CN102721584A - Quick preparation method and device for embedded sample - Google Patents
Quick preparation method and device for embedded sample Download PDFInfo
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- CN102721584A CN102721584A CN2012102066930A CN201210206693A CN102721584A CN 102721584 A CN102721584 A CN 102721584A CN 2012102066930 A CN2012102066930 A CN 2012102066930A CN 201210206693 A CN201210206693 A CN 201210206693A CN 102721584 A CN102721584 A CN 102721584A
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Abstract
The invention discloses a quick preparation method for an embedded sample. The quick preparation method comprises the following steps: firstly, weighing an epoxy resin curing agent solution and epoxy resin solution in a preset weight ratio; secondly, pouring the weighed epoxy resin curing agent solution and epoxy resin solution into the same stirring cup; thirdly, stirring the epoxy resin curing agent solution and epoxy resin solution which are poured into the stirring cup to form a mixed solution; fourthly, pouring the mixed solution into an embedded sample die; and fifthly, heating the embedded sample die and finally, preparing the required embedded sample in the embedded sample die. In addition, the invention also discloses a quick preparation device for the embedded sample. According to the quick preparation method and the device for the embedded sample, which are disclosed by the invention, the embedded sample with a remarkable effect can be quickly and stably prepared, the production deficiency of the embedded sample is greatly improved and the production quality of the embedded sample is improved.
Description
Technical field
The present invention relates to the sample preparation technology field, particularly relate to a kind of fast preparation method and device thereof of inlaying sample, be used for the inlay sample of preparation fast based on polishing (Polish).
Background technology
At present, in order to obtain to inlay sample, need inlay earlier; Promptly form netted space polymer by epoxy curing agent and epoxy resin generation chemical reaction; Then compound substance aggregate envelope among reticulate body, thereby make the epoxy resin of line style finally become tough and tensile build solid, the sample solidifies that needs are observed is in this solid; In addition, can come the aspect effect pattern of observation sample through further grinding.
And in the process of the preparation of inlaying sample; At first need carry out proportioning to epoxy curing agent and epoxy resin solution; Require solution quantity accurate, when solution ratio, utilize balance to weigh usually, manually solution is stirred to stirring in the vessel by the workman.In view of when solution ratio, choosing the mode of agitating solution manually usually; And under room temperature environment, make epoxy curing agent and epoxy resin generation chemical reaction, to reach the effect of curing, therefore; The time of solidifying usually is unstable; And the mode of when solution stirring, generally taking glass bar manually to stir also can cause the stirring frequency of solution unstable, thereby brings bad influence also for the set time of sample and the final effect of inlaying.
Therefore, provide a kind of method simple to operate, that obvious results is inlayed the quick preparation of sample to become one of these those skilled in the art problem anxious to be addressed.
Therefore, press for a kind of method of developing at present, it can fast, stably be prepared obvious results and inlay sample, improves the production efficiency of inlaying sample greatly, reduces the production cost of inlaying sample.
Summary of the invention
In view of this, the purpose of this invention is to provide a kind of fast preparation method and device thereof of inlaying sample, it can fast, stably be prepared obvious results and inlay sample; Improve the production efficiency of inlaying sample greatly; Improve the quality of production of inlaying sample, reduce the production cost of inlaying sample, apply in helping producing widely; Further improve the produce market application prospect of inlaying sample manufacturer, be of great practical significance.
For this reason, the invention provides a kind of fast preparation method of inlaying sample, may further comprise the steps:
The first step: the epoxy curing agent solution and the epoxy resin solution that take by weighing preset weight ratio;
Second step: epoxy curing agent solution that is taken by weighing and epoxy resin solution are poured in same jar;
The 3rd step: epoxy curing agent solution and epoxy resin solution to putting in the jar at the uniform velocity stir, and form mixed solution;
The 4th step: said mixed solution is poured into one inlays in the sample mould;
The 5th step: the said sample mould of inlaying is heated, finally in inlaying the sample mould, prepare the needed sample of inlaying.
Wherein, also comprise step between said the 3rd step and the 4th step: the mixed solution that stirs the back acquisition is carried out deaeration handle.
Wherein, the weight ratio between said epoxy curing agent solution and the epoxy resin solution is 1:5.
Wherein, in the first step, come to take by weighing respectively epoxy curing agent solution and epoxy resin solution through transparent epoxy curing agent vessel, transparent epoxy resin vessel;
Has the weight scale line respectively on the outer wall of said epoxy curing agent vessel 1 and epoxy curing agent vessel.
