CN102876223B - Environment-friendly water-based UV (ultraviolet) curable coating and production method - Google Patents
Environment-friendly water-based UV (ultraviolet) curable coating and production method Download PDFInfo
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- CN102876223B CN102876223B CN201210369632.6A CN201210369632A CN102876223B CN 102876223 B CN102876223 B CN 102876223B CN 201210369632 A CN201210369632 A CN 201210369632A CN 102876223 B CN102876223 B CN 102876223B
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- 238000000576 coating method Methods 0.000 title claims abstract description 39
- 239000011248 coating agent Substances 0.000 title claims abstract description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 21
- 239000013530 defoamer Substances 0.000 claims abstract description 18
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 17
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 9
- 229920002635 polyurethane Polymers 0.000 claims abstract description 9
- 239000004814 polyurethane Substances 0.000 claims abstract description 9
- 239000000080 wetting agent Substances 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 238000001816 cooling Methods 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 238000006243 chemical reaction Methods 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 12
- 239000006185 dispersion Substances 0.000 claims description 10
- -1 polysiloxane Polymers 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- 229920001296 polysiloxane Polymers 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 8
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 6
- 229920000642 polymer Polymers 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 4
- KTALPKYXQZGAEG-UHFFFAOYSA-N 2-propan-2-ylthioxanthen-9-one Chemical compound C1=CC=C2C(=O)C3=CC(C(C)C)=CC=C3SC2=C1 KTALPKYXQZGAEG-UHFFFAOYSA-N 0.000 claims description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 4
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 4
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims description 4
- 150000002009 diols Chemical class 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 4
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 claims description 4
- WXPWZZHELZEVPO-UHFFFAOYSA-N (4-methylphenyl)-phenylmethanone Chemical compound C1=CC(C)=CC=C1C(=O)C1=CC=CC=C1 WXPWZZHELZEVPO-UHFFFAOYSA-N 0.000 claims description 3
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 3
- 150000001336 alkenes Chemical class 0.000 claims description 3
- 239000012752 auxiliary agent Substances 0.000 claims description 3
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 claims description 3
- 239000012965 benzophenone Substances 0.000 claims description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 3
- 229910052731 fluorine Inorganic materials 0.000 claims description 3
- 239000011737 fluorine Substances 0.000 claims description 3
- 150000003866 tertiary ammonium salts Chemical class 0.000 claims description 3
- WCGUUGGRBIKTOS-GPOJBZKASA-N (3beta)-3-hydroxyurs-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CC[C@@H](C)[C@H](C)[C@H]5C4=CC[C@@H]3[C@]21C WCGUUGGRBIKTOS-GPOJBZKASA-N 0.000 claims description 2
- 229910002012 Aerosil® Inorganic materials 0.000 claims description 2
- COVZYZSDYWQREU-UHFFFAOYSA-N Busulfan Chemical compound CS(=O)(=O)OCCCCOS(C)(=O)=O COVZYZSDYWQREU-UHFFFAOYSA-N 0.000 claims description 2
- XHIKSLHIZYVEQI-UHFFFAOYSA-N CC1=C(C(=O)[PH2]=O)C(=CC(=C1)C)C Chemical compound CC1=C(C(=O)[PH2]=O)C(=CC(=C1)C)C XHIKSLHIZYVEQI-UHFFFAOYSA-N 0.000 claims description 2
- 239000004952 Polyamide Substances 0.000 claims description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- 244000028419 Styrax benzoin Species 0.000 claims description 2
- 235000000126 Styrax benzoin Nutrition 0.000 claims description 2
- 235000008411 Sumatra benzointree Nutrition 0.000 claims description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Substances CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 2
- 230000002378 acidificating effect Effects 0.000 claims description 2
- 239000013543 active substance Substances 0.000 claims description 2
- 150000008431 aliphatic amides Chemical class 0.000 claims description 2
