the south the Yangtze valley cultivation is arranged all now, the provinces such as main product Zhejiang, Jiangsu, Fujian, Jiangxi, Hunan and Guangdong, but cultivated area, output and quality etc. all with Zhejiang for.Red bayberry is nutritious, has better nutritivity and health care to be worth, and fresh fruit sugar degree 8%~12% contains organic acid 1.0%~3.2%, and contains abundant VITAMIN and mineral substance.According to the mature fruit color and luster, red bayberry can divide white race, Red Indian race, pink kind and crow to plant 4 classes, wherein the crow kind red bayberry take the water chestnut kind as representative because it is rich in the characteristics tempos such as anthocyanidin, acidity are lower, sour and sweet palatability very fast.
Except the white race red bayberry, most ripe red bayberries are scarlet in atropurpureus, are rich in take Cy-3-G as main anthocyanidin.Studies show that more and more the multiple pharmacological effect such as that anthocyanidin has is anti-oxidant, antitumor, reducing blood-fat, hypoglycemic, control cardiovascular and cerebrovascular diseases, anti-inflammatory, promotion eyesight have broad application prospects in the exploitation of protective foods and medicine.
Red bayberry belongs to berry, and juice is abundant, adopts to rot easily afterwards, and the marketing fresh shelf-lives is shorter.Because the Waxberry fruit ripening stage, listing was concentrated on the occasion of rainy season in midsummer, again not storage tolerance transportation of the utmost point, along with the increase of red bayberry output, the problem of red bayberry " it is difficult to sell fruit " becomes increasingly conspicuous, and the processing of carrying out red bayberry is more and more important.Red bayberry adopts the method for sugaring, steeping in wine to preserve usually traditionally, and main products has glazed waxberry, canned arbutu, gooseberry jam, red bayberry soaking wine etc., and is wherein famous with the red bayberry soaking wine.Develop again in recent years a series of red bayberry converted products, such as red bayberry juice, waxberry wine, red bayberry inspissated juice etc.Seed selection success along with good red bayberry kind is rapidly developed take products such as production cranberry juice and red hayberry wines as main red bayberry processing industry.
In the deep processed product of red bayberry, red hayberry wine is to be subject to the kind that industry is paid much attention to always.This mainly is that if can brew and the similar fruit wine product of cranberry juice color and luster, one obtains the human consumer surely likes because red bayberry is bright in colour; Next is that the fruit wine industry is the direction that China greatly develops.But in the practice that red hayberry wine is produced, it is found that cranberry juice bright in colour during the fermentation its color disappear gradually and take off, its anthocyanidin content remains little when finishing to whole fruit wine production process, and appearance luster and human consumer's expected value differs larger, seriously perplexs the development of red hayberry wine industry.
Patent 200610052087.2 discloses a kind of production method of red bayberry (myrica rubra) dry wine wine, and the method is by three sugaring primary fermentations, three tank switchings and three sealing secondary fermentation, again through clarification, freezing ageing, blend and the process such as ultrafiltration membrance filter, acquisition red bayberry (myrica rubra) dry wine wine.But since red bayberry in anthocyanidin be Cy-3-G more than 90%, wait art breading by fermentation after, the anthocyanidin more than 80% all is decomposed, and just finds that aborning red cranberry juice becomes gradually near incarnadine even colourless red hayberry wine.In order to preserve better the anthocyanidin of red hayberry wine product, Zhong Ruimin etc. (2005) report adopts the aluminium alginate Immobilized yeast, can make anthocyanidin keep 40%~50%, think that the vigor that immobilization makes yeast produce beta-glucosidase descends, aluminum ion and bayberry cyanidin react and form the more stable mixture of color and luster simultaneously, have therefore improved the retention rate of anthocyanidin.Patent 200510111686.2 discloses a kind of bayberry cyanidin extract for preparing to method, the method comprises that mainly the techniques such as extraction using alcohol, filtration, Recycled ethanol, macroporous resin adsorption, water washing resin post, ethanol elution, Recycled ethanol, vacuum-drying obtain bayberry cyanidin extract, use as food dye.The method is the universal method of anthocyanidin preparation, the technological process more complicated.And since in the red bayberry anthocyanidin content be not very high, in Cy-3-G, the high-content of bibliographical information is 250mg/L only, only produces bayberry cyanidin, utilization rate of raw materials is very low.In addition, according to our research, anthocyania pigment is made after the powder, when again dissolving, and water-soluble to some extent decline.The present invention must have fermentable sugars to exist according to yeast and be produced cofactor by the yeast utilization, by could the degrade principle of anthocyanidin of cofactor and enzyme acting in conjunction, propose first its anthocyanidin to be separated before the cranberry juice fermentation, row joins the method for karusen again after Primary Fermentation and secondary fermentation end, thereby significantly improves the anthocyanidin content of red hayberry wine.Not yet find same or similar patent report.