Wherein, in the 3rd step, epoxy curing agent solution and the epoxy resin solution of putting in the jar at the uniform velocity stirred through a heating magnetic stirrer;
In the 5th step, the said sample mould of inlaying is heated through said heating magnetic stirrer.
In addition; The present invention also provides a kind of quick preparation device of inlaying sample; Include the heating magnetic stirrer, said heating magnetic stirrer top is used to place a jar or one and inlays the sample mould, and said jar is placed with a magneton with inlaying in the sample mould.
Wherein, also include transparent epoxy curing agent vessel and transparent epoxy resin vessel, have the weight scale line respectively on the outer wall of said epoxy curing agent vessel and epoxy curing agent vessel.
Wherein, said heating magnetic stirrer front panel is provided with a temperature adjustment knob and a magnetic force frequency adjustment knob.
Visible by above technical scheme provided by the invention; Compared with prior art, the invention provides a kind of fast preparation method and device thereof of inlaying sample, it can fast, stably be prepared obvious results and inlay sample; Improve the production efficiency of inlaying sample greatly; Improve the quality of production of inlaying sample, reduce the production cost of inlaying sample, apply in helping producing widely; Further improve the produce market application prospect of inlaying sample manufacturer, be of great practical significance.
Description of drawings
Fig. 1 is a kind of process flow diagram of inlaying the fast preparation method of sample provided by the invention;
Fig. 2 is the surface structure synoptic diagram of employed epoxy curing agent vessel in a kind of fast preparation method of inlaying sample provided by the invention and the device thereof;
Fig. 3 is the surface structure synoptic diagram of employed epoxy resin vessel in a kind of fast preparation method of inlaying sample provided by the invention and the device thereof;
Fig. 4 is the surface structure synoptic diagram of employed jar in a kind of fast preparation method of inlaying sample provided by the invention and the device thereof;
Fig. 5 is the surface structure synoptic diagram of employed mould in a kind of fast preparation method of inlaying sample provided by the invention and the device thereof;
Fig. 6 is that institute uses the surface structure synoptic diagram that heats magnetic stirrer in a kind of fast preparation method of inlaying sample provided by the invention and the device thereof;
Among the figure, 1 is the epoxy curing agent vessel, and 2 is the epoxy resin vessel, and 3 is jar, and 4 are the heating magnetic stirrer, and 5 is magneton, and 6 for inlaying the sample mould, and 7 are temperature adjustment knob, and 8 are magnetic force frequency adjustment knob.
Embodiment
In order to make those skilled in the art person understand the present invention program better, the present invention is done further detailed description below in conjunction with accompanying drawing and embodiment.
A kind of fast preparation method of inlaying sample provided by the invention is used for the inlay sample of preparation fast based on polishing (Polish), and referring to Fig. 1, this method may further comprise the steps:
The first step: the epoxy curing agent solution and the epoxy resin solution that take by weighing preset weight ratio;
Second step: epoxy curing agent solution that is taken by weighing and epoxy resin solution are poured in same jar (as shown in Figure 4);
The 3rd step: epoxy curing agent solution and epoxy resin solution to putting in the jar at the uniform velocity stir, and form mixed solution;
The 4th step: the mixed solution that stirs the back acquisition is carried out deaeration handle;
The 5th step: said mixed solution is poured into one inlays in the sample mould (as shown in Figure 5);
The 6th step: the said sample mould of inlaying is heated, finally in inlaying the sample mould, prepare the needed sample of inlaying.
In the present invention; In the first step; Weight ratio between said epoxy curing agent solution and the epoxy resin solution is preferably 1:5 (for example the epoxy curing agent solution of 5g and the epoxy resin solution of 10g); Certainly, according to user's needs, can also be by the solution of this proportional arrangement greater number.
In the present invention, the first step is concrete realizes that the present invention can come to take by weighing apace respectively epoxy curing agent solution and epoxy resin solution through transparent epoxy curing agent vessel shown in Figure 2, transparent epoxy resin vessel shown in Figure 3.Need to prove that said epoxy curing agent vessel 1 and the epoxy resin vessel 2 of showing adopt transparent material (for example glass) to process.
