CN102824882B - Circular inverted cone type bubbling stirred tank reactor - Google Patents

Circular inverted cone type bubbling stirred tank reactor Download PDF

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Publication number
CN102824882B
CN102824882B CN201210270096.4A CN201210270096A CN102824882B CN 102824882 B CN102824882 B CN 102824882B CN 201210270096 A CN201210270096 A CN 201210270096A CN 102824882 B CN102824882 B CN 102824882B
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China
Prior art keywords
circular arc
bubbler
back taper
reactor
air inlet
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Expired - Fee Related
Application number
CN201210270096.4A
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Chinese (zh)
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CN102824882A (en
Inventor
马晶
王济刚
高红鹰
于明
朱金璇
牟宗刚
鲍猛
王晓轩
李平
倪献智
矫强
许崇娟
许华芳
殷建玲
李倩
李敏
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University of Jinan
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University of Jinan
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Priority to CN201210270096.4A priority Critical patent/CN102824882B/en
Publication of CN102824882A publication Critical patent/CN102824882A/en
Application granted granted Critical
Publication of CN102824882B publication Critical patent/CN102824882B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The invention relates to the technical field of bubbling stirred tank reactors. A circular inverted cone bubbling stirred tank reactor provided by the invention comprises a reaction kettle, a circular inverted cone bubbler, an inlet valve, an air inlet pipe, a discharge valve, a discharging pipe, bubbling holes, a connecting device, etc. The circular inverted cone bubbler is installed at a central part at the lower part of the reaction kettle and is connected with the air inlet pipe; the air inlet pipe is provided with the inlet valve; the bottom of the reaction kettle is connected with the discharging pipe, and the discharging pipe is provided with the discharge valve; the circular inverted cone bubbler is provided with N bubbling holes with varying directions; the external surface of the circular inverted cone bubbler is in a streamline shape, flowing resistance of a fluid is small, the moving trajectory of agitated bubbles is long, continuous stirring effects last for a long time, and high stirring efficiency is obtained; the bubbling holes are located at the lower part of a circular inverted cone, and bubbles move along an inclined downward direction at first and act on the bottom of the reaction kettle, leaving no stirring dead angle.