Summary of the invention
The object of the present invention is to provide a kind of preparation method who is rich in anthocyanidin red hayberry wine product.
Be that the present invention is take new arbutus as main raw material, after squeezing the juice, the anthocyanidin in the cranberry juice is separated in advance, avoid anthocyanidin to be subject to the effect of yeast and meta-bolites thereof, the cranberry juice of anthocyanidin to be separated adds after fermenting and finishing again, thereby significantly improves the anthocyanidin content in the red hayberry wine product.Also utilize the edible ethanol of processing through deodorization to soak waxberry flesh, anthocyanidin alcohol vat liquor is rich in acquisition, also after finishing, the cranberry juice fermentation adds, further improve the anthocyanidin content of red hayberry wine, in the situation that does not add exogenous anthocyanidin, improve the anthocyanidin content of red hayberry wine product, thereby improve the quality of red hayberry wine.
The present invention realizes by following manner:
1, obtaining of cranberry juice: fresh dark red bayberry is pressed extracting juice with squeezing machine after cleaning, avoid the fruit stone of crushing, and obtains the turbid juice of red bayberry.After red bayberry is got juice, after filtration with speed centrifugal treating more than 3000 rev/mins, obtain clear waxberry juice and pulp.
2, the separation of anthocyanidin in the clear waxberry juice: clear waxberry juice is with adsorbing through pretreated macroporous adsorptive resins, the materials such as anthocyanidin are adsorbed on the resin column, the decolouring cranberry juice flows out in post, treat that resin column adsorbs when saturated, with solvent with material wash-outs such as anthocyanidin, thereby original juice of red bayberry is divided into anthocyanidin part and decolouring cranberry juice two portions.The materials such as bayberry cyanidin that are adsorbed in resin column are that 0.1%~0.5% concentrated hydrochloric acid, volume fraction of ethanol are 30%~95% edible alcohol water solution wash-out with containing volume fraction, obtain the bayberry cyanidin spirituous solution, and adding after decolour cranberry juice Primary Fermentation and secondary fermentation are finished.The resin column that has adsorbed anthocyanidin need not the water flushing, directly contains sour edible ethanol wash-out and gets final product with above-mentioned.The anthocyanidin edible alcohol solution of wash-out also need not through other subsequent disposal, directly adds karusen and gets final product.
3, the extraction of waxberry flesh anthocyanidin: the turbid juice of red bayberry filters/pulp after centrifugal with 0.5~1.0 times of volume, to contain volume fraction be that 0.1%~0.5% concentrated hydrochloric acid, volume fraction of ethanol are 30%~95% edible ethanol immersion, 4~30 ℃ of extraction temperatures, extraction time 1~7 day, then filter and obtain vat liquor, and adding after decolour cranberry juice Primary Fermentation and secondary fermentation are finished.
4, the fermentation of decolouring cranberry juice: decolouring cranberry juice routinely brewing fruit wine technology ferments, and mainly comprises the technological processs such as composition adjustment, sterilization, cooling, inoculation yeast, Primary Fermentation and secondary fermentation.With the sucrose sugar addition be 23~26 the degree, leavening temperature is 18~35 ℃.
5, the adding of pigment solution: after the cranberry juice fermentation ends of decolouring, to add decolouring cranberry juice karusen from pigment solution and the pulp lixiviate pigment solution of polymeric adsorbent wash-out, and then carry out the processing such as follow-up lower glue, clarification, ageing according to conventional technique for producing fruit wine, thereby obtain high anthocyanidin content red hayberry wine product.Also can not add and from pulp, extract the pigment that obtains, only add the pigment that from cranberry juice, separates.