- 229960002130 benzoin Drugs 0.000 claims description 2
- LUZSPGQEISANPO-UHFFFAOYSA-N butyltin Chemical class CCCC[Sn] LUZSPGQEISANPO-UHFFFAOYSA-N 0.000 claims description 2
- 239000004359 castor oil Substances 0.000 claims description 2
- 235000019438 castor oil Nutrition 0.000 claims description 2
- 239000003153 chemical reaction reagent Substances 0.000 claims description 2
- MZRQZJOUYWKDNH-UHFFFAOYSA-N diphenylphosphoryl-(2,3,4-trimethylphenyl)methanone Chemical compound CC1=C(C)C(C)=CC=C1C(=O)P(=O)(C=1C=CC=CC=1)C1=CC=CC=C1 MZRQZJOUYWKDNH-UHFFFAOYSA-N 0.000 claims description 2
- 239000000428 dust Substances 0.000 claims description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 2
- 235000019382 gum benzoic Nutrition 0.000 claims description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
- 239000003999 initiator Substances 0.000 claims description 2
- 238000009413 insulation Methods 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 229920002647 polyamide Polymers 0.000 claims description 2
- 229920001610 polycaprolactone Polymers 0.000 claims description 2
- 239000004632 polycaprolactone Substances 0.000 claims description 2
- 229920000515 polycarbonate Polymers 0.000 claims description 2
- 239000004417 polycarbonate Substances 0.000 claims description 2
- 229920000728 polyester Polymers 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 229920000909 polytetrahydrofuran Polymers 0.000 claims description 2
- 150000003376 silicon Polymers 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims description 2
- 229940096998 ursolic acid Drugs 0.000 claims description 2
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 claims description 2
- 239000002270 dispersing agent Substances 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000003973 paint Substances 0.000 description 9
- 230000007613 environmental effect Effects 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 5
- 238000003848 UV Light-Curing Methods 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- 230000001804 emulsifying effect Effects 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 2
- 238000001723 curing Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004945 emulsification Methods 0.000 description 2
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000008589 Cortex Fraxini Substances 0.000 description 1
- 229920001730 Moisture cure polyurethane Polymers 0.000 description 1
- 241000237502 Ostreidae Species 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 229950002895 cellaburate Drugs 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920003009 polyurethane dispersion Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 description 1
- 238000007761 roller coating Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
Description
Composition | Weight fraction |
Self-control urethane acrylate | 30 |
Self-control emulsifying agent | 5 |
Dispersion agent | 2 |
Flow agent (mixture of weight ratio BYK333 and BNK222) | 1 |
BYK1770 | 0.5 |
BYK-P104S | 0.5 |
Light trigger (weight ratio 907:ITX:1173=1:0.3:5) | 3 |
Deionized water | 58 |
Composition | Weight fraction |
Urethane acrylate (German Baeyer 2587) | 30 |
Emulsifying agent (TX-10) | 5 |
Dispersion agent | 2 |
Flow agent (mixture of weight ratio BYK333 and BNK222) | 1 |
BYK1770 | 0.5 |
BYK-P104S | 0.5 |
Light trigger (weight ratio 907:ITX:1173=1:0.3:5) | 3 |
Deionized water | 58 |
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210369632.6A CN102876223B (en) | 2012-09-28 | 2012-09-28 | Environment-friendly water-based UV (ultraviolet) curable coating and production method |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210369632.6A CN102876223B (en) | 2012-09-28 | 2012-09-28 | Environment-friendly water-based UV (ultraviolet) curable coating and production method |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102876223A CN102876223A (en) | 2013-01-16 |
CN102876223B true CN102876223B (en) | 2015-02-04 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201210369632.6A Active CN102876223B (en) | 2012-09-28 | 2012-09-28 | Environment-friendly water-based UV (ultraviolet) curable coating and production method |
Country Status (1)
Country | Link |
