CN102871846A - Solid typed cosmetic formulation - Google Patents
Solid typed cosmetic formulation Download PDFInfo
- Publication number
- CN102871846A CN102871846A CN2012102385315A CN201210238531A CN102871846A CN 102871846 A CN102871846 A CN 102871846A CN 2012102385315 A CN2012102385315 A CN 2012102385315A CN 201210238531 A CN201210238531 A CN 201210238531A CN 102871846 A CN102871846 A CN 102871846A
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- CN
- China
- Prior art keywords
- wax
- cosmetic formulations
- solid cosmetic
- formulations according
- cosmetics
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/14—Liposomes; Vesicles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
Abstract
A method for manufacturing a solid cosmetic formulation is provided to ensure stability at high temperature and excellent skin applicability. CONSTITUTION: A method for manufacturing a solid cosmetic formulation comprises: a step of mixing wax, cosmetics, and emulsifier and melting; a step of adding purified water and uniformly stirring; a step of injecting to a mold; and a step of cooling the mold. The wax includes C30-45 alkyldimethyl silyl polypropyl silsesquioxane, stearyl dimethicone, ceresin wax, carnauba wax, micro crystalline wax, shea butter, mango butter, Japan wax, stearic acid, or glyceryl monoester.
Description
Technical field
The present invention relates to a kind of solid cosmetic formulations, in more detail, relate to a kind of shell that forms with the wax of sclerosis and form the outside, and have the solid cosmetic formulations of the cosmetics of colloidal sol (sol) state in inside.
Background technology
As rod and cake type solid cosmetics, the compact etc. that lip pomade, cosmetic pencil, wet-milling is generally arranged and powder is carried out extrusion forming.
These cosmetics and paste or aqueous cosmetics are different, require littlely for the difference of hardness of variations in temperature, must possess the what is called " temperature stability " that rod and cake can not flow out, can not scatter till the uniform temperature (about 45 ℃).
But, when consumer is adapted on the skin at normal temperatures, although be solid, can what is called " the skin suitability " soft and that smear equably outstanding.
But there are the each other one side of contradiction in above-mentioned " temperature stability " and " the skin suitability ", if although hardness is high or firm good thermal stability, when being adapted to skin, use sense not soft, exist to have the problem of the low skin suitability.
In addition, if a little less than the hardness, although then the skin suitability might be outstanding, the stability degradation of product at high temperature, thus might cause reducing storage property and as the problem of the value of product.
Therefore, currently need urgently to develop when having the effective skin suitability, keep suitable hardness and heat-staple prescription.
Summary of the invention
The present invention proposes in order to solve the conflicting problem of the skin suitability and hardness, and its purpose is, develops the solid prescription with outstanding heat stability and skin suitability.
The invention provides a kind of solid cosmetic formulations, the outside of this cosmetic formulations be by have 20～60 ℃ fusing point wax sclerosis and form shell, and have the cosmetics of colloidal sol (sol) state in inside.
In solid cosmetic formulations of the present invention, as an example of cosmetics, can be water-soluble substances, and the water solublity cosmetics can also comprise emulsifying agent.
The shape of solid cosmetic formulations of the present invention can be circle, quadrangle, hexagon, triangle, ellipse, cylindrical, rod, starlike, specific character shape etc.
In solid cosmetic formulations of the present invention, as an example of wax, can be more than any one that from the silica-based poly-propyl group silsesquioxane of C30-45 alkyl dimethyl, stearic polydimethylsiloxane, ceresin, palm wax, microwax, Adeps Bovis seu Bubali resin, Fructus Mangifera Indicae oil, Japan wax, stearic acid and monoglyceride, select.
Solid cosmetic formulations of the present invention is that the mode of packing separately cosmetics according to a use amount is used, and therefore can prevent the pollution by the caused exterior materials of Reusability of cosmetics, thereby can improve storage.
Solid cosmetic formulations of the present invention is at room temperature kept its shape, and on being placed on skin and can break with when pressurization finger.At this moment, expose to the outside at the cosmetics that are present in inside.The cosmetic composition that is exposed to skin mixes with the wax of crushing and is coated on the skin.When continuing rubbing with finger, because wax of the present invention has 20～60 ℃ fusing point, therefore can be by being melted by the pressure of finger pressurization and skin temperature and frictional heat.When wax melts, can when coating, give soft sense of touch, can not bring special sense of discomfort to user.If have than 20 ℃ of low fusing points, the problem that then exists hardness to descend if having than 60 ℃ of high fusing points, is not easy to melt when then existing on being applied to skin and reduces the problem of the skin suitability.
The shell of general disposable cosmetic capsules is made of the composition that skin produces sense of discomfort synthetic resin material etc., existing needs to separate and discarded inconvenience in addition in use, when the capsule pressure break, content breaks away from skin and splashes towards periphery, thereby can cause problems such as polluting clothes.
