CN102807809B - A kind of alkyd paint and preparation method - Google Patents
A kind of alkyd paint and preparation method Download PDFInfo
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- CN102807809B CN102807809B CN201210278248.5A CN201210278248A CN102807809B CN 102807809 B CN102807809 B CN 102807809B CN 201210278248 A CN201210278248 A CN 201210278248A CN 102807809 B CN102807809 B CN 102807809B
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- octoate
- alkyd paint
- toluene
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Abstract
The invention provides a kind of low cost alkyd paint and preparation method thereof, be made up of 1036 resin 90-110 parts, 582 aminoresin 5.4-6.6 parts, isocaprylic acid zinc 2.6-3.2, cobalt iso-octoate 0.40-0.50, manganese iso-octoate 0.27-0.33, toluene 4-14 part.During construction, by said components normal temperature mix and blend.1036 resins are composed as follows: behenic acid 75-91 part, phthalic anhydride 90-110 part, glycerine 39-57 part, dimethylbenzene 22-28 part, 200# solvent oil 45-55 part, toluene 69-81 part.Alkyd paint prepared by the present invention has low cost, stability in storage is good, and firmly, tenacity is feature all preferably.
Description
Technical field
The invention belongs to paint field, be specifically related to a kind of alkyd paint.
Background technology
Alkyd paint has good gloss, weathering resistance, water tolerance, strong adhesion, and film is plentiful hard, and low price, construction are simple, less demanding to construction environment, can through the strong variations of climate.Can be used for metal, wooden, the aspects such as the application of various vehicle mechanical instrument and steel and iron member boats and ships waterborne.
Synolac good film-forming property, rete has excellent weathering resistance, resistance to salt water, gloss, resistance to aliphatic solvent, thermotolerance, shock-resistance.Account for 95% as application of paints, it is most popular one in all coating resins.
Summary of the invention
The object of the present invention is to provide a kind of is the formulated alkyd paint of main raw material by 1036 resins.
Another object of the present invention is to the preparation method that a kind of alkyd paint is provided.
Another object of the present invention is to provide a kind of 1036 resins and preparation method thereof.
In order to realize object of the present invention, the technical solution adopted in the present invention is as follows:
A kind of alkyd paint, is characterized in that the component primarily of following weight part forms,
1036 resin 80-120 parts;
DCP 0.6-0.8 part;
Cobalt iso-octoate 0.04-0.07 part;
Vinylbenzene 4-14 part.
Described 1036 resins form primarily of the component of following weight part,
Behenic acid 75-91 part;
Phthalic anhydride 90-110 part;
Glycerine 39-57 part;
Dimethylbenzene 22-28 part;
200# solvent oil 45-55 part;
Toluene 69-81 part.
The preparation method of described 1036 resins comprises the following steps:
(1), by behenic acid, behenic acid, glycerine and dimethylbenzene mix, be warming up to 220-230 DEG C of back flow reaction, being incubated to pH value is 7.5, checks viscosity, qualified i.e. termination reaction.
(2), in advance in dilution still, drop into 200# solvent oil and toluene, slowly put into by resin in dilution still, the strict temperature controlling mixture more than 90 DEG C, must not be stirred to room temperature (≤50 DEG C).
The preparation method of alkyd paint of the present invention, comprises the following steps:
(1) 1036 resins, 582 aminoresin, isocaprylic acid zinc, cobalt iso-octoate, manganese iso-octoate and toluene normal temperature are mixed, stir 30 minutes.
(2), through being up to the standards, packaging.
Alkyd paint prepared by the present invention has low cost, stability in storage is good, and firmly, tenacity is feature all preferably.
Embodiment:
Describe technology contents of the present invention in detail below in conjunction with embodiment, but the invention is not restricted to following examples.
Embodiment 1
1. fill a prescription
The present embodiment 1036 resin composed as follows:
Behenic acid 200kg;
Phthalic anhydride 240kg;
Glycerine 115kg;
Dimethylbenzene 60kg;
200# solvent oil 120kg;
Toluene 180kg.
2. preparation method
(1), by behenic acid, behenic acid, glycerine and dimethylbenzene mix by above weight, be warming up to 220-230 DEG C of back flow reaction, being incubated to pH value is 7.5, checks viscosity, qualified i.e. termination reaction.
(2), in advance in dilution still, drop into 200# solvent oil and toluene by above weight, gained resin prepared by step (1) and slowly put in dilution still, the strict temperature controlling mixture more than 90 DEG C, must not be stirred to room temperature (≤50 DEG C).
Embodiment 2
1. fill a prescription
The present embodiment 1036 resin composed as follows:
Behenic acid 220kg;
Phthalic anhydride 250kg;
Glycerine 105kg;
Dimethylbenzene 50kg;
200# solvent oil 140kg;
Toluene 200kg.
2. preparation method
(1), by behenic acid, behenic acid, glycerine and dimethylbenzene mix by above weight, be warming up to 220-230 DEG C of back flow reaction, being incubated to pH value is 7.5, checks viscosity, qualified i.e. termination reaction.
(2), in advance in dilution still, drop into 200# solvent oil and toluene by above weight, gained resin prepared by step (1) and slowly put in dilution still, the strict temperature controlling mixture more than 90 DEG C, must not be stirred to room temperature (≤50 DEG C).
