CN102728129B - Solid-liquid separator for electronic chemical production - Google Patents

Solid-liquid separator for electronic chemical production Download PDF

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Publication number
CN102728129B
CN102728129B CN201210203344.3A CN201210203344A CN102728129B CN 102728129 B CN102728129 B CN 102728129B CN 201210203344 A CN201210203344 A CN 201210203344A CN 102728129 B CN102728129 B CN 102728129B
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Prior art keywords
rotary drum
driver
collection bucket
solid
pipe
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CN102728129A (en
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刘飞
杨毅
孟文祥
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Wengfu Group Co Ltd
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Wengfu Group Co Ltd
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  • Centrifugal Separators (AREA)

Abstract

The invention discloses a solid-liquid separator for electronic chemical production, and relates to the technical field of solid-liquid separation. The separator comprises a machine base, a housing, a rotary drum, a rotary drum driver and a collecting hopper. A side of the housing is provided with a filtrate outlet pipe. The upper part of the housing is provided with a machine cover, wherein the machine cover is provided with a feed pipe, a visuscope, a washing pipe and a scraper driving device. The lower part of the housing is connected with the machine base. The rotary drum is arranged inside the housing, wherein the bottom of the rotary drum is provided with a material outlet. The collecting hopper is arranged on the machine base. The center of the rotary drum is provided with the rotary drum driver, wherein the rotary drum driver is fixedly connected with the collecting hopper, and the rotary drum and the rotary drum driver are coaxially and fixedly connected. The top of the rotary drum driver is provided with an umbrella-like material distribution disc, and a belt pulley is arranged below the rotary drum driver. A scraper driving device stretching rod penetrates through the machine cover, and is connected with a scraper, wherein the scraper extends into the rotary drum. The upper part of the collecting hopper and the material outlet of the rotary drum are connected. A side of the collecting hopper is provided with a leakage liquid discharging pipe and a leakage liquid discharging valve. The bottom of the collecting hopper is provided with a material discharge valve connected with a material discharge pipe. The solid-liquid separator of the present invention is applicable for fields of electronic chemical production.

