CN102703105A - Refining method of fuel oil by organic refuse - Google Patents

Refining method of fuel oil by organic refuse Download PDF

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CN102703105A
CN102703105A CN2012101186136A CN201210118613A CN102703105A CN 102703105 A CN102703105 A CN 102703105A CN 2012101186136 A CN2012101186136 A CN 2012101186136A CN 201210118613 A CN201210118613 A CN 201210118613A CN 102703105 A CN102703105 A CN 102703105A
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oil
tower
gas
organic waste
oil fuel
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CN102703105B (en
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林柏辉
郑仲新
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel

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Abstract

A refining unit of fuel oil by organic refuse comprises a reactor, a gasifier, a catalytic tower, a primary condensing tower, a catalytic reforming tower and a secondary condensing tower. The reactor is communicated with the catalytic tower through a gas guide pipe. The catalytic tower is communicated with the primary condensing tower through a gas guide pipe. The gasifier, the catalytic tower and the primary condensing tower are respectively connected with an oil-water separator. The oil-water separator is provided with a water outlet and an oil outlet, is communicated with the catalytic reforming tower through the oil outlet, and is connected with a sewage treatment tank through the water outlet. The catalytic reforming tower is communicated with the secondary condensing tower through a gas guide pipe. The secondary condensing tower is respectively communicated with an oil storage tank and the sewage treatment tank through the oil-water separator. The gasifier and the primary condensing tower are connected with a combustion device of the reactor through a gas guide pipe. The secondary condensing tower is connected with a combustion device of the catalytic reforming tower through a gas guide pipe. The organic refuse is reused reasonably, which helps reduce refuse burden for cities.

Description

Utilize the method for organic waste refining oil fuel
Technical field
The present invention relates to technology of garbage disposal, especially utilize the method for organic waste refining oil fuel.
Background technology
The human being's production life produces a large amount of rubbish, and it is a kind of source of pollution