CN102807377B - Method for manufacturing refractory clay for constructing refractory bricks of flame path walls of baking furnaces - Google Patents

Method for manufacturing refractory clay for constructing refractory bricks of flame path walls of baking furnaces Download PDF

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CN102807377B
CN102807377B CN201110144674.5A CN201110144674A CN102807377B CN 102807377 B CN102807377 B CN 102807377B CN 201110144674 A CN201110144674 A CN 201110144674A CN 102807377 B CN102807377 B CN 102807377B
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parts
granularity
content
bauxite chamotte
refractory
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CN102807377A (en
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靳艳军
董建军
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HENAN XINCHENG REFRACTORY MATERIAL CO Ltd
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HENAN XINCHENG REFRACTORY MATERIAL CO Ltd
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Abstract

The invention provides a method for manufacturing refractory clay for constructing refractory bricks of flame path walls of baking furnaces. Raw materials for manufacturing the refractory clay are obtained from mixing four or more than four of bauxite chamotte I, bauxite chamotte II, bauxite chamotte III, mullite chamotte, alumina powder and high-quality porcellanite, and adding mixture of two or more than two of sodium carboxymethylcellulose, sodium tripolyphosphate, sodium hexametaphosphate and yellow dextrin, wherein the bauxite chamotte I, the bauxite chamotte II and the bauxite chamotte III are different in finenesses and Al2O3 contents. The method includes the steps of weighing, stirring, sealing and packing the raw material mixture in bags; when in construction of the refractory bricks on the construction site, adding the mixture into a slurry mixer, weighing and adding 33-38 weight parts of clean tap water into every 100 weight parts of mixture, and fully stirring for at least 10 minutes. Thickness of the refractory clay is determined for the convenience of utilization. The method for manufacturing the refractory clay for constructing the refractory bricks of the flame path walls of the baking furnaces is simple in process and low in cost, the refractory clay manufactured is high in bonding strength and strong in fire retardance under the conditions of low temperature, middle temperature and high temperature, and the flame path walls constructed are firm, durable and long in service life.