Embodiment 3
1. fill a prescription
The present embodiment alkyd paint composed as follows:
1036 resin 100kg;
582 aminoresin 6kg;
Isocaprylic acid zinc 2.9kg;
Cobalt iso-octoate 0.45kg;
Manganese iso-octoate 0.3kg;
Toluene 10kg;
2. preparation method
(1) 1036 resins, 582 aminoresin, isocaprylic acid zinc, cobalt iso-octoate, manganese iso-octoate and toluene are mixed by above weight normal temperature, stir 30 minutes.
(2), through being up to the standards, packaging.
The present embodiment prepares the technical indicator of gained alkyd paint in table 1
Embodiment 4
1. fill a prescription
The present embodiment alkyd paint composed as follows:
1036 resin 110kg;
582 aminoresin 5.5kg;
Isocaprylic acid zinc 3.0kg;
Cobalt iso-octoate 0.5kg;
Manganese iso-octoate 0.2kg;
Toluene 13kg.
2. preparation method
(1), by 1036 resins, 582 aminoresin, isocaprylic acid zinc, cobalt iso-octoate, manganese iso-octoate and toluene by above weight normal temperature mixing, stir 30 minutes.
(2), through being up to the standards, packaging.
The present embodiment prepares the technical indicator of gained alkyd paint in table 1.
Table 1
| Technical indicator | Embodiment 3 | Embodiment 4 |
| Coated plate hardness (pencil hardness) | H | H |
| Gloss | 90% | 87% |
| Surface drying | 8 hours | 7 hours |
| Stability in storage (35 DEG C, 60 days) | Without precipitation | Without precipitation |
| Impact strength | ≥50cm | ≥50cm |
Claims (1)
1. an alkyd paint, is characterized in that, the component primarily of following weight part forms:
Described 1036 resins form primarily of the component of following weight part:
The preparation method of 1036 described resins comprises the following steps:
(1), by behenic acid, phthalic anhydride, glycerine and dimethylbenzene mix, be warming up to 220-230 DEG C of back flow reaction, being incubated to pH value is 7.5, checks viscosity, qualified i.e. termination reaction;
(2), in advance in dilution still, drop into 200# solvent oil and toluene, gained resin prepared by step (1) and slowly put in dilution still, the strict temperature controlling mixture more than 90 DEG C, must not be stirred to room temperature;
The preparation method of described alkyd paint, is characterized in that, comprises the following steps:
(a), by 1036 resins, 582 aminoresin, isocaprylic acid zinc, cobalt iso-octoate, manganese iso-octoate and toluene normal temperature mix, stir 30 minutes;
(b), through being up to the standards, packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210278248.5A CN102807809B (en) | 2012-08-07 | 2012-08-07 | A kind of alkyd paint and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210278248.5A CN102807809B (en) | 2012-08-07 | 2012-08-07 | A kind of alkyd paint and preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102807809A CN102807809A (en) | 2012-12-05 |
| CN102807809B true CN102807809B (en) | 2015-08-19 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210278248.5A Active CN102807809B (en) | 2012-08-07 | 2012-08-07 | A kind of alkyd paint and preparation method |
Country Status (1)
| Country | Link |
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| CN (1) | CN102807809B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103694463A (en) * | 2013-12-02 | 2014-04-02 | 安庆菱湖涂料有限公司 | Preparation method of soya alkyd resin |
| CN107936795A (en) * | 2017-12-12 | 2018-04-20 | 茂名市英达精细化工有限公司 | A kind of alkyd neulating varnish and preparation method thereof |
| CN109852228A (en) * | 2018-12-20 | 2019-06-07 | 中国电子科技集团公司第三十研究所 | Two component polyurethane varnish and its coating processes for printed circuit board protection |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102363691A (en) * | 2011-06-28 | 2012-02-29 | 衡阳恒缘电工材料有限公司 | Dipping technology of high-temperature-resistant alkyd paint |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6183263A (en) * | 1984-09-29 | 1986-04-26 | Kansai Paint Co Ltd | Oxidative drying-type paint |
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2012
- 2012-08-07 CN CN201210278248.5A patent/CN102807809B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102363691A (en) * | 2011-06-28 | 2012-02-29 | 衡阳恒缘电工材料有限公司 | Dipping technology of high-temperature-resistant alkyd paint |
Non-Patent Citations (2)
| Title |
|---|
| 利用大豆油脚或皂脚生产醇酸树脂原料;王公新;《中国油脂》;19981231;第23卷(第6期);第27页配方1 * |
| 涂料工艺编委会.醇酸树脂漆.《涂料工艺第三版》.1997,第361页. * |
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| CN102807809A (en) | 2012-12-05 |
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Address after: 421008 Hunan city of Hengyang Province Huang Cha Ling Yuan Cun Heng Yanfeng District No. 4 Applicant after: Hunan Heng Yuan green wood Science and Technology Co., Ltd. Address before: 421008 Hunan city of Hengyang Province Huang Cha Ling Yuan Cun Heng Yanfeng District No. 4 Applicant before: Hengyang Hengyuan Electrical Material Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: HENGYANG HENGYUAN ELECTRICAL MATERIAL CO., LTD. TO: HUNAN HENGYUAN NEW MATERIAL TECHNOLOGY CO., LTD. |
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