But, solid cosmetic formulations of the present invention, if continuation is crumpled with finger after the crust shell of pressure break wax composition, meeting is naturally melted and is applied on the skin with cosmetic composition, therefore can not cause above-mentioned problem.
On the other hand, the invention provides a kind of manufacture method of solid cosmetic formulations, it comprises: mix wax, cosmetics, emulsifying agent with 20～60 ℃ of fusing points, the step (a) that dissolves with the temperature of the fusing point that surpasses wax; After dissolving, adding purifies waste water stirs the step (b) of mixing with equably; After the stirring, be injected into the step (c) in the mould (mold); And be injected into after the mould, make mold cools down to the step (d) of the temperature of the fusing point that is lower than wax.Below, segment manufacture method of the present invention according to each step and describe.
Step (a): dissolve step
This step (a) is to mix wax, cosmetics, the emulsifying agent of the fusing point with 20～60 ℃, uses the temperature of the fusing point that surpasses wax to dissolve process.About the composition that when dissolving, mixes, except wax, cosmetics, emulsifying agent, all right mixed stabilizer, antiseptic, pigment, the various compositions of wet goods.In addition, can also mix simultaneously the performance whitening, improve functional liposoluble constituents such as wrinkle, ultraviolet blocking.
Dissolve so long as can melt as the above temperature of the wax of the main constituent in the composition that adds and get final product.
About the wax that adds, although also can use the wax of a plurality of kinds that differ from one another, also can use by the different wax of mixed melting point.As an example of wax, can be more than any one that from the silica-based poly-propyl group silsesquioxane of C30-45 alkyl dimethyl, stearic polydimethylsiloxane, ceresin, palm wax, microwax, Adeps Bovis seu Bubali resin, Fructus Mangifera Indicae oil, Japan wax, stearic acid and monoglyceride, select.About the wax composition, preferably add the amount of 0.10～40.00 % by weight of overall weight of the prescription of manufacturing.
On the other hand, when in step of the present invention (a), mixing, in order to give stability and the outstanding use sense under the high temperature, can append and add cyclopentasiloxane, polydimethylsiloxane, polydimethylsiloxane/Polyethylene Glycol-10/15 cross linked polymer, and the summation of preferably adding above-mentioned three compositions accounts for the amount of 0.10～30.00 % by weight in the whole weight of prescription of manufacturing.When content during less than 0.10 % by weight, gelatinous texture and viscosity are excessively low, when surpassing 30.00 % by weight, have the shortcoming that is not suitable as cosmetics owing to too stiff texture.
On the other hand, when in step of the present invention (a), mixing, can append the increase oil component, as an example, there are Cyclomethicone, polydimethylsiloxane, cyclopentasiloxane, stearol, cetearyl alcohol ethylhexoate, spermol ethylhexoate, isopropyl myristate, myristyl octyl dodecanol ester, caprylic/capric triglyceride, triglyceride etc.The composition of the oil that adds is preferably the amount of 1.00～50.00 % by weight in the overall weight of prescription of manufacturing.
On the other hand, when in step of the present invention (a), mixing, can append the interpolation pigment composition, as an example, there are titanium dioxide, Talcum, Muscovitum, zinc oxide, Margarita, aluminium stearate, polymethyl methacrylate, black iron oxide, red iron oxide, yellow iron oxide, silicon dioxide, nylon powder etc.The pigment composition that adds is preferably the amount of 1.00～90.00 % by weight in the overall weight of prescription of manufacturing.
Step (b): whipping step
This step is the process of purifying waste water and stirring of adding after dissolving.When stirring, can be mixed equably by the emulsifying agent that in above-mentioned steps, adds.At this moment, also water-soluble functional material or additive can be dissolved in the water and add.
About stirring, as long as carry out in the mode of mixing equably, preferably carried out 40～200 minutes.
Step (c): mould implantation step
This step is the step that is injected into mould (mold) after stirring.In this step, the mixture that will mix in above-mentioned steps (b) is injected into mould.Mould can have various shapes, determines the external shape of the solid cosmetic formulations of manufacturing according to its shape.
On the other hand, solid cosmetic formulations manufacture method of the present invention can also be appended the step (c-1) of carrying out vacuum outgas between step (b) and step (c).If append the execution vacuum outgas, then can more easily make the cosmetic formulations of solid, make the outward appearance commodity of prescription of manufacturing also outstanding.
Step (d): cooling step
This step is with the step of mold cools down to the temperature of the fusing point that is lower than wax after mould injects.After mould injected, if make the temperature of mould be reduced to the temperature of the fusing point that is lower than wax, then wax can harden, and finishes thus the shell of cosmetic formulations.