Advantage of the present invention is: the degradation characteristic of brewageing middle anthocyanidin according to red hayberry wine, bayberry cyanidin is separated in advance, add again after the fermentation ends, avoid the effect of yeast, in the situation of not adding exogenous anthocyanidin, significantly improve the anthocyanidin content of red hayberry wine product.In the anthocyanidin process in separating original juice of red bayberry, adsorb saturated macroporous resin column and need not the water flushing, directly get final product with containing sour edible alcohol solution wash-out, elutriant also need not through other subsequent disposal, directly adds decolouring cranberry juice karusen and gets final product.
Description of drawings
Accompanying drawing is processing technology routine figure of the present invention.
Embodiment
Following examples only are used for setting forth the present invention, do not limit protection scope of the present invention.Those skilled in the art all can realize purpose of the present invention according to above scope of disclosure.
Embodiment 1
Ripe fresh Biqi bayberry 10kg, the tap water flushing is filtered dry moisture, fruit stone is pulled in making beating out, pulp place 4000 rev/mins centrifugal, must clarify the about 7.5kg of cranberry juice, the about 0.8kg of pulp.The clarification cranberry juice is equipped with 480mL with diameter 3.5cm, high 60cm and adsorbs at twice through the chromatographic column of pretreated macroporous resin (resin of the models such as X-5, AB-8 all can), collects the cranberry juice 7.0kg through decolouring.Be adsorbed in the anthocyanidin of resin column with containing the 60% edible ethanol wash-out that volume fraction is 0.2% hydrochloric acid, obtain the about 0.5L of elutriant.Pulp at 4 ℃ of lower immersion 48h, filters to get soak solution 0.5L with the 0.5L same solvent.Decolouring cranberry juice sucrose sugar addition to 25 ° Brix, be heated to 90 ℃ and keep 10min to sterilize, be cooled to the activated wine active dry yeast of inoculation after 35 ℃, the yeast consumption is 0.02% mass concentration, tank switching separate fermentation throw out after 25 ℃ of 2 weeks of fermentation, carry out 2 weeks of secondary fermentation, add bayberry cyanidin elutriant and pulp soak solution, again according to technique for producing fruit wine carry out lower glue, clarification, ageing, blend, the processing such as can, obtain at last about color and luster is scarlet, anthocyanidin content is high red hayberry wine product 6.5L.The anthocyanidin that keeps in the new wine of red bayberry reaches more than 80% of raw material anthocyanidin total amount.
Embodiment 2
Ripe fresh Biqi bayberry 10kg, the tap water flushing is filtered dry moisture, fruit stone is pulled in making beating out, pulp place 4000 rev/mins centrifugal, must clarify the about 7.5kg of cranberry juice, the about 0.8kg of pulp.The clarification cranberry juice is equipped with 480mL with diameter 3.5cm, high 60cm and adsorbs at twice through the chromatographic column of pretreated macroporous resin (resin of the models such as X-5, AB-8 all can), collects the cranberry juice 7.0kg through decolouring.Be adsorbed in the anthocyanidin of resin column with containing the 60% edible ethanol wash-out that volume fraction is 0.2% hydrochloric acid, obtain the about 0.5L of elutriant.Decolouring cranberry juice sucrose sugar addition to 25 ° Brix, be heated to 90 ℃ and keep 10min to sterilize, be cooled to the activated wine active dry yeast of inoculation after 35 ℃, the yeast consumption is 0.02% mass concentration, tank switching separate fermentation throw out after 25 ℃ of 2 weeks of fermentation, carry out 2 weeks of secondary fermentation, add the bayberry cyanidin elutriant, again according to technique for producing fruit wine carry out lower glue, clarification, ageing, blend, the processing such as can, obtain at last about color and luster is scarlet, anthocyanidin content is high red hayberry wine product 6.5L.The anthocyanidin that keeps in the new wine of red bayberry reaches more than 80% of original juice of red bayberry anthocyanidin total amount.