In the present invention, referring to Fig. 2, Fig. 3, has the weight scale line respectively on the outer wall of said epoxy curing agent vessel 1 and epoxy curing agent vessel 2.Need to prove that the weight scale line on said epoxy curing agent vessel 1 outer wall can be through in advance to being positioned at the acquisition of weighing of epoxy curing agent solution on this weight scale line; Weight scale line on said epoxy curing agent vessel 2 outer walls can be through in advance to being positioned at the acquisition of weighing of epoxy resin solution on this weight scale line.For example, can be provided with 2g and two weight scale lines of 4g on the said epoxy curing agent vessel 1 of Fig. 2 in advance, 10g and two weight scale lines of 20g can be set on the epoxy curing agent vessel 2 of Fig. 3 in advance.
Need to prove; The present invention is through using epoxy curing agent vessel 1 and epoxy curing agent vessel 2 these two kinds of special utensils of weighing; Can substitute electronic balance, measurement ring epoxy resins curing agent solution and epoxy resin solution accurately, easily, thus quantity variance is bigger because solution is more in the bucket when pouring out when avoiding directly using electronic balance; Cause solution ratio inaccurate, can realize solution proportioning accurately.
For the present invention; In the 3rd step; Can at the uniform velocity stir through epoxy curing agent solution and the epoxy resin solution that 5 pairs of the magnetons of a heating magnetic stirrer 4 as shown in Figure 6 are put in the jar; Specific operation process is: the magnetic agitation function of opening heating magnetic stirrer 4; (this pre-set velocity can be adjusted according to user's needs through magnetic force frequency adjustment knob 8 stirring rate to be adjusted to preset even speed; When the general assembly (TW) of epoxy curing agent solution that is taken by weighing and epoxy resin solution increased, the stirring rate that can heat magnetic stirrer 4 through magnetic force frequency adjustment knob 8 was set to fast speeds) and remain a constant speed, at the uniform velocity stir through 5 pairs of epoxy curing agent solution of magneton and epoxy resin solution then; Mixing time can be 10 minutes, can also be the other times of user preset certainly.
Need to prove; The present invention carries out solution stirring through utilizing heating magnetic stirrer 4 and adding magneton 5; Substitute the mode of existing manual agitating solution, stirring efficiency can be provided, and can guarantee epoxy curing agent solution and epoxy resin solution are evenly stirred; The quality of stirring is provided, and then guarantees the final end product quality of inlaying sample that obtains and attractive in appearance.
For the present invention, in the 4th step, can come that the mixed solution that stirs the back acquisition is carried out deaeration through a notes film machine or vacuum defoamation machine and handle.Need to prove that the 4th step was selectable step, can select to use with concrete stirring state according to user's needs.For example; When putting into epoxy curing agent solution and epoxy resin solution in the jar through 5 pairs of the magnetons of heating magnetic stirrer 4 and at the uniform velocity stir; Because epoxy curing agent solution and epoxy resin solution produce bubble in whipping process minimizing significantly at this time can be omitted the deaeration process, promptly omits for the 4th step; Further make the whole preparation time of inlaying sample shorten
For the present invention; In the 5th step; Employed shape, size of inlaying sample mould 6 determined by the shape of inlaying sample, the size of the required preparation of user; For example as shown in Figure 5, said sample mould 6 shapes, the size and the shape of inlaying sample of required preparation, big or small corresponding coupling of inlaying.
For the present invention; In the 6th step; Can heat through 4 pairs of said sample moulds 6 of inlaying of a heating magnetic stirrer as shown in Figure 6, specific operation process is: open the heating function of heating magnetic stirrer 4, through temperature adjustment knob 7 heating-up temperature is set to preset temperature then and (is preferably 50 ℃; Can certainly be other temperature); Continue the preset time period (be preferably 30 minutes, can certainly be the time period of other length) of heating, thus finally in inlaying sample mould 6 by behind epoxy curing agent solution and the epoxy resin solution generation chemical reaction; Reach the effect of curing, obtain the needed sample of inlaying thereby solidify.
To combine concrete embodiment that the present invention is carried out more detailed elaboration below, but should be understood that the present invention is not limited to this.
Fig. 2 to Fig. 4 prepares employed apparatus of stage for a kind of fast preparation method of inlaying sample provided by the invention at solution.Through Fig. 2, transparent epoxy curing agent vessel 1 shown in Figure 3 and transparent epoxy curing agent vessel 2; Because the top of them is designed with the weight scale line by the weight of weighing; Thereby can let the weight of epoxy curing agent solution and epoxy resin solution take by weighing very convenient, quick; Can also omit simultaneously the process of scales/electronic balance weighing, directly can obtain concrete gravimetric value through visual type.