When the drop in temperature that makes mould was following to the fusing point of wax, the wax that is injected in the mixture in the mould can begin sclerosis, and begins sclerosis from the face side that contacts with mould.When the elapsed time, mould contact surface is hardened gradually and is formed shell, and the composition that can not harden is assembled and the content of formation colloidal sol (sol) state to the inboard.
When being judged as wax and having hardened fully, stop the cooling engineering.Carry out longways cooling step if cross, then being filled into inner material might freeze, and is worthless therefore.
The cooling engineering is preferably finished in (as an example, about-10 ℃) short time under the much lower temperature than the temperature of wax as far as possible.This is because by rapid temperature difference wax is promptly hardened.
The invention effect
Although solid cosmetic formulations hardness of the present invention is not high, at high temperature stable, when being adapted to skin, the wax layer that forms shell melts and raising use sense, therefore also has the outstanding characteristics of the skin suitability.
The specific embodiment
Below, in following embodiment, further describe content of the present invention.But claim of the present invention is not limited to following embodiment, also comprises the distortion of the technological thought that is equal to following examples.
Embodiment 1～14: the manufacturing of solid cosmetic formulations of the present invention
[table 1]
After mixing is recorded in composition 1～34 in the above-mentioned table 1, heats and dissolve.Afterwards, composition 35,36,38 is being put into above-mentioned 1) in after, stir equably more than 40 minutes.Carry out vacuum outgas after stirring, drop into composition 37.Afterwards, after being injected into the spherical mould that diameter is 10mm, make its molding make the solid cosmetic formulations of embodiment 1～14.
The organoleptic test of experimental example: embodiment 1～14
Take 50 20～30 years old women as object, make them carry embodiment product 3 months and the use of above-mentioned manufacturing, implement afterwards to heat stability, product hardness, use the organoleptic test of sense, resistance to water and color representation and be evaluated as 4 ranks, its result is illustrated in the table 2.
[table 2]
As from above-mentioned table 2 as can be known, show good heat stability, hardness and use sense all of embodiment 1～14.
But, the embodiment 1～4 that comprises the amount of cyclopentasiloxane, polydimethylsiloxane, polydimethylsiloxane/Polyethylene Glycol-10/15 cross linked polymer and the combination of suitable wax compares and contains excessive or a small amount of cyclopentasiloxane, polydimethylsiloxane, polydimethylsiloxane/Polyethylene Glycol-10/15 cross linked polymer, the embodiment 5～14 that perhaps shows not too suitable wax combination shows more outstanding heat stability, uses sense, color representation and resistance to water etc.
Claims (10)
1. a solid cosmetic formulations is characterized in that,
The outside of this cosmetic formulations be by have 20～60 ℃ fusing point wax sclerosis and form shell, and have the cosmetics of colloidal sol (sol) state in inside.
2. solid cosmetic formulations according to claim 1 is characterized in that,
Described cosmetics have water solublity.
3. solid cosmetic formulations according to claim 2 is characterized in that,
Described water solublity cosmetics comprise emulsifying agent.
4. solid cosmetic formulations according to claim 1 is characterized in that,
Described wax is more than any one that select from the silica-based poly-propyl group silsesquioxane of C30-45 alkyl dimethyl, stearic polydimethylsiloxane, ceresin, palm wax, microwax, Adeps Bovis seu Bubali resin, Fructus Mangifera Indicae oil, Japan wax, stearic acid and monoglyceride.
5. the manufacture method of a solid cosmetic formulations is characterized in that, comprising:
Mix wax, cosmetics, emulsifying agent with 20～60 ℃ of fusing points, the step (a) that dissolves with the temperature of the fusing point that surpasses wax;
After dissolving, adding purifies waste water stirs the step (b) of mixing with equably;
After the stirring, be injected into the step (c) in the mould (mold); And
Be injected into after the mould, make mold cools down to the step (d) of the temperature of the fusing point that is lower than wax.
6. the manufacture method of solid cosmetic formulations according to claim 5 is characterized in that,
About the wax of described step (a), use the wax of a plurality of kinds that differ from one another.
7. the manufacture method of solid cosmetic formulations according to claim 5 is characterized in that,
The wax of described step (a) is more than any one that select from the silica-based poly-propyl group silsesquioxane of C30-45 alkyl dimethyl, stearic polydimethylsiloxane, ceresin, palm wax, microwax, Adeps Bovis seu Bubali resin, Fructus Mangifera Indicae oil, Japan wax, stearic acid and monoglyceride.
8. the manufacture method of solid cosmetic formulations according to claim 5 is characterized in that,
When in described step (a), mixing, append adding cyclopentasiloxane, polydimethylsiloxane, polydimethylsiloxane/Polyethylene Glycol-10/15 cross linked polymer.