Embodiment 3
Ripe fresh Biqi bayberry 500kg, the tap water flushing is filtered dry moisture, and juice extractor is squeezed the juice, and avoids fruit stone broken in the process of squeezing the juice, and pulp places 8000 rev/mins of industry high speed whizzers centrifugal, must clarify the about 375kg of cranberry juice, the about 40kg of pulp.The clarification cranberry juice is equipped with 7.5L through the chromatographic column gradation absorption of pretreated macroporous resin (resin of the models such as X-5, AB-8 all can) with diameter 10cm, high 120cm, collects the cranberry juice 350kg through decolouring.Be adsorbed in the anthocyanidin of resin column with containing the 60% edible ethanol wash-out that volume fraction is 0.2% hydrochloric acid, obtain the about 25L of elutriant.Pulp at 4 ℃ of lower immersion 48h, filters to get soak solution 25L with the 25L same solvent.Decolouring cranberry juice sucrose sugar addition to 25 ° Brix, be heated to 90 ℃ and keep 10min to sterilize, be cooled to the activated wine active dry yeast of inoculation after 35 ℃, the yeast consumption is 0.02% mass concentration, tank switching separate fermentation throw out after 25 ℃ of 2 weeks of fermentation, carry out 2 weeks of secondary fermentation, add bayberry cyanidin elutriant and pulp soak solution, again according to technique for producing fruit wine carry out lower glue, clarification, ageing, blend, the processing such as can, obtain at last about color and luster is scarlet, anthocyanidin content is high red hayberry wine product 325L.The anthocyanidin that keeps in the new wine of red bayberry reaches more than 80% of raw material anthocyanidin total amount.
Embodiment 4
Ripe fresh Biqi bayberry 500kg, the tap water flushing is filtered dry moisture, and juice extractor is squeezed the juice, and avoids fruit stone broken in the process of squeezing the juice, and pulp places 8000 rev/mins of industry high speed whizzers centrifugal, must clarify the about 375kg of cranberry juice, the about 40kg of pulp.The clarification cranberry juice is equipped with 7.5L through the chromatographic column gradation absorption of pretreated macroporous resin (resin of the models such as X-5, AB-8 all can) with diameter 10cm, high 120cm, collects the cranberry juice 350kg through decolouring.Be adsorbed in the anthocyanidin of resin column with containing the 60% edible ethanol wash-out that volume fraction is 0.2% hydrochloric acid, obtain the about 25L of elutriant.Decolouring cranberry juice sucrose sugar addition to 25 ° Brix, be heated to 90 ℃ and keep 10min to sterilize, be cooled to the activated wine active dry yeast of inoculation after 35 ℃, the yeast consumption is 0.02% mass concentration, tank switching separate fermentation throw out after 25 ℃ of 2 weeks of fermentation, carry out 2 weeks of secondary fermentation, add the bayberry cyanidin elutriant, again according to technique for producing fruit wine carry out lower glue, clarification, ageing, blend, the processing such as can, obtain at last about color and luster is scarlet, anthocyanidin content is high red hayberry wine product 325L.The anthocyanidin that keeps in the new wine of red bayberry reaches more than 80% of original juice of red bayberry anthocyanidin total amount.
Reference
Zhong Ruimin, Ceng Qingxiao, Liu Feng, etc. the aluminium alginate fixed yeast improves the anthocyanogen stability study in the waxberry wine fermentation. Food science, 2005,26 (11): 94-98.
Claims (9)
1. method that improves the blue or green cellulose content of fermentation waxberry hops, it is characterized in that, original juice of red bayberry is divided into decolouring cranberry juice and anthocyanidin two portions before fermentation, the cranberry juice that only decolours becomes the decolouring karusen through Primary Fermentation and secondary fermentation, anthocyanidin adds after fermentation ends, and then carry out the subsequent disposal such as lower glue, clarification, ageing by the fruit wine production method, thereby obtain high anthocyanidin content fermentation waxberry wine.
2. the method for the blue or green cellulose content of described raising fermentation waxberry hops according to claim 1 is characterized in that, after new arbutus is squeezed the juice, by filtering/technology such as centrifugal, obtains clear waxberry juice and waxberry flesh.
3. the method for the blue or green cellulose content of described raising fermentation waxberry hops according to claim 1, it is characterized in that, the clear waxberry juice that claim 2 obtains is processed with macroporous adsorptive resins, the decolouring original juice of red bayberry directly flows out from resin column, be adsorbed in anthocyanidin acid concentration in the resin column and be 0.1%~0.5% the sour solvent elution that contains, thereby original juice of red bayberry is divided into decolouring original juice of red bayberry and bayberry cyanidin class pigment two portions.
4. the method for the blue or green cellulose content of described raising fermentation waxberry hops according to claim 1, it is characterized in that, the decolouring cranberry juice that claim 3 obtains is after allotment, sterilization, the inoculation fruit wine yeast, regulate leavening temperature and be 20~35 ℃ and carried out Primary Fermentation and secondary fermentation totally 20~60 days, obtain the karusen that decolours.