On concrete the realization, for example, when needs begin to prepare one when inlaying sample; At first epoxy curing agent solution is poured into to epoxy curing agent vessel 1; Pour into to epoxy resin vessel 2 to the first weight scale line (being the weight scale line of 2g as shown in Figure 2), and with epoxy resin solution, to first scale mark (being the weight scale line of 10g as shown in Figure 3); Again epoxy curing agent vessel 1 and the solution in the epoxy resin vessel 2 are poured into respectively to jar 3; At this moment can in time in time clean, cause cleaning difficulty, so need after vessel use, in time utilize burnisher to clean for fear of resin and hardening agent overstand in vessel to epoxy curing agent vessel 1 and epoxy resin vessel 2; With the accuracy of guaranteeing that use next time, the solution preparation primary stage accomplishes.The method reduces the preparation time of solution, weight scale line visual measurement when pouring solution into simultaneously, and it is more convenient to operate.
Referring to Fig. 5, Fig. 6, Fig. 5, Fig. 6 are that a kind of fast preparation method of inlaying sample provided by the invention is at the employed apparatus of preparation process.As shown in Figure 6, fill the epoxy curing agent solution and the epoxy resin solution of the ratio of configuring in the jar 3, the magneton 5 of heating magnetic stirrer 4 is put into to this jar 3; Then jar 3 is positioned on the heating magnetic stirrer 4, the speed of the magnetic force frequency being adjusted knob 8 is adjusted at the uniform velocity, and epoxy curing agent solution and epoxy resin solution are fully at the uniform velocity stirred; After continuing to stir 10 minutes; Magnetic force frequency adjustment knob 8 is adjusted to initial position, at this moment can jar 3 be taken off, earlier the magneton in the jar 35 is taken out and in time cleans; To stir the mixed solution that forms by epoxy curing agent solution and epoxy resin solution again pours into to inlaying in the sample mould 6; Then will inlay sample mould 6 then and put to heating magnetic stirrer 4, and again temperature adjusted knob 7 and be adjusted to 50 ℃, continue heating after 30 minutes; Temperature is adjusted knob 7 be adjusted to initial position; To inlay sample mould 6 and take off, at this time, in inlaying sample mould 6, prepare the needed sample of inlaying of user from heating magnetic stirrer 4.After inlaying the sample cooling, can inlay the next rubbing down link of sample, the preparation process is accomplished.
The sample solidifies time of inlaying that a kind of fast preparation method of inlaying sample provided by the invention can be avoided causing because of room temperature influence effectively is elongated; Make operate more convenient; Make epoxy curing agent solution and epoxy resin solution in whipping process, produce the minimizing significantly of bubble simultaneously; Can omit the time of deaeration, make the preparation time of inlaying sample shorten, thereby improved work efficiency.
Based on the described a kind of fast preparation method of inlaying sample of Fig. 1; Referring to Fig. 2 to Fig. 6; The present invention also provides a kind of quick preparation device of inlaying sample; Include heating magnetic stirrer 4, said heating magnetic stirrer 4 tops are placed with a jar 3 or one and inlay sample mould 6, said jar 3 with inlay the magneton 5 that is placed with a said heating magnetic stirrer 4 in the sample mould 6.
In addition; A kind of quick preparation device of inlaying sample provided by the invention also includes transparent epoxy curing agent vessel shown in Figure 21 and transparent epoxy resin vessel 2 shown in Figure 3, and said epoxy curing agent vessel 1 are used for taking by weighing respectively epoxy curing agent solution and epoxy resin solution with epoxy resin vessel 2.Need to prove that said epoxy curing agent vessel 1 and the epoxy resin vessel 2 of showing adopt transparent material (for example glass) to process.
In the present invention, referring to Fig. 2, Fig. 3, has the weight scale line respectively on the outer wall of said epoxy curing agent vessel 1 and epoxy curing agent vessel 2.Need to prove that the weight scale line on said epoxy curing agent vessel 1 outer wall can be through in advance to being positioned at the acquisition of weighing of epoxy curing agent solution on this weight scale line; Weight scale line on said epoxy curing agent vessel 2 outer walls can be through in advance to being positioned at the acquisition of weighing of epoxy resin solution on this weight scale line.For example, can be provided with 2g and two weight scale lines of 4g on the said epoxy curing agent vessel 1 of Fig. 2 in advance, 10g and two weight scale lines of 20g can be set on the epoxy curing agent vessel 2 of Fig. 3 in advance.