Description

The solid-liquid separator that a kind of electronic chemical product is produced
Technical field
The present invention relates to solid-liquid separation technique field, furthermore, relate to the solid-liquid separator that a kind of electronic chemical product is produced.
Background technology
Electronic chemical product is widely used in the electronics industry such as large scale integrated circuit, film liquid crystal display (TFT-LCD), be mainly used in cleaning and the etchant of chip, its purity and cleanliness factor ratio defective product, electrical property, the reliability to electronic devices and components has a great impact.When crystallisation is produced electronic chemical product, solid-liquid filtration need be separated and obtains needed product, filter output and quality influence that electronic chemical product is produced very large, the general filter centrifugal that adopts, mainly there are the following problems for current domestic filter centrifugal: Pig filter centrifugal manipulation strength is large, treating capacity is little, efficiency is low, filter cloth is damaged replacing frequently easily, product vulnerable to pollution; Horizontal discharging filter centrifugal treating capacity is large, but material water capacity after separating is large, and product purity is not high, and easily the crystalline form of solid is produced to destruction; Same vertical discharging filter centrifugal treating capacity is large, but material moisture content after separating is high, easily the crystalline form of solid is produced to destruction; The separation equipment of prior art, while carrying out Separation of Solid and Liquid in process of production, solid and separation equipment can produce friction, and polluted product will take out solid after separation, has increased production cost and easily electronic chemical product has been produced to secondary pollution.And the application of above filter in electronic chemical product Separation of Solid and Liquid has no document announcement.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, the solid-liquid separator that provides a kind of electronic chemical product to produce, the difficulty existing to overcome prior art electronic chemical product Separation of Solid and Liquid, further improves the Quality and yield of product.
The solid-liquid separator that a kind of electronic chemical product of the present invention is produced, it comprises support, shell, rotary drum, rotary drum driver and collection bucket; A side that it is characterized in that described shell is provided with filtrate and goes out pipe, and shell upper is equipped with cover, is equipped with feed pipe, visor, sluicing pipe and scrapes driving device for cutter on cover, and outer casing underpart and support join; Described rotary drum is put in the enclosure, and rotary drum sidewall is provided with roundlet type filter opening, and bottom of the drum is provided with feed opening; Described collection bucket is placed on support; Described rotary drum center is equipped with rotary drum driver, and rotary drum driver is fixed on collection bucket, and rotary drum and rotary drum driver are coaxially fastenedly connected; Rotary drum driver top is equipped with umbrella cloth tray, under rotary drum driver, has belt pulley, the belt pulley belt transmission of described rotary drum driver, and motor and driving wheel are located at outside collection bucket; The described driving device for cutter expansion link of scraping, through cover, is scraped driving device for cutter expansion link and is connected to scraper, and scraper stretches in rotary drum; Collection bucket top and rotary drum feed opening join, and collection bucket one side is provided with leakage delivery pipe and leakage drain valve, and collection bucket bottom has discharge valve to be connected with discharge duct.
Described visor is 1~4.
When use, above-mentioned drum inner wall requires filter screen is installed, and filter screen can be metal screen, polypropylene filter screen or filter cloth, and aperture of filter screen is determined according to filtered solid size.
The rotating speed of rotary drum is determined according to the character of feed separation, is generally charging in the time of rotary drum low speed rotation, de-liquid when high speed.
Above-mentioned collection bucket bottom is provided with discharge valve, and in the time of rotary drum charging and washing, discharge valve cuts out, and a small amount of filtrate and cleaning solution enter collection bucket by feed opening, can discharge by collection bucket one side leakage liquid delivery pipe and leakage drain valve; In the time of discharging, discharge valve is opened, and product enters collection bucket by feed opening, then discharges by discharge valve and discharge duct.
Adopt equipment operating of the present invention, start motor, belt drives rotary drum driver, make drum rotating, slip enters in rotary drum by material feeding pipe, is distributed in uniformly on rotary drum filter screen through umbrella cloth tray, and filtrate is by the small sircle hole on filter screen and rotary drum, enter the inner side of shell, discharge by filtrate port; Solids distribution, on filter screen, when solid reaches certain thickness, stops charging, because the liquid being attached on the surface of solids contains a large amount of impurity, can add washing agent to wash by sluicing pipe, makes product purity purer; Then according to the requirement of solid water capacity, improve rotary drum rotating speed, to further de-liquid of solid, make solid reach the requirement of water capacity; When discharging, reduce rotary drum rotating speed, start and scrape driving device for cutter, scraper rotation, to certain angle, is contacted with solid, scraper moves up and down and carries out discharging, and solid enters collection bucket by feed opening, then discharges through discharge valve and discharge duct.