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CN (1) | CN102876223B (en) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103614079A (en) * | 2013-12-12 | 2014-03-05 | 南宝树脂(佛山)有限公司 | Production process of water-based UV (ultraviolet) treatment agent |
CN103951774B (en) * | 2014-05-04 | 2015-11-11 | 天津工业大学 | The preparation method of urethane capsule |
CN104448200A (en) * | 2014-12-19 | 2015-03-25 | 江南大学 | Preparation method of plant oil-based UV-curable waterborne organosilicone polyurethane resin |
CN106047141B (en) * | 2016-07-12 | 2018-10-26 | 叶有国 | A kind of optical curing of UV coating and its preparation method and application with strong adhesive force |
CN106752870A (en) * | 2016-12-14 | 2017-05-31 | 太仓佩琦涂料有限公司 | Aqueous vacuum plating UV dope |
CN106752871A (en) * | 2016-12-14 | 2017-05-31 | 太仓佩琦涂料有限公司 | Environment-friendly water-based UV coating and preparation method thereof |
CN107325603B (en) * | 2017-07-14 | 2019-06-21 | 张家港康得新光电材料有限公司 | A kind of aqueous photochromic coating, nail polish and ornament materials |
CN108504274A (en) * | 2018-03-28 | 2018-09-07 | 三河亮克威泽工业涂料有限公司 | Aqueous bis- curing metal coating of UV and its preparation method and application |
CN115651509A (en) * | 2022-10-20 | 2023-01-31 | 湖州市南浔区绿色家居产业研究院 | Photocuring floor coating and preparation method thereof |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5300615A (en) * | 1992-09-24 | 1994-04-05 | Bayer Aktiengesellschaft | Polyurethanes containing acryloyl groups, a process for their preparation and their use as binders for coating compositions |
CN101372530A (en) * | 2008-08-08 | 2009-02-25 | 中国工程物理研究院化工材料研究所 | Water-based light-cured polyurethane resin and preparation method thereof |
-
2012
- 2012-09-28 CN CN201210369632.6A patent/CN102876223B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5300615A (en) * | 1992-09-24 | 1994-04-05 | Bayer Aktiengesellschaft | Polyurethanes containing acryloyl groups, a process for their preparation and their use as binders for coating compositions |
CN101372530A (en) * | 2008-08-08 | 2009-02-25 | 中国工程物理研究院化工材料研究所 | Water-based light-cured polyurethane resin and preparation method thereof |
Also Published As
Publication number | Publication date |
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CN102876223A (en) | 2013-01-16 |
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Owner name: ZHONGWU FUNCTION MATERIAL INSTITUTE CO., LTD. Free format text: FORMER OWNER: SICHUAN RESEARCH CENTER OF NEW MATERIALS Effective date: 20150209 |
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Free format text: CORRECT: ADDRESS; FROM: 610000 CHENGDU, SICHUAN PROVINCE TO: 518040 SHENZHEN, GUANGDONG PROVINCE |
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Effective date of registration: 20150209 Address after: 518040, Shenzhen, Guangdong, Futian District, Che Kung Temple Tian An Digital City Futian Tian Tian hi tech building A block 402 room Patentee after: SINOMATERIAL FUNCTION MATERIAL INSTITUTE CO.,LTD. Address before: 610000, No. 24, No. 1, south section of No. 1 Ring Road, Sichuan, Chengdu, No. 312 Patentee before: Sichuan Research Center of New Materials |
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Address after: 518040, Shenzhen, Guangdong, Futian District, Che Kung Temple Tian An Digital City Futian Tian Tian hi tech building A block 402 room Patentee after: LENGINE DEFENSE TECHNOLOGY GROUP CO.,LTD. Address before: 518040, Shenzhen, Guangdong, Futian District, Che Kung Temple Tian An Digital City Futian Tian Tian hi tech building A block 402 room Patentee before: SINOMATERIAL FUNCTION MATERIAL INSTITUTE CO.,LTD. |
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Denomination of invention: Environment Friendly Waterborne UV curing coating and its production method Effective date of registration: 20210208 Granted publication date: 20150204 Pledgee: Bank of Beijing Limited by Share Ltd. Shenzhen branch Pledgor: LENGINE DEFENSE TECHNOLOGY GROUP Co.,Ltd. Registration number: Y2021980001151 |
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Date of cancellation: 20220805 Granted publication date: 20150204 Pledgee: Bank of Beijing Limited by Share Ltd. Shenzhen branch Pledgor: LENGINE DEFENSE TECHNOLOGY GROUP CO.,LTD. Registration number: Y2021980001151 |