In the present invention; Weight ratio between said epoxy curing agent solution and the epoxy resin solution is preferably 1:5 (for example the epoxy curing agent solution of 5g and the epoxy resin solution of 10g); Certainly, according to user's needs, can also utilize the solvent of this proportional arrangement greater number.
Need to prove; The present invention is through using epoxy curing agent vessel 1 and epoxy curing agent vessel 2 these two kinds of special utensils of weighing; Can substitute electronic balance, measurement ring epoxy resins curing agent solution and epoxy resin solution accurately, easily, thus quantity variance is bigger because solution is more in the bucket when pouring out when avoiding directly using electronic balance; Cause solution ratio inaccurate, can realize solution proportioning accurately.
For the present invention; Employed shape, size of inlaying sample mould 6 determined by the shape of inlaying sample, the size of the required preparation of user; For example as shown in Figure 5, said sample mould 6 shapes, the size and the shape of inlaying sample of required preparation, big or small corresponding coupling of inlaying.
Referring to Fig. 6; Said heating magnetic stirrer 4 front panels are provided with a temperature adjustment knob 7 and a magnetic force frequency adjustment knob 8; Said temperature adjustment knob 7 is used for that heating-up temperature is set to preset temperature and (is preferably 50 ℃; Can certainly be other temperature); Said magnetic force frequency adjustment knob 8 is used for stirring rate is adjusted to preset even speed (this pre-set velocity can be adjusted according to user's needs, when the general assembly (TW) of the epoxy curing agent solution that is taken by weighing and epoxy resin solution increases, adjusts the stirring rate that knob 8 can heat magnetic stirrer 4 through the magnetic force frequency and is set to fast speeds) and remained a constant speed.
Need to prove; Magneton 5 through heating magnetic stirrer 4 as shown in Figure 6 can carry out at the uniform velocity stirring operation to epoxy curing agent solution and the epoxy resin solution of putting in the jar; Specific operation process is: the magnetic agitation function of opening heating magnetic stirrer 4; Through magnetic force frequency adjustment knob 8 even speed (this pre-set velocity can be adjusted according to user's needs) that the stirring rate adjustment is preset and remain a constant speed; At the uniform velocity stir through 5 pairs of epoxy curing agent solution of magneton and epoxy resin solution then, mixing time can be 10 minutes, can also be the other times of user preset certainly.
Therefore; The present invention carries out solution stirring through utilizing heating magnetic stirrer 4 and adding magneton 5; Substitute the mode of existing manual agitating solution, stirring efficiency can be provided, and can guarantee epoxy curing agent solution and epoxy resin solution are evenly stirred; The quality of stirring is provided, and then guarantees the final end product quality of inlaying sample that obtains and attractive in appearance.
For the present invention; Can also carry out heating operation through 4 pairs of said sample moulds 6 of inlaying of heating magnetic stirrer as shown in Figure 6, specific operation process is: open the heating function of heating magnetic stirrer 4, through temperature adjustment knob 7 heating-up temperature is set to preset temperature then and (is preferably 50 ℃; Can certainly be other temperature); Continue the preset time period (be preferably 30 minutes, can certainly be the time period of other length) of heating, thus finally in inlaying sample mould 6 by behind epoxy curing agent solution and the epoxy resin solution generation chemical reaction; Reach the effect of curing, obtain the needed sample of inlaying thereby solidify.
For the invention discloses a kind of fast preparation method and device thereof of inlaying sample; At first in the solution preparation stage; Improve the failure that the manual error in when falling solution causes and inlay the sample generation; Epoxy curing agent solution and epoxy resin solution poured into respectively in the vessel that have weight scale line baffle plate, and quantity is inaccurate and the failure proportioning that causes makes the ratio preparation of solution more accurate when having avoided directly barreled solution being poured out; In the agitation phases of solution original manual alr mode is improved then; Solution is positioned on the heating magnetic stirrer that has magnetic function, speed is adjusted at the uniform velocity, make solution stirring more even; Reduce the generation of bubble in the whipping process; Even can omit the deaeration process, and make specimen preparation more attractive in appearance, reduced the specimen preparation time.The present invention can use the magnetic stirrer that is used for general solution stirring at the higher solution of other viscosity had new exploitation, thereby also promoted the range of application of stirring machine in other solution, makes work more convenient, effective.