Description

The preparation method of refractory mortar for a kind of baking furnace flame path wall laying fireproof bricks
Technical field
The invention belongs to the technical field of the stoving oven of anode carbon cellulose product sintering, be specifically related to the preparation method of a kind of baking furnace flame path wall laying fireproof bricks refractory mortar.
Background technology
Aluminium cell anode carbon cellulose product used is fired and is formed in stoving oven, the stoving oven that roasting is used, its flue wall part refractory brick will be used refractory mortar building by laying bricks or stones, because the maturing temperature of stoving oven generally will exceed 1200 DEG C even higher, therefore refractory mortar need to have higher cohesive strength and higher refractoriness in the time of low temperature, middle temperature, high temperature.At present, the clayey refractory mortar that the refractory mortar of most baking furnace flame path wall all adopts, its Al 2o 3content is between 45~48%, and manufacture craft is simple, while building refractory brick by laying bricks or stones, its cohesive strength is lower, flue wall in applied at elevated temperature process, due to clay refractory mortar cohesive strength and refractoriness lower, its low temperature and high temperature cohesive strength are not high, constantly be subject under the impact of high temperature and high temperature air pressure, cause brickwork joint loose, and come off out under effect along with high temperature gas flow, cause flue wall brickwork joint to damage, notch distortion under flue wall, the work-ing life of having reduced baking furnace flame path wall.
Summary of the invention
For above-mentioned defect, the present invention is the preparation method with refractory mortar in a kind of baking furnace flame path wall laying fireproof bricks, causes that refractory mortar comes off, the defect of flue wall deformed damaged to solve refractory mortar of the prior art cohesive strength is low under low temperature, the middle gentle condition of high temperature, refractoriness is not high.
To achieve these goals, technical scheme of the present invention is: the preparation method of refractory mortar for a kind of baking furnace flame path wall laying fireproof bricks, its raw material is made up of powder, admixture two portions.
Described powder, in its component, each composition parts by weight are as follows:
Bauxite chamotte I (Al 2o 3content>=75%) 45~55 parts of granularity≤0.088mm,
Mullite grogs (Al 2o 3content>=70%) 15~20 parts of granularity≤0.088mm,
Aluminum oxide powder (Al 2o 3content>=98%) 5~8 parts of granularity≤0.043mm,
Bauxite chamotte II (Al 2o 3content>=75%) 5~10 parts of granularity≤0.043mm,
Bauxite chamotte III (Al 2o 3content>=55%) 10~15 parts of granularity≤0.043mm,
High quality white potter's clay (Al 2o 3content>=30%) 8~15 parts of granularity≤0.043mm,
Form with four or more mixed preparing wherein;
Described admixture, each parts by weight of its material component are as follows:
1.5~3 parts of Xylo-Mucines,
1~3 part of tripoly phosphate sodium STPP,
0.5~2 part of Sodium hexametaphosphate 99,
1.5~3 parts of yellow starch gums,
Form with two or more mixed preparing wherein;
The step that manufacture method of the present invention comprises is:
(1) weigh: powder and admixture are weighed by above-mentioned parts by weight,
(2) stir: weighted raw material is added in stirrer and carries out mix and blend, stir Shi Jian≤10 minute,
(3) pack: by stand-by the mixture sealing pack after fully stirring,
While building refractory brick by laying bricks or stones, on-the-spot packed mixture is joined to slurry mixer, then by mixture gross weight umber by 100, take the clean tap water of 33~38 parts, join in stirrer and fully stir, stir Shi Jian≤10 minute, thick dilution is as the criterion with easy to use.
The refractory mortar of made of the present invention has the advantages that cohesive strength is high, refractoriness is high under low temperature, the middle gentle condition of high temperature, and the flue wall of building by laying bricks or stones by refractory mortar of the present invention is durable, long service life.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1: the feed composition of choosing following parts by weight:
Bauxite chamotte I (Al 2o 3content>=75%) 45 parts of granularity≤0.088mm,
Mullite grogs (Al 2o 3content>=70%) 20 parts of granularity≤0.088mm,
Aluminum oxide powder (Al 2o 3content>=98%) 5 parts of granularity≤0.043mm,
Bauxite chamotte II (Al 2o 3content>=75%) 10 parts of granularity≤0.043mm,
Bauxite chamotte III (Al 2o 3content>=55%) 10 parts of granularity≤0.043mm,
High quality white potter's clay (Al 2o 3content>=30%) 8 parts of granularity≤0.043mm,
2 parts of Xylo-Mucines,
2 parts of tripoly phosphate sodium STPPs,
2 parts of yellow starch gums,
After preparing by weight, add in stirrer and carry out mix and blend, stir Shi Jian≤10 minute, by stand-by the mixture sealing pack after fully stirring,
While building refractory brick by laying bricks or stones, on-the-spot by packed mixture join slurry mixer then by mixture gross weight umber by 100, take the clean tap water of 34 parts, join in stirrer and fully stir, when stirring between≤10 minutes, thick dilution is as the criterion with easy to use.
Embodiment 2: the feed composition of choosing following parts by weight:
Bauxite chamotte I (Al 2o 3content>=75%) 48 parts of granularity≤0.088mm,
Mullite grogs (Al 2o 3content>=70%) 15 parts of granularity≤0.088mm,
Aluminum oxide powder (Al 2o 3content>=98%) 6 parts of granularity≤0.043mm,
Bauxite chamotte II (Al 2o 3content>=75%) 10 parts of granularity≤0.043mm,
Bauxite chamotte III (Al 2o 3content>=55%) 12 parts of granularity≤0.043mm,
High quality white potter's clay (Al 2o 3content>=30%) 10 parts of granularity≤0.043mm,
1 part of Xylo-Mucine,
2 parts of tripoly phosphate sodium STPPs,
1 part of Sodium hexametaphosphate 99,
2.5 parts of yellow starch gums,
After preparing by weight, add in stirrer and carry out mix and blend, stir Shi Jian≤10 minute, by stand-by the mixture sealing pack after fully stirring,
While building refractory brick by laying bricks or stones, on-the-spot packed mixture is joined to slurry mixer, then by mixture gross weight umber by 100, take the clean tap water of 37 parts, join in stirrer and fully stir, when stirring between≤10 minutes, thick dilution is as the criterion with easy to use.
Embodiment 3: the feed composition of choosing following parts by weight:
Bauxite chamotte I (Al 2o 3content>=75%) 53 parts of granularity≤0.088mm,
Mullite grogs (Al 2o 3content>=70%) 18 parts of granularity≤0.088mm,
Aluminum oxide powder (Al 2o 3content>=98%) 8 parts of granularity≤0.043mm,
High quality white potter's clay (Al 2o 3content>=30%) 15 parts of granularity≤0.043mm,
1.5 parts of Xylo-Mucines,
1.5 parts of tripoly phosphate sodium STPPs,
1.5 parts of yellow starch gums,
After preparing by weight, add in stirrer and carry out mix and blend, stir Shi Jian≤10 minute, by stand-by the mixture sealing pack after fully stirring,
While building refractory brick by laying bricks or stones, on-the-spot packed mixture is joined to slurry mixer, then by mixture gross weight umber by 100, take the clean tap water of 33 parts, join in stirrer and fully stir, when stirring between≤10 minutes, thick dilution is as the criterion with easy to use.
Embodiment 4: the feed composition of choosing following parts by weight:
Bauxite chamotte I (Al 2o 3content>=75%) 55 parts of granularity≤0.088mm,
Bauxite chamotte II (Al 2o 3content>=75%) 20 parts of granularity≤0.043mm,
Bauxite chamotte III (Al 2o 3content>=55%) 15 parts of granularity≤0.043mm,
High quality white potter's clay (Al 2o 3content>=30%) 12 parts of granularity≤0.043mm,
2 parts of tripoly phosphate sodium STPPs,
1.5 parts of yellow starch gums,
After preparing by weight, add in stirrer and carry out mix and blend, stir Shi Jian≤10 minute, by stand-by the mixture sealing pack after fully stirring,
While building refractory brick by laying bricks or stones, on-the-spot packed mixture is joined to slurry mixer, then by mixture gross weight umber by 100, take the clean tap water of 38 parts, join in stirrer and fully stir, when stirring between≤10 minutes, thick dilution is as the criterion with easy to use.
Refractory mortar of the present invention contrasts with now using refractory mortar physical and chemical index, Al in refractory mortar 2o 3content improves greatly, has that cohesive strength is high, High anti bending strength, feature that refractoriness is high under low temperature, the middle gentle condition of high temperature, and the flue wall that uses refractory mortar of the present invention to build by laying bricks or stones is durable, long service life.Its performance perameter contrasts as following table.
Protection scope of the present invention is not limited to the described scope of above-described embodiment, and every technology distortion of doing according to technical solution of the present invention principle, within all falling into protection scope of the present invention.