9. the manufacture method of solid cosmetic formulations according to claim 5 is characterized in that,
The stirring of described step (b) is to carry out 40～200 minutes.
10. the manufacture method of solid cosmetic formulations according to claim 5 is characterized in that, between described step (b) and step (c), appends the step (c-1) of carrying out vacuum outgas.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2011-0070119 | 2011-07-14 | ||
| KR1020110070119A KR101133098B1 (en) | 2011-07-14 | 2011-07-14 | Solid typed cosmetic formulation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102871846A true CN102871846A (en) | 2013-01-16 |
Family
ID=46143221
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012102385315A Pending CN102871846A (en) | 2011-07-14 | 2012-07-11 | Solid typed cosmetic formulation |
Country Status (2)
| Country | Link |
|---|---|
| KR (1) | KR101133098B1 (en) |
| CN (1) | CN102871846A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107982095A (en) * | 2017-10-19 | 2018-05-04 | 珀莱雅化妆品股份有限公司 | A kind of preparation method with crease-resistant slow-release solid microballoon |
| CN108883053A (en) * | 2016-04-04 | 2018-11-23 | 株式会社 Lg 生活健康 | Hide the make-up composition of wrinkle |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101450387B1 (en) | 2012-04-17 | 2014-10-14 | 양승호 | Thermal stable solid formulation of water in oil type emulsion |
| GB2507522B (en) | 2012-11-01 | 2014-12-31 | Cosmetic Warriors Ltd | Solid cosmetic composition |
| KR101692769B1 (en) * | 2016-07-29 | 2017-01-05 | 주식회사 나우코스 | Cosmetic composition for skin cooing and make-up comprising phase transition wax |
| KR101984277B1 (en) * | 2016-09-23 | 2019-05-30 | 주식회사 엘지생활건강 | Cosmetics concealing wrinkles |
| KR102159744B1 (en) * | 2018-10-29 | 2020-09-24 | 주식회사 러브바드 | Solid Cosmetic Composition with Improved Stability and Method for Preparing Same |
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| US20040223989A1 (en) * | 2003-04-30 | 2004-11-11 | L'oreal | Water-in-oil solid emulsion-type cosmetic compositions |
| US20080089913A1 (en) * | 2003-08-27 | 2008-04-17 | Beiersdorf Ag | Capsule Whose Envelope Is Separately Imperceptible During The Topical Use Thereof |
| CN101606901A (en) * | 2008-06-20 | 2009-12-23 | 赢创德固赛(中国)投资有限公司 | Lipstick with high water content and preparation method thereof |
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| FR2721210B1 (en) * | 1994-06-17 | 1996-08-02 | Oreal | Cleaning composition containing lipid grains. |
| DE10353780A1 (en) | 2003-11-18 | 2005-06-23 | Beiersdorf Ag | Particles comprising solid wax shell and polyol core, useful for incorporating moisture-sensitive and/or water-insoluble active agents into cosmetic and/or dermatological formulations |
| US7622132B2 (en) * | 2005-06-27 | 2009-11-24 | Elc Management, Llc | Encapsulated cosmetic composition |
| KR101053471B1 (en) * | 2008-10-09 | 2011-08-03 | 한불화장품주식회사 | Manufacturing method of solid wax microcapsules containing functional material and cosmetic composition containing same |
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2011
- 2011-07-14 KR KR1020110070119A patent/KR101133098B1/en active IP Right Grant
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2012
- 2012-07-11 CN CN2012102385315A patent/CN102871846A/en active Pending
Patent Citations (3)
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| US20040223989A1 (en) * | 2003-04-30 | 2004-11-11 | L'oreal | Water-in-oil solid emulsion-type cosmetic compositions |
| US20080089913A1 (en) * | 2003-08-27 | 2008-04-17 | Beiersdorf Ag | Capsule Whose Envelope Is Separately Imperceptible During The Topical Use Thereof |
| CN101606901A (en) * | 2008-06-20 | 2009-12-23 | 赢创德固赛(中国)投资有限公司 | Lipstick with high water content and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108883053A (en) * | 2016-04-04 | 2018-11-23 | 株式会社 Lg 生活健康 | Hide the make-up composition of wrinkle |
| CN107982095A (en) * | 2017-10-19 | 2018-05-04 | 珀莱雅化妆品股份有限公司 | A kind of preparation method with crease-resistant slow-release solid microballoon |
| CN107982095B (en) * | 2017-10-19 | 2020-03-27 | 珀莱雅化妆品股份有限公司 | Preparation method of sustained-release solid microspheres with anti-wrinkle effect |
Also Published As
| Publication number | Publication date |
|---|---|
| KR101133098B1 (en) | 2012-04-04 |
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Application publication date: 20130116 |