Description

Circular arc inverted-cone bubbling stirred autoclave
Technical field
The present invention relates to bubbling stirred autoclave technical field.
Background technology
In Chemical Manufacture, for making the abundant hybrid reaction of liquid-solid phase material, in reactor, can stir in bubbling mode.The bubbling agitating device Chinese patent CN201887067U of prior art discloses bubbling stirring-type liquid-replenishing device with texturing tank, its complex structure, adopt the bubbling form of the venthole in square tube, air-flow is realized the stirring to material in retort with the venthole of horizontal direction vertically upward by square tube, this kind of agitating device, the deficiency existing, first venthole vertically upward, initial velocity direction is vertically upward, the ascent rate of bubble is also vertically upward, after bubble disengagement venthole, hightail reaction interface with the synthetic upward velocity direction of two speed, stirring efficiency is low, therefore power consumption is large, it two easily forms and stirs dead angle in reactor bottom, it three is multiple bubbling mixing components, is placed in bottom, and complex structure easily stops up, is unfavorable for to clean.Application number is that 200910252129.0 Chinese patent is simple in structure, clean and maintenance is convenient, but exist equally reactor bottom to be prone to stir dead angle and initial velocity direction is vertically upward, the ascent rate of bubble is also vertically upward, after bubble disengagement venthole, hightail reaction interface, the defect that power consumption is large, stirring efficiency is low with the synthetic upward velocity direction of two speed.
Summary of the invention
The defect existing in order to overcome above-mentioned prior art, the object of the present invention is to provide a kind of can directly act on reactor bottom deposition solid phase, stirring efficiency is high, power consumption is low, without stir dead angle, simple in structure, be easy to install, simple to operate, not susceptible to plugging bubbling stirred autoclave.
The technical solution used in the present invention comprises reactor 1, circular arc back taper bubbler 2, intake valve 3, air inlet pipe 4, outlet valve 5, discharge nozzle 6, bubble holes 21, interior tightening screw 22, interior sealing gasket 23, external seal pad 24, outer tightening screw 25, common fine thread 26, taper pipe thread 27, it is characterized in that reactor 1 lower central place is equipped with circular arc back taper bubbler 2, circular arc back taper bubbler 2 connects air inlet pipe 4, and intake valve 3 is housed in air inlet pipe 4; Reactor 1 bottom connects discharge nozzle 6, and outlet valve 5 is housed on discharge nozzle 6; Described circular arc back taper bubbler is characterized in that outer surface is similar to circular arc reverse taper, and back taper bottom surface is the arc surface of evagination, and back taper side is inside recessed cambered surface, has the bubble holes 21 of N equal aperture on the inner concave arc surface of back taper side.
Described circular arc back taper bubbler 2 back taper bottom surfaces are excessively connected with side circular arc.
The opening direction of N bubble holes 21 on described circular arc back taper bubbler 2 changes with the inner concave arc surface of back taper side, by laterally downward gradually.
In described air inlet pipe 4, there is common fine thread 26 to be connected with reactor by interior tightening screw 22, interior sealing gasket 23, external seal pad 24, outer tightening screw 25 with taper pipe thread 27.
Described circular arc back taper bubbler 2 bottom surface diameters and reactor diameter ratio are 1: 4.
Beneficial effect
The bubble bloating by the bubble holes 21 on circular arc back taper bubbler 2 is realized the stirring to liquid-solid material in reactor, bubble is because of the opening direction difference of the bubble holes 21 on circular arc back taper bubbler 2, the bubble initial velocity direction that different bubble holes overflow is from down to up by laterally downward direction transition gradually, directly act on reactor bottom, do not stay and stir dead angle;
Bubble holes is in the bottom of circular arc reverse taper, and bubble first oliquely downward moves, and is subject to the resistance of the material that reactor is stirred, and speed slows down gradually, and finally moved upward by the effect of material buoyancy.Stirring bubble running orbit is that circuit is long, continues the stirring action time long, and stirring efficiency is high, can reduce power consumption.
Circular arc back taper bubbler 2 outer surfaces are circular arc streamlined, and the flow resistance of convection cell is little;
Bubble holes 21 openings are positioned at circular arc back taper bubbler 2 belows, are difficult for being stopped up by solid material;
Circular arc back taper bubbler 2 volume urine are in the cleaning to reactor;
Circular arc back taper bubbler 2 is simple in structure, is convenient to install and change, with low cost.
Brief description of the drawings
Fig. 1: circular arc inverted-cone bubbling stirred autoclave schematic diagram;
Fig. 2: circular arc back taper bubbler 2 partial sectional views;
Fig. 3: circular arc back taper bubbler 2 upward views;
The local amplification profile of Fig. 4: I; Fig. 5: air inlet pipe 4 partial enlarged drawings.
In figure: 1 reactor, 2 circular arc back taper bubblers, 3 intake valves, 4 air inlet pipe, 5 outlet valves, 6 discharge nozzles, 21 bubble holes, 22 interior tightening screws, 23 interior sealing gaskets, 24 external seal pads, 25 outer tightening screws, 26 common fine threads, 27 taper pipe threads.
Detailed description of the invention
Below in conjunction with drawings and Examples, the present invention will be further described.
Embodiment
Circular arc inverted-cone bubbling stirred autoclave comprises reactor 1, circular arc back taper bubbler 2, intake valve 3, air inlet pipe 4, outlet valve 5, discharge nozzle 6, bubble holes 21, interior tightening screw 22, interior sealing gasket 23, external seal pad 24, outer tightening screw 25, common fine thread 26, taper pipe thread 27, it is characterized in that reactor 1 lower central place is equipped with circular arc back taper bubbler 2, circular arc back taper bubbler 2 connects air inlet pipe 4, and intake valve 3 is housed in air inlet pipe 4; Reactor 1 bottom connects discharge nozzle 6, and outlet valve 5 is housed on discharge nozzle 6; Described circular arc back taper bubbler is characterized in that outer surface is circular arc reverse taper, and back taper bottom surface is the arc surface of evagination, and back taper side is inside recessed cambered surface, has the bubble holes 21 of N equal aperture on the inner concave arc surface of back taper side.
Described circular arc back taper bubbler 2 back taper bottom surfaces are excessively connected with side circular arc.
The opening direction of N bubble holes 21 on described circular arc back taper bubbler 2 changes with the inner concave arc surface of back taper side, by laterally downward gradually.
In described air inlet pipe 4, there is common fine thread 26 to be connected with reactor by interior tightening screw 22, interior sealing gasket 23, external seal pad 24, outer tightening screw 25 with taper pipe thread 27.
Described circular arc back taper bubbler 2 bottom surface diameters and reactor diameter ratio are 1: 4.
Compressed air enters circular arc back taper bubbler 2 by air inlet pipe 4, is entered in reactor 1 by the bubble holes 21 of N different directions of circular arc back taper bubbler 2, realizes the material stirring in reactor 1; N bubble holes 21 is in the following side of circular arc back taper bubbler 2, bubble first oliquely downward moves, directly the solid material of reactor bottom is stirred, bubble is subject to the resistance of reactor material, speed slows down gradually, because of the density contrast of bubble and liquid-solid material, the buoyancy that is subject to material finally moves upward simultaneously.Under stirring bubble running orbit elder generation is oblique, then turn back upwards, because opening direction is that bubble is uniformly distributed in the radially formation of reactor by laterally excessive downwards, the whole motion process of bubble in reactor continues to stir to the material in reactor.