The present invention stirs solution through the heating magnetic stirrer automatically, and heats through heating magnetic stirrer or climatic chamber, thereby can realize quick curing.On concrete the realization, need to solidify fast use when inlaying sample, can carry out a large amount of samples through climatic chamber and heat, to realize quick curing owing to prepare in a large number.Through different heating conditions and heat time heating time are set, the preparation efficiency of inlaying sample can be higher, and the preparation process is simply quick, and effect is remarkable.
Therefore, compared with prior art, a kind of fast preparation method and device thereof of inlaying sample provided by the invention; It can fast, stably be prepared obvious results and inlay sample, improves the production efficiency of inlaying sample greatly, improves the quality of production of inlaying sample; Reduce the production cost of inlaying sample; Apply in helping producing widely, further improve the produce market application prospect of inlaying sample manufacturer, be of great practical significance.
The above only is a preferred implementation of the present invention; Should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention; Can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (8)
1. a fast preparation method of inlaying sample is characterized in that, may further comprise the steps:
The first step: the epoxy curing agent solution and the epoxy resin solution that take by weighing preset weight ratio;
Second step: epoxy curing agent solution that is taken by weighing and epoxy resin solution are poured in same jar;
The 3rd step: epoxy curing agent solution and epoxy resin solution to putting in the jar at the uniform velocity stir, and form mixed solution;
The 4th step: said mixed solution is poured into one inlays in the sample mould;
The 5th step: the said sample mould of inlaying is heated, finally in inlaying the sample mould, prepare the needed sample of inlaying.
2. preparation method as claimed in claim 1 is characterized in that, also comprises step between said the 3rd step and the 4th step: the mixed solution that stirs the back acquisition is carried out deaeration handle.
3. preparation method as claimed in claim 1 is characterized in that, the weight ratio between said epoxy curing agent solution and the epoxy resin solution is 1:5.
4. preparation method as claimed in claim 1 is characterized in that, in the first step, comes to take by weighing respectively epoxy curing agent solution and epoxy resin solution through transparent epoxy curing agent vessel, transparent epoxy resin vessel;
Has the weight scale line respectively on the outer wall of said epoxy curing agent vessel and epoxy curing agent vessel.
5. like each described preparation method in the claim 1 to 4, it is characterized in that, in the 3rd step, epoxy curing agent solution and the epoxy resin solution of putting in the jar at the uniform velocity stirred through a heating magnetic stirrer;
In the 5th step, the said sample mould of inlaying is heated through said heating magnetic stirrer.
6. quick preparation device of inlaying sample; It is characterized in that; Include heating magnetic stirrer (4); Said heating magnetic stirrer (4) top is used to place a jar (3) or one and inlays sample mould (6), said jar (3) and inlay and be placed with a magneton (5) in the sample mould (6).
7. preparation facilities as claimed in claim 6; It is characterized in that; Also include transparent epoxy curing agent vessel (1) and transparent epoxy resin vessel (2), have the weight scale line respectively on the outer wall of said epoxy curing agent vessel (1) and epoxy curing agent vessel (2).
8. preparation facilities as claimed in claim 6 is characterized in that, said heating magnetic stirrer (4) front panel is provided with a temperature adjustment knob (7) and a magnetic force frequency adjustment knob (8).