The present invention has following characteristics:
(1) feed pipe, scraper, feed opening, collection bucket, discharge valve and discharge duct serve as a contrast high-purity plastics, and other parts adopt stainless steel (as 316,904L etc.), to reach anticorrosion, clean effect.
(2) have visor, be convenient to observe at any time charging and filtration situation.
(3) rotary drum is installed filter cloth, and material is uniformly distributed on filter cloth by cloth tray, can ensure the intact of solid crystalline.
(4) equipment is simple, and operating process is easy to control, and output is high, and energy consumption is low, can realize automation control.
(5) whole separation process is all carried out under sealing condition, does not contact cleanliness without any pollution with external environment.
(6) product purity obtaining is high, has very high economic benefit and social benefit.
The present invention is applicable to the production field of electronic chemical product.
Brief description of the drawings
Fig. 1 is solid-liquid separator structural representation of the present invention;
Mark in figure: 1-cover; 2-feed pipe; 3-visor; 4-scrapes driving device for cutter; 5-sluicing pipe; 6-cloth tray; 7-rotary drum; 8-scraper; 9-shell; 10-filtrate port; 11-support; 12-leakage delivery pipe; 13-leakage drain valve; 14-rotary drum driver; 15-discharge duct; 16-discharge valve; 17-feed opening; 18-collection bucket; 19-motor; 20-V belt.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
embodiment:
Certain Co., Ltd is used the present invention to produce electron-level phosphoric acid product, as shown in the figure, a kind of electronic chemical product solid-liquid separator, it comprises support 11, shell 9, rotary drum 7, rotary drum driver 14 and collection bucket 18; One side of shell 9 is provided with filtrate pipe 10, and shell 9 tops are equipped with cover 1, is equipped with feed pipe 2, visor 3, sluicing pipe 5 and scrapes driving device for cutter 4 on cover 1, and shell 9 bottoms and support 11 weld; Rotary drum 7 sidewalls are provided with roundlet type filter opening, and rotary drum 7 bottoms are provided with 3~4 feed openings 17, and rotary drum driver 14 is erected on collection bucket 18, and rotary drum 7 is coaxially fastenedly connected with rotary drum driver 14; Rotary drum driver 14 tops are equipped with umbrella cloth tray 6, and rotary drum driver has pulley concial disk 14 times; Scrape driving device for cutter 4 expansion links through cover 1, scrape driving device for cutter 4 expansion links and be connected to scraper 8, scraper 8 stretches in rotary drum 7; The feed opening 17 of collection bucket 18 tops and rotary drum 7 joins, and collection bucket 18 1 sides are provided with leakage delivery pipe 12 and leakage drain valve 13, and collection bucket 18 bottoms are connected with discharge duct 15 by discharge valve 16.The present embodiment visor 3 is 2.
Rotary drum 7 inwalls are installed filter screen, and filter screen is filter cloth, and filter cloth is fixed on rotary drum 7 inwalls, the roundlet type filter opening of establishing on rotary drum 7 sidewalls, and aperture is 200 orders; V belt 20 transmissions for the belt pulley of rotary drum driver 14, motor 19 and driving wheel are located at outside collection bucket 18, and when the charging of above-mentioned rotary drum 7 and washing, rotating speed is 380r/min, and when de-liquid, rotating speed is 750r/min, and when discharging, rotating speed is 50r/min;
When work, start motor 19, the pulley concial disk that V belt 20 drives rotary drum driver to have for 14 times, rotary drum driver 14 and rotary drum 7 are rotated, slip enters in rotary drum 7 by material feeding pipe 2, is distributed in uniformly on rotary drum 7 filter screens through umbrella cloth tray 6, and filtrate is by the small sircle hole on filter screen and rotary drum 7, enter the inner side of shell 9, discharge by filtrate port 10; When solid reaches certain thickness, stop charging, when washing, cleaning solution adds from sluicing pipe 5; Washing improves rotary drum rotating speed while end, to further de-liquid of solid, make solid reach the requirement of water capacity; When work, a small amount of filtrate and cleaning solution enter collection bucket 18 by feed opening 17, can discharge by collection bucket 18 1 side leakage liquid drain valves 13 and leakage delivery pipe 12; In the time of discharging, reduce rotary drum 7 rotating speeds, start and scrape driving device for cutter 4, scraper 8 is rotated to certain angle, contact with solid, scraper 8 moves up and down and carries out discharging, discharge valve 16 is opened, and product enters collection bucket 18 by feed opening 17, then discharges by discharge valve 16 and discharge duct 15.
As follows by the isolated electron-level phosphoric acid product quality of the present invention:
Product impurity content
Index subjet Impurity concentration Index subjet Impurity concentration
Aluminium (Al) 8ppb Iron (Fe) 197ppb
Copper (Cu) 30ppb Magnesium (Mg) 100ppb
Potassium (K) 49ppb Arsenic (As) 40ppb
Manganese (Mn) 20ppb Calcium (Ca) 89ppb
Sodium (Na) 90ppb Plumbous (Pb) 5ppb
Nickel (Ni) 30ppb Chromium (Cr) 71ppb
Lithium (Li) 2ppb Barium (Ba) 10ppb
Strontium (Sr) 1 ppb Gold (Au) 2 ppb