Claims (4)

1. circular arc inverted-cone bubbling stirred autoclave comprises reactor, circular arc back taper bubbler, intake valve, air inlet pipe, outlet valve, discharge nozzle, bubble holes, interior tightening screw, interior sealing gasket, external seal pad, outer tightening screw, common fine thread, taper pipe thread, it is characterized in that reactor lower central place is equipped with circular arc back taper bubbler, circular arc back taper bubbler connects air inlet pipe, and intake valve is housed in air inlet pipe; Reactor bottom connects discharge nozzle, and outlet valve is housed on discharge nozzle; Described circular arc back taper bubbler is characterized in that outer surface is similar to circular arc reverse taper, and bottom surface is the arc surface of evagination, and back taper side is inside recessed cambered surface, has the bubble holes of N equal aperture on the inner concave arc surface of back taper side;
The opening direction of N bubble holes on described circular arc back taper bubbler changes with the inner concave arc surface of back taper side, by laterally downward gradually.
2. circular arc inverted-cone bubbling stirred autoclave as claimed in claim 1, is characterized in that, described circular arc back taper bubbler back taper bottom surface is connected with side arc transition.
3. circular arc inverted-cone bubbling stirred autoclave as claimed in claim 1, is characterized in that, has common fine thread to be connected with reactor by interior tightening screw, interior sealing gasket, external seal pad, outer tightening screw with taper pipe thread in described air inlet pipe.
4. circular arc inverted-cone bubbling stirred autoclave as claimed in claim 1, is characterized in that, described circular arc back taper bubbler bottom surface diameter and reactor diameter ratio are 1: 4.
CN201210270096.4A 2012-07-31 2012-07-31 Circular inverted cone type bubbling stirred tank reactor Expired - Fee Related CN102824882B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210270096.4A CN102824882B (en) 2012-07-31 2012-07-31 Circular inverted cone type bubbling stirred tank reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210270096.4A CN102824882B (en) 2012-07-31 2012-07-31 Circular inverted cone type bubbling stirred tank reactor

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CN102824882A CN102824882A (en) 2012-12-19
CN102824882B true CN102824882B (en) 2014-08-13

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Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2381634Y (en) * 1999-06-14 2000-06-07 天津国水设备工程有限公司 Microporous aerator for all directional aeration
CN2394915Y (en) * 1999-08-02 2000-09-06 中国科学院化工冶金研究所 Bubble tower type light biological reactor
JP2003001224A (en) * 2001-06-18 2003-01-07 Shinto Eco Techno:Kk Air bubble treating method of excreta fermentation treating device and mechanism thereof
CN201342262Y (en) * 2008-03-11 2009-11-11 张雪容 Automatic extraction conjoint device for sampling bottle
CN202016896U (en) * 2011-03-21 2011-10-26 郑州宇通环保科技有限公司 Conical surface type jet aerator

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Granted publication date: 20140813

Termination date: 20170731