5. the method for the blue or green cellulose content of described raising fermentation waxberry hops according to claim 1, it is characterized in that, with the waxberry flesh acid concentration that obtains in the claim 2 be 0.1%~0.5% contain sour solvent soaking 4~24 hours, squeeze and filter obtains containing anthocyanidin solution.
6. the method for the blue or green cellulose content of described raising fermentation waxberry hops according to claim 1, it is characterized in that, anthocyanidin solution with claim 3 acquisition, waxberry flesh soak solution independent or that obtain with claim 5 adds the decolouring karusen that obtains in the claim 4, thereby obtains being rich in anthocyanidin red bayberry karusen.
7. the method for the blue or green cellulose content of described raising fermentation waxberry hops according to claim 1, it is characterized in that, claim 6 obtains is rich in anthocyanidin red bayberry karusen and need passes through the subsequent techniques such as lower glue, clarification, ageing and process, thereby obtains to be rich in anthocyanidin fermentation waxberry wine.
According to claim 3 with the method for the blue or green cellulose content of the described raising fermentation waxberry of claim 5 hops, it is characterized in that described solvent is edible ethanol, its concentration is 30~95%.
According to claim 3 with the method for the blue or green cellulose content of the described raising fermentation waxberry of claim 5 hops, it is characterized in that described acid is hydrochloric acid or acetic acid.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201210392290 CN102876539B (en) | 2012-10-16 | 2012-10-16 | Method for improving anthocyanin content in red bayberry wine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201210392290 CN102876539B (en) | 2012-10-16 | 2012-10-16 | Method for improving anthocyanin content in red bayberry wine |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102876539A true CN102876539A (en) | 2013-01-16 |
CN102876539B CN102876539B (en) | 2013-08-28 |
Family
ID=47478062
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 201210392290 Active CN102876539B (en) | 2012-10-16 | 2012-10-16 | Method for improving anthocyanin content in red bayberry wine |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102876539B (en) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103396913A (en) * | 2013-07-30 | 2013-11-20 | 苏州苏东庭生物科技有限公司 | Processing method for novel waxberry sparkling wine |
CN105273954A (en) * | 2015-11-24 | 2016-01-27 | 来凤县古杨梅食品开发有限责任公司 | Method for preparing steeping liquor rich in waxberry polyphenol |
CN105995988A (en) * | 2016-05-26 | 2016-10-12 | 湖南省星城明月生态农业科技发展有限公司 | Blueberry tablet rich in anthocyanin |
CN105995344A (en) * | 2016-05-26 | 2016-10-12 | 长沙湘资生物科技有限公司 | Blueberry vinegar beverage product and making method thereof |
CN105995369A (en) * | 2016-05-26 | 2016-10-12 | 董爱文 | Radix polygonati officinalis healthcare compound particle |
CN106281842A (en) * | 2015-06-08 | 2017-01-04 | 伊春市丰园森林食品有限公司 | The preparation method of Isatis indigotica Fort (Indigofera tinctoria L, Baphicanthus cusia (nees) Brem. Polygonum tinctorium Ait) fruit wine |
CN106957779A (en) * | 2017-04-14 | 2017-07-18 | 安徽金鹰农业科技有限公司 | A kind of blueberry fruit wine preparation method for extracting anthocyanidin |
CN110713886A (en) * | 2019-12-04 | 2020-01-21 | 湖南瑞生源生物科技有限公司 | Preparation method of red bayberry wine |
CN113493728A (en) * | 2020-03-20 | 2021-10-12 | 九阳股份有限公司 | Fruit wine brewing method of food processor and food processor |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1806699A (en) * | 2006-01-26 | 2006-07-26 | 浙江工商大学 | Color-protecting clarification technique of waxberry wind and waxberry juice |
CN1896215A (en) * | 2006-06-22 | 2007-01-17 | 周文兴 | Brewing method of red wine of bayberry claret |
CN1986539A (en) * | 2005-12-20 | 2007-06-27 | 苏州市思源医药科技有限公司 | Bayberry cyanidin extract |
-
2012
- 2012-10-16 CN CN 201210392290 patent/CN102876539B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1986539A (en) * | 2005-12-20 | 2007-06-27 | 苏州市思源医药科技有限公司 | Bayberry cyanidin extract |