Claims (1)

1. the solid-liquid separator that electronic chemical product is produced, it comprises support (11), shell (9), rotary drum (7), rotary drum driver (14) and collection bucket (18); A side that it is characterized in that described shell (9) is provided with filtrate and goes out pipe (10), shell (9) top is equipped with cover (1), on cover (1), be equipped with feed pipe (2), visor (3), sluicing pipe (5) and scrape driving device for cutter (4), shell (9) bottom and support (11) join; Described rotary drum (7) is put in shell (9), and rotary drum (7) sidewall is provided with roundlet type filter opening, and rotary drum (7) bottom is provided with feed opening (17); Described collection bucket (18) is placed on support (11); Described rotary drum (7) center is equipped with rotary drum driver (14), and it is upper that rotary drum driver (14) is fixed in collection bucket (18), and rotary drum (7) is coaxially fastenedly connected with rotary drum driver (14); Rotary drum driver (14) top is equipped with umbrella cloth tray (6), rotary drum driver has belt pulley under (14), the belt pulley belt transmission of described rotary drum driver (14), motor (19) and driving wheel are located at outside collection bucket (18); Described driving device for cutter (4) expansion link of scraping, through cover (1), is scraped driving device for cutter (4) expansion link and is connected to scraper (8), and scraper (8) stretches in rotary drum (7); The feed opening (17) of collection bucket (18) top and rotary drum (7) joins, collection bucket (18) one sides are provided with leakage delivery pipe (12) and leakage drain valve (13), and collection bucket (18) bottom has discharge valve (16) to be connected with discharge duct (15).
CN201210203344.3A 2012-06-20 2012-06-20 Solid-liquid separator for electronic chemical production Active CN102728129B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210203344.3A CN102728129B (en) 2012-06-20 2012-06-20 Solid-liquid separator for electronic chemical production

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Application Number Priority Date Filing Date Title
CN201210203344.3A CN102728129B (en) 2012-06-20 2012-06-20 Solid-liquid separator for electronic chemical production

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CN102728129B true CN102728129B (en) 2014-06-18

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104906857B (en) * 2015-06-19 2016-09-28 深圳市凯宏膜环保科技有限公司 Influent stream web plate grid sewage-removing machine in a kind of
CN107233761B (en) * 2017-07-25 2019-10-25 深圳市普盛旺科技有限公司 Sewage-treatment plant
CN110773333A (en) * 2018-07-31 2020-02-11 王政 Centrifugal solid-liquid separator

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Publication number Priority date Publication date Assignee Title
BE629234A (en) * 1962-03-07
CN85201392U (en) * 1985-04-02 1986-01-01 山东大学 Separating funnel-type centrifuge tube
CN2593911Y (en) * 2002-12-13 2003-12-24 黄晓军 Vertical scraper discharging centrifuge with liftable rotary cover
CN201940107U (en) * 2011-01-30 2011-08-24 合肥通用机械研究院 Filtering-screen self-cleaning type filter with two-stage drainage openings
CN202654790U (en) * 2012-06-20 2013-01-09 瓮福(集团)有限责任公司 Solid-liquid separator for production of electronic chemicals

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Address after: 550500 Guizhou Province, Qiannan Buyei and Miao Autonomous Prefecture Fuquan Racecourse town Yingbin Road No. 1 Wengfu group

Patentee after: WENGFU GROUP Co.,Ltd.

Address before: 23, 550002 floor, International Building, No. 57, South City Road, Nanming District, Guiyang, Guizhou

Patentee before: WENGFU GROUP Co.,Ltd.

CP02 Change in the address of a patent holder