Claims (1)

1. a preparation method for refractory mortar for baking furnace flame path wall laying fireproof bricks, is characterized in that: its raw material is made up of powder, admixture two portions;
Described powder, in its component, each composition parts by weight are as follows:
Bauxite chamotte I Al 2o 345~55 parts of content>=75% granularity≤0.088mm,
Mullite grogs Al 2o 315~20 parts of content>=70% granularity≤0.088mm,
Aluminum oxide powder Al 2o 35~8 parts of content>=98% granularity≤0.043mm,
Bauxite chamotte II Al 2o 35~10 parts of content>=75% granularity≤0.043mm,
Bauxite chamotte III Al 2o 310~15 parts of content>=55% granularity≤0.043mm,
High quality white potter's clay Al 2o 38~15 parts of content>=30% granularity≤0.043mm,
Form with more than four kinds mixed preparing wherein;
Described admixture, each parts by weight of its material component are as follows:
1.5~3 parts of Xylo-Mucines,
1~3 part of tripoly phosphate sodium STPP,
0.5~2 part of Sodium hexametaphosphate 99,
1.5~3 parts of yellow starch gums,
Form with two or more mixed preparing wherein;
The steps include:
(1) weigh: powder and admixture are weighed by above-mentioned parts by weight,
(2) stir: add stirrer to carry out mix and blend weighted raw material, stir Shi Jian≤10 minute,
(3) pack: by stand-by the mixture sealing pack after fully stirring.
CN201110144674.5A 2011-06-01 2011-06-01 Method for manufacturing refractory clay for constructing refractory bricks of flame path walls of baking furnaces Active CN102807377B (en)

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CN105130390A (en) * 2015-08-27 2015-12-09 郑州安耐克实业有限公司 Low-temperature sintered refractory slurry and preparation method therefor
CN107540389A (en) * 2017-07-11 2018-01-05 河南鑫诚耐火材料股份有限公司 A kind of carbon anode roasting furnace andalusite brick and preparation method thereof
CN108314433B (en) * 2018-03-26 2020-07-31 宜兴瑞泰耐火材料有限公司 High-alumina erosion-resistant micro-expansion refractory mortar and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1214327A (en) * 1997-10-09 1999-04-21 济南东方工业炉新技术开发总公司 Inorganic combined high-strength refractory deposit material and its preparation
CN101353262A (en) * 2008-09-17 2009-01-28 刘放 Fire-resistant material formula and method for preparing fire-resistant material using the same
CN102070347A (en) * 2009-11-23 2011-05-25 德清县钢友耐火材料有限公司 Preparation method for high-alumina bricks

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5261917B2 (en) * 2006-10-26 2013-08-14 新日鐵住金株式会社 Refractory construction method, refractory, and kiln

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1214327A (en) * 1997-10-09 1999-04-21 济南东方工业炉新技术开发总公司 Inorganic combined high-strength refractory deposit material and its preparation
CN101353262A (en) * 2008-09-17 2009-01-28 刘放 Fire-resistant material formula and method for preparing fire-resistant material using the same
CN102070347A (en) * 2009-11-23 2011-05-25 德清县钢友耐火材料有限公司 Preparation method for high-alumina bricks

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
JP特开2008-107038A 2008.05.08

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