CN1806699A (en) * | 2006-01-26 | 2006-07-26 | 浙江工商大学 | Color-protecting clarification technique of waxberry wind and waxberry juice |
CN1896215A (en) * | 2006-06-22 | 2007-01-17 | 周文兴 | Brewing method of red wine of bayberry claret |
Non-Patent Citations (2)
Title |
---|
钟瑞敏等: "海藻酸铝固定化酵母在杨梅果酒发酵中提高花色苷稳定性研究(英文)", 《食品科学》 * |
陈亦辉等: "杨梅加工技术及其产业发展分析", 《农产品加工》 * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103396913A (en) * | 2013-07-30 | 2013-11-20 | 苏州苏东庭生物科技有限公司 | Processing method for novel waxberry sparkling wine |
CN106281842A (en) * | 2015-06-08 | 2017-01-04 | 伊春市丰园森林食品有限公司 | The preparation method of Isatis indigotica Fort (Indigofera tinctoria L, Baphicanthus cusia (nees) Brem. Polygonum tinctorium Ait) fruit wine |
CN105273954A (en) * | 2015-11-24 | 2016-01-27 | 来凤县古杨梅食品开发有限责任公司 | Method for preparing steeping liquor rich in waxberry polyphenol |
CN105995988A (en) * | 2016-05-26 | 2016-10-12 | 湖南省星城明月生态农业科技发展有限公司 | Blueberry tablet rich in anthocyanin |
CN105995344A (en) * | 2016-05-26 | 2016-10-12 | 长沙湘资生物科技有限公司 | Blueberry vinegar beverage product and making method thereof |
CN105995369A (en) * | 2016-05-26 | 2016-10-12 | 董爱文 | Radix polygonati officinalis healthcare compound particle |
CN106957779A (en) * | 2017-04-14 | 2017-07-18 | 安徽金鹰农业科技有限公司 | A kind of blueberry fruit wine preparation method for extracting anthocyanidin |
CN110713886A (en) * | 2019-12-04 | 2020-01-21 | 湖南瑞生源生物科技有限公司 | Preparation method of red bayberry wine |
CN113493728A (en) * | 2020-03-20 | 2021-10-12 | 九阳股份有限公司 | Fruit wine brewing method of food processor and food processor |
Also Published As
Publication number | Publication date |
---|---|
CN102876539B (en) | 2013-08-28 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102876539B (en) | Method for improving anthocyanin content in red bayberry wine | |
US11512271B2 (en) | Fruit wine aroma enhancement brewing technology using cutinase | |
CN102010809B (en) | Red date wine | |
CN101892147B (en) | Method for rapidly brewing grape vinegar based on microbial technology | |
CN102676329A (en) | Process for brewing fortified grape wine by using amur grape | |
CN107475015B (en) | Red-heart pitaya and white-heart pitaya composite fruit wine and preparation method thereof | |
CN103525610B (en) | Red grape spirit production technology | |
CN111718821B (en) | Novel medlar fermented wine and brewing method thereof | |
KR20120123774A (en) | Aronia mandschurica | |
CN102827722A (en) | Purple sweet potato medlar dry red wine | |
KR100941002B1 (en) | A method of grape with rice make raw rice wine | |
CN109593630B (en) | Fermented seedless wampee vinegar and preparation method and application thereof | |
CN109294807A (en) | A kind of preparation method of Sugarless type black rice wine | |
CN104327997A (en) | Waxberry fruit wine and processing method thereof | |
CN111196981A (en) | Fruit wine prepared from subtropical fruit as raw material and preparation method thereof | |
CN101165158A (en) | Method for preparing juicy peach wine | |
KR101293694B1 (en) | Method for preparing schizandra distilled liquor | |
JPS63216463A (en) | Production of fruit fermented liquors | |
CN103642640A (en) | Preparation method for litchi brandy | |
CN102634427B (en) | Novel grape wine made by using double-feeding and double-bacterium compound fermentation process and making method thereof | |
CN112852182A (en) | Pigment extraction process of blackcurrant raisin skin residues | |
CN110862895A (en) | Preparation method of dragon fruit and mulberry fruit wine | |
CN110643449A (en) | Brewing method of cherry wine | |
CN104371900A (en) | Method for brewing grape flavor type white wine | |
CN104694331A (en) | Brewing method of three-berry wine |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
DD01 | Delivery of document by public notice | ||
DD01 | Delivery of document by public notice |
Addressee: Liu Xueming Document name: payment instructions |
|
DD01 | Delivery of document by public notice |
Addressee: Liu Xueming Document name: Notice of Termination of Patent Rights |