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| CN2012102066930A CN102721584A (en) | 2012-06-21 | 2012-06-21 | Quick preparation method and device for embedded sample |
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| CN2012102066930A CN102721584A (en) | 2012-06-21 | 2012-06-21 | Quick preparation method and device for embedded sample |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103487312A (en) * | 2013-10-15 | 2014-01-01 | 攀钢集团攀枝花钢铁研究院有限公司 | Specimen embedding device |
| CN107631917A (en) * | 2016-07-18 | 2018-01-26 | 中国电力科学研究院 | A kind of solidifying and molding device and method of superconductor test specimen |
| CN108226203A (en) * | 2018-01-02 | 2018-06-29 | 无锡小天鹅股份有限公司 | The detection method of the forked frame of washing machine and the forked frame of washing machine |
| CN108827742A (en) * | 2018-04-20 | 2018-11-16 | 朱兆明 | A kind of portable sample processing device and its application method |
| CN114633389A (en) * | 2022-03-29 | 2022-06-17 | 上海喆航航空科技有限公司 | Method for preparing bi-component mixture and application |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2411842Y (en) * | 2000-02-29 | 2000-12-27 | 陈妙凤 | Heating magnetic agitator |
| CN201537471U (en) * | 2009-11-20 | 2010-08-04 | 北京四环科学仪器厂有限公司 | Lifting heat-collecting magnetic stirring equipment |
| CN101900647A (en) * | 2010-07-30 | 2010-12-01 | 西北有色金属研究院 | Micron-sized metal powder metallic phase mounting method |
| CN101949791A (en) * | 2010-09-16 | 2011-01-19 | 中国科学院西安光学精密机械研究所 | Sample preparation method for mechanical property test of carbon fiber |
| US20110103175A1 (en) * | 2008-06-24 | 2011-05-05 | Ika-Werke Gmbh & Co. Kg | Magnetic stirrer with mounting feet |
| CN102359904A (en) * | 2011-09-30 | 2012-02-22 | 黑龙江建龙钢铁有限公司 | Multifunctional metallic phase sample inlaying machine |
| CN102419276A (en) * | 2011-08-16 | 2012-04-18 | 上海华碧检测技术有限公司 | Preparation method of metallographic microsection sample |
| CN202837053U (en) * | 2012-06-21 | 2013-03-27 | 三星高新电机（天津）有限公司 | Fast manufacture device of embedding samples |
-
2012
- 2012-06-21 CN CN2012102066930A patent/CN102721584A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2411842Y (en) * | 2000-02-29 | 2000-12-27 | 陈妙凤 | Heating magnetic agitator |
| US20110103175A1 (en) * | 2008-06-24 | 2011-05-05 | Ika-Werke Gmbh & Co. Kg | Magnetic stirrer with mounting feet |
| CN201537471U (en) * | 2009-11-20 | 2010-08-04 | 北京四环科学仪器厂有限公司 | Lifting heat-collecting magnetic stirring equipment |
| CN101900647A (en) * | 2010-07-30 | 2010-12-01 | 西北有色金属研究院 | Micron-sized metal powder metallic phase mounting method |
| CN101949791A (en) * | 2010-09-16 | 2011-01-19 | 中国科学院西安光学精密机械研究所 | Sample preparation method for mechanical property test of carbon fiber |
| CN102419276A (en) * | 2011-08-16 | 2012-04-18 | 上海华碧检测技术有限公司 | Preparation method of metallographic microsection sample |
| CN102359904A (en) * | 2011-09-30 | 2012-02-22 | 黑龙江建龙钢铁有限公司 | Multifunctional metallic phase sample inlaying machine |
| CN202837053U (en) * | 2012-06-21 | 2013-03-27 | 三星高新电机（天津）有限公司 | Fast manufacture device of embedding samples |
Non-Patent Citations (1)
| Title |
|---|
| 王斌 等: "《物理金相实验工基本操作技能（初级工适用）》", 31 August 1992, article "训练3-4 试样冷镶嵌的准备及操作", pages: 42-45 * |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103487312A (en) * | 2013-10-15 | 2014-01-01 | 攀钢集团攀枝花钢铁研究院有限公司 | Specimen embedding device |
| CN103487312B (en) * | 2013-10-15 | 2016-02-17 | 攀钢集团攀枝花钢铁研究院有限公司 | Sample inlaying device |
| CN107631917A (en) * | 2016-07-18 | 2018-01-26 | 中国电力科学研究院 | A kind of solidifying and molding device and method of superconductor test specimen |
| CN108226203A (en) * | 2018-01-02 | 2018-06-29 | 无锡小天鹅股份有限公司 | The detection method of the forked frame of washing machine and the forked frame of washing machine |
| CN108226203B (en) * | 2018-01-02 | 2020-09-22 | 无锡小天鹅电器有限公司 | Detection method of washing machine fork-shaped frame and washing machine fork-shaped frame |
| CN108827742A (en) * | 2018-04-20 | 2018-11-16 | 朱兆明 | A kind of portable sample processing device and its application method |
| CN108827742B (en) * | 2018-04-20 | 2020-12-18 | 林雅娟 | Portable sample processing device and using method thereof |
| CN114633389A (en) * | 2022-03-29 | 2022-06-17 | 上海喆航航空科技有限公司 | Method for preparing bi-component mixture and application |
| CN115728194A (en) * | 2022-11-21 | 2023-03-03 | 山东大学 | Method for detecting crystal grain morphology of copper foil section |
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Application publication date: 20121010 |