CN102850965B - Binder, preparation method of the binder and insect bonding plate coated with the binder - Google Patents
Binder, preparation method of the binder and insect bonding plate coated with the binder Download PDFInfo
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- CN102850965B CN102850965B CN201210287373.2A CN201210287373A CN102850965B CN 102850965 B CN102850965 B CN 102850965B CN 201210287373 A CN201210287373 A CN 201210287373A CN 102850965 B CN102850965 B CN 102850965B
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Abstract
The invention discloses a binder, a preparation method of the binder and an insect bonding plate coated with the binder. The binder is prepared from 2 to 7 parts by weight of high-molecular weight solid polyisobutene, 10 to 20 parts by weight of intermediate-molecular weight solid polyisobutene, 30 to 50 parts by weight of liquid polyisobutene, 10 to 20 parts by weight of rubber oil, 12 to 25 parts by weight of hydrogenated petroleum resin, 4 to 10 parts by weight of an amorphous alpha-olefin copolymer, 0.5 to 0.8 parts by weight of an antioxidant and 0.5 to 0.8 parts by weight of an ultraviolet light absorber. The binder has a high resource utilization rate, can be used in the open air for a period of 6-8 weeks, belongs to a hot melt adhesive and does not damage the environment and people and livestock.
Description
Technical field
The present invention relates to binding agent, particularly relate to the binding agent for the insect that bonds etc.
The invention still further relates to the preparation method of above-mentioned binding agent.
The invention still further relates to the pest haftplatte that is coated with above-mentioned binding agent.
Background technology
Viscose glue on the haftplatte of the sticky pest type of selling on market now, the performance that it is ageing-resistant, UV resistant is irradiated is all lower, and the time that it is used out of doors is continuously shorter, generally about 2 week, has just lost the effect of sticky insect, replacement frequency is higher, causes the waste of resource.
Summary of the invention
The present invention completes in order to solve deficiency of the prior art, the utilization ratio that the object of this invention is to provide resource is high, the binding agent that can use out of doors for a long time, can reach 6-8 week its duration of service out of doors, and binding agent itself belongs to hot melt adhesive, the binding agent to environment, person poultry harmless.
Binding agent of the present invention, it is prepared from by following proportioning according to weight ratio: 2-7 part high molecular solid polyisobutene, the solid polyisobutene of molecular weight in 10-20 part, 30-50 part liquid polyisobutene, 10-20 rubber oil, 12-25 part hydrogenated petroleum resin, 4-10 part non-crystalline state alpha-olefin copolymer, 0.5-0.8 part oxidation inhibitor and 0.5-0.8 part UV light absorber.
Binding agent of the present invention can also be:
Described non-crystalline state alpha-olefin copolymer is: a kind of in the APAO-888 of Degussa, APAO-828 and APAO-608.
Described oxidation inhibitor is three [2,4-di-tert-butyl-phenyl] phosphorous acid ester or AT10, described UV light absorber is 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole or 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole.
Binding agent of the present invention, because it is prepared from by following proportioning according to weight ratio: 2-7 part high molecular solid polyisobutene, the solid polyisobutene of molecular weight in 10-20 part, 30-50 part liquid polyisobutene, 10-20 rubber oil, 12-25 part hydrogenated petroleum resin, 4-10 part non-crystalline state alpha-olefin copolymer, 0.5-0.8 part oxidation inhibitor and 0.5-0.8 part UV light absorber.Like this, the utilization ratio of resource is high, the binding agent that can use out of doors for a long time, and can reach 6-8 week its duration of service out of doors, and binding agent itself belongs to hot melt adhesive, to environment, person poultry harmless.
The utilization ratio that another object of the present invention is to provide resource is high, the binding agent that can use out of doors for a long time, and can reach 6-8 week its duration of service out of doors, and binding agent itself belongs to hot melt adhesive, the preparation method to environment, person poultry harmless's binding agent.
Binding agent preparation method of the present invention, comprises the following steps:
A. the high molecular solid polyisobutene of 2 parts-7 parts of part by weight and the liquid polyisobutene of the 5%-25% of the high molecular solid polyisobutene quality adding are put into pressurization rubber mixing machine, mixing under the pressure of 0.2-0.6Mpa, mixing 0.4-1 hour;
B. by the mixture of the high molecular solid polyisobutene having refined and liquid polyisobutene and remaining whole liquid polyisobutene, the oxidation inhibitor of 0.2 part-0.3 part, join in glue still, under the condition of 140 ℃-180 ℃ of normal pressures, temperature, stir 10-20 hour;
C. after the mixture of the high molecular weight polyisobutylene having refined and liquid polyisobutene and remaining liquid polyisobutene are fully mixed, the rubber oil that adds 10 parts-20 parts, the solid polyisobutene of the middle molecular weight of 10 parts-20 parts, 5 parts of-10 parts of non-crystalline state alpha-olefin copolymers, the hydrogenated petroleum resin of 12 parts-25 parts continues to stir 2-4 hour under the condition of 140 ℃-180 ℃ of normal pressures, temperature;
D. after various materials fully mix in still, add remaining oxidation inhibitor, the UV light absorber of 0.5 part-0.8 part, gets final product discharging after stirring 30min.
Owing to having adopted above-mentioned steps, system binding agent utilization ratio high, the binding agent that can use out of doors for a long time, can reach 6-8 week its duration of service out of doors, and binding agent itself belongs to hot melt adhesive, to environment, person poultry harmless.
Another object of the present invention be resource utilization high, provide to reach 6-8 week duration of service out of doors, and binding agent itself belongs to hot melt adhesive, the mouse sticking plate to environment, person poultry harmless.
Mouse sticking plate of the present invention, comprises the positive and plate body back side of plate body, the described plate body front surface coated binding agent described in requirement 1 or 2 of having the right.
Mouse sticking plate of the present invention in terms of existing technologies, the advantage having be resource utilization high, provide to reach 6-8 week duration of service out of doors, and binding agent itself belongs to hot melt adhesive, to environment, person poultry harmless.
Accompanying drawing explanation
Fig. 1 the present invention is coated with binding agent mouse sticking plate embodiment front schematic view.
Figure number explanation
1 ... plate body 2 ... binding agent
Embodiment
Below in conjunction with Fig. 1 of accompanying drawing, binding agent of the present invention, its preparation method and the pest haftplatte that applies it are described in further detail.
Binding agent of the present invention, please refer to Fig. 1, it is prepared from by following proportioning according to weight ratio: 2-7 part high molecular solid polyisobutene, the solid polyisobutene of molecular weight in 10-20 part, 30-50 part liquid polyisobutene, 10-20 rubber oil, 12-25 part hydrogenated petroleum resin, 4-10 part non-crystalline state alpha-olefin copolymer, 0.5-0.8 part oxidation inhibitor and 0.5-0.8 part UV light absorber.The material of concrete analysis molecular weight between 350 to 3500 claims low-molecular-weight polyisobutylene, and molecular weight is middle molecular weight products between 10,000 to 100,000, and molecular weight is high molecular weight products between 100,000 to 10,000,000.Molecular weight is in a liquid state conventionally at the product below 30,000, and the material that molecular weight is higher is solid-state.The producer of liquid polyisobutene and model are: Korea S great Lin, PB-1300; Non-crystalline state alpha-olefin copolymer is: the APAO-888 of Degussa, APAO-828, APAO-608; Oxidation inhibitor: AT10, irgasfos 168; UV light absorber: 326,329.
Because starting material used, its molecular structure is saturated structures, ageing resistance is fine, sizing agent system is these several raw-material physical mixed, in mixing process, there is not chemical reaction, each component still keeps saturated structures in sizing agent system, and institute is so that sizing agent also has good ageing resistance.Can use out of doors for a long time, can reach 6-8 week duration of service out of doors.Duration of service is longer, has reduced and has changed the number of times of product, thereby improved the utilization ratio of resource.And binding agent itself belongs to hot melt adhesive, in glue goods, containing solvent, can not send harmful toxic smog, to environment, person poultry harmless yet.
Binding agent of the present invention can also be that described non-crystalline state alpha-olefin copolymer is: a kind of in the APAO-888 of Degussa, APAO-828 and APAO-608.。Adopt non-crystalline state alpha-olefin copolymer can improve sizing agent system force of cohesion, be conducive to peeling off and reducing costs of protection sheet, the APAO-888 of Degussa, APAO-828, APAO-608 constant product quality, can guarantee the stable of pest haftplatte quality.Can also be that described oxidation inhibitor is three [2,4-di-tert-butyl-phenyl] phosphorous acid ester or AT10, described UV light absorber is 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole or 2 ' (2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole.Adopt oxidation inhibitor and UV light absorber can prevent raw-material degradation with aging in glue process and affect performance and increase the time that product is used out of doors.
The preparation method of binding agent of the present invention, comprises the following steps:
A. the high molecular solid polyisobutene of 2 parts-7 parts of part by weight and the liquid polyisobutene of the 5%-25% of the high molecular solid polyisobutene quality adding are put into pressurization rubber mixing machine, mixing under the pressure of 0.2-0.6Mpa, mixing 0.4-1 hour;
B. by the mixture of the high molecular solid polyisobutene having refined and liquid polyisobutene and remaining whole liquid polyisobutene, the oxidation inhibitor of 0.2 part-0.3 part, join in glue still, under the condition of 140 ℃-180 ℃ of normal pressures, temperature, stir 10-20 hour;
C. after the mixture of the high molecular weight polyisobutylene having refined and liquid polyisobutene and remaining liquid polyisobutene are fully mixed, the rubber oil that adds 10 parts-20 parts, the solid polyisobutene of the middle molecular weight of 10 parts-20 parts, 5 parts of-10 parts of non-crystalline state alpha-olefin copolymers, the hydrogenated petroleum resin of 12 parts-25 parts continues to stir 2-4 hour under the condition of 140 ℃-180 ℃ of normal pressures, temperature;
D. after various materials fully mix in still, add remaining oxidation inhibitor, the UV light absorber of 0.5 part-0.8 part, gets final product discharging after stirring 30min.
The utilization ratio that can obtain resource by above-mentioned steps is high, the binding agent that can use out of doors for a long time, and can reach 6-8 week its duration of service out of doors, and binding agent itself belongs to hot melt adhesive, the binding agent to environment, person poultry harmless.Further preferred technical scheme is that described oxidation inhibitor is three [2,4-di-tert-butyl-phenyl] phosphorous acid ester or AT10, described UV light absorber is 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole or 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole.Adopt oxidation inhibitor and UV light absorber can prevent in glue process raw-material degradation with aging and increase the time that product is used out of doors.
The present invention also provides the sticky insect plate that is coated with above-mentioned binding agent, please refer to Fig. 1, comprises positive and plate body 1 back side of plate body 1, the described plate body 1 front surface coated binding agent 2 described in requirement 1 or 2 of having the right.Like this, above-mentioned binding agent 2 is coated in plate body 1 front for the insect that bonds.The advantage of such pest haftplatte be resource utilization high, provide to reach 6-8 week duration of service out of doors, and binding agent itself belongs to hot melt adhesive, to environment, person poultry harmless.The upper surface that further preferred technical scheme is described binding agent is coated with the protection sheet of easily openable.The effect of protection sheet is that protection viscose glue avoids it folding, to affect in use and transportation and be stained with dust etc.
Example one
Proportioning raw materials: high molecular weight polyisobutylene: 3.9 parts; Middle molecular weight polyisoprene iso-butylene: 15 parts; Liquid polyisobutene: 41 parts; Rubber oil: 13.9 parts; Hydrogenated petroleum resin: 20 parts; Degussa APAO-888:5 part; AT10:0.6 part; UV light absorber 326:0.6 part.
Making method:
(1) liquid polyisobutene of the high molecular weight polyisobutylene of 3.9 parts and 0.4 part is put into rubber mixing machine, mixing under the pressure of 0.2Mpa, mixing 0.6 hour;
(2) by the mixture of the high molecular solid polyisobutene having refined and liquid polyisobutene, the liquid polyisobutene of 40.6 parts, the oxidation inhibitor of 0.3 part, joins in glue still.Under the condition of 160 ℃ of normal pressures, temperature, stir 15 hours;
(3) after the liquid polyisobutene of the mixture of the high molecular weight polyisobutylene having refined and liquid polyisobutene and 40.6 parts is fully mixed, the rubber oil that adds 13.9 parts, the middle molecular weight solid polyisobutene of 15 parts, the Degussa APAO-888 of 5 parts, the hydrogenated petroleum resin of 20 parts continues to stir 3 hours under the condition of 160 ℃ of normal pressures, temperature;
(4) after in still, various materials fully mix, add the oxidation inhibitor of 0.3 part, the UV light absorber of 0.6 part, gets final product discharging after stirring 30min.
Application step:
(1) binding agent of making is joined in hot melt coating machine, set and add 160 ℃ of hot glue case temperature, 170 ℃ of coater head temperature, single spreading amount is 65g/m
2,, each technic index complete when setting can be coated with after all reaching set(ting)value;
(2), by coated product, the corresponding regulation of peace cuts, cases.
Example two
High molecular weight polyisobutylene: 7 parts; Middle molecular weight polyisoprene iso-butylene: 20 parts; Liquid polyisobutene: 50 parts; Rubber oil: 20 parts; Hydrogenated petroleum resin: 25%; Degussa APAO-828:10 part; AT10:0.6 part; UV light absorber 326:0.8 part.
Preparation method
(1) liquid polyisobutene of the high molecular weight polyisobutylene of 7 parts and 0.4 part is put into rubber mixing machine, mixing under the pressure of 0.5Mpa, mixing 0.6 hour;
(2) by the mixture of the high molecular solid polyisobutene having refined and liquid polyisobutene, the liquid polyisobutene of 40.6 parts, the oxidation inhibitor of 0.3 part, joins in glue still, under the condition of 160 ℃ of normal pressures, temperature, stirs 15 hours.
(3) after the liquid polyisobutene of the mixture of the high molecular weight polyisobutylene having refined and liquid polyisobutene and 40.6 parts is fully mixed, the rubber oil that adds 20 parts, the middle molecular weight solid polyisobutene of 20 parts, the Degussa APAO-828 of 10 parts, the hydrogenated petroleum resin of 25 parts continues to stir 3 hours under the condition of 160 ℃ of normal pressures, temperature.
(4) after in still, various materials fully mix, add the oxidation inhibitor of 0.3 part, the UV light absorber of 0.8 part, can discharging obtain the binding agent needing after stirring 30min.
(5) sizing agent of making is joined in hot melt coating machine, set and add 160 ℃ of hot glue case temperature, 170 ℃ of coater head temperature, single spreading amount is 65g/m
2,, each technic index complete when setting can be coated with after all reaching set(ting)value.
(6), by coated product, the corresponding regulation of peace cuts, cases.
Example three
High molecular weight polyisobutylene: 2 parts; Middle molecular weight polyisoprene iso-butylene: 10 parts; Liquid polyisobutene: 35 parts; Rubber oil: 17.9 parts; Hydrogenated petroleum resin: 20 parts; Degussa APAO-608:10 part; AT10:0.8 part; UV light absorber 326:0.8 part.
Preparation method:
(1) liquid polyisobutene of the high molecular weight polyisobutylene of 2 parts and 0.5 part is put into rubber mixing machine, mixing under the pressure of 0.6Mpa, mixing 0.6 hour.
(2) by the mixture of the high molecular solid polyisobutene having refined and liquid polyisobutene, the liquid polyisobutene of 34.6 parts, the AT10 of 0.3 part, joins in glue still.Under the condition of 160 ℃ of normal pressures, temperature, stir 15 hours.
(3) after the liquid polyisobutene of the mixture of the high molecular weight polyisobutylene having refined and liquid polyisobutene and 34.5 parts is fully mixed, the rubber oil that adds 17.9 parts, the middle molecular weight solid polyisobutene of 10 parts, the Degussa APAO-608 of 10 parts, the hydrogenated petroleum resin of 20 parts continues to stir 3 hours under the condition of 160 ℃ of normal pressures, temperature.
(4) after in still, various materials fully mix, add the oxidation inhibitor of 0.5 part, the UV light absorber of 0.8 part, stirs after 30min the binding agent of needs that can discharging system.
(5) sizing agent of making is joined in hot melt coating machine, set and add 160 ℃ of hot glue case temperature, 170 ℃ of coater head temperature, single spreading amount is 65g/m
2,, each technic index complete when setting can be coated with after all reaching set(ting)value.
(6), by coated product, the corresponding regulation of peace cuts, cases.
Above-described embodiment is through experimental test, and the result of test is as following table:
Table one: embodiment table with test results
Above-mentionedly only several specific embodiments in the present invention are illustrated; but can not be as protection scope of the present invention; every equivalence variation of having done according to the design spirit in the present invention or modification or equal proportion zoom in or out etc., all should think and fall into protection scope of the present invention.
Claims (5)
1. binding agent preparation method, it is characterized in that: by following proportioning, be prepared from: 2-7 part high molecular solid polyisobutene, the solid polyisobutene of molecular weight in 10-20 part, 30-50 part liquid polyisobutene, 10-20 part rubber oil, 12-25 part hydrogenated petroleum resin, 5-10 part non-crystalline state alpha-olefin copolymer, 0.5-0.8 part oxidation inhibitor and 0.5-0.8 part UV light absorber, the solid polyisobutene of molecular weight between 10,000 to 100,000 is middle molecular weight solid polyisobutene, the solid polyisobutene of molecular weight between 100,000 to 10,000,000 is high molecular solid polyisobutene, and comprise the following steps:
A. the high molecular solid polyisobutene of 2 parts-7 parts of part by weight and the liquid polyisobutene of the 5%-25% of the high molecular solid polyisobutene quality adding are put into pressurization rubber mixing machine, mixing under the pressure of 0.2-0.6Mpa, mixing 0.4-1 hour;
B. by the mixture of the high molecular solid polyisobutene having refined and liquid polyisobutene and remaining whole liquid polyisobutene, the oxidation inhibitor of 0.2 part-0.3 part, join in glue still, under the condition of 140 ℃-180 ℃ of normal pressures, temperature, stir 10-20 hour;
C. after the mixture of the high molecular weight polyisobutylene having refined and liquid polyisobutene and remaining liquid polyisobutene are fully mixed, the rubber oil that adds 10 parts-20 parts, the solid polyisobutene of the middle molecular weight of 10 parts-20 parts, 5 parts of-10 parts of non-crystalline state alpha-olefin copolymers, the hydrogenated petroleum resin of 12 parts-25 parts continues to stir 2-4 hour under the condition of 140 ℃-180 ℃ of normal pressures, temperature;
D. after various materials fully mix in still, add remaining oxidation inhibitor, the UV light absorber of 0.5 part-0.8 part, gets final product discharging after stirring 30min.
2. binding agent preparation method according to claim 1, it is characterized in that: described oxidation inhibitor is three [2,4-di-tert-butyl-phenyl] phosphorous acid ester or AT10, described UV light absorber is 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole.
3. the pest haftplatte that is coated with binding agent prepared by the binding agent preparation method described in claim 1 or 2, is characterized in that: comprise the positive and plate body back side of plate body, the described plate body front surface coated binding agent described in requirement 1 or 2 of having the right.
4. be coated with according to claim 3 the pest haftplatte of binding agent prepared by binding agent preparation method, it is characterized in that: described oxidation inhibitor is three [2,4-di-tert-butyl-phenyl] phosphorous acid ester or AT10, described UV light absorber is 2 '-(2 '-hydroxyl-3 '-tertiary butyl-5 '-aminomethyl phenyl)-5-chlorobenzotriazole.
5. the pest haftplatte that is coated with according to claim 3 binding agent prepared by binding agent preparation method, is characterized in that: the upper surface of described binding agent is coated with the protection sheet of easily openable.
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| CN103497711B (en) * | 2013-08-07 | 2015-11-11 | 佛山力得高科技有限公司 | Sticky mouse glue and preparation method thereof |
| CN107141619B (en) * | 2017-04-20 | 2020-10-23 | 杭州福斯特应用材料股份有限公司 | Polyisobutylene backboard with ultralow water vapor transmittance |
| CN107099267A (en) * | 2017-05-27 | 2017-08-29 | 浙江固特热熔胶有限公司 | The high just viscous cockroach glue of low temperature |
| CN111269668B (en) * | 2020-03-27 | 2021-01-26 | 山东双圆密封科技有限公司 | Exposed flexible flashing sealing repairing adhesive tape and preparation method thereof |
| CN111777971A (en) * | 2020-07-15 | 2020-10-16 | 厦门祺星新材料有限公司 | Low-tensile-strength hot melt adhesive and preparation method and application thereof |
| CN115521733A (en) * | 2022-10-24 | 2022-12-27 | 苏州绿力士生物科技有限公司 | Mouse sticking glue and preparation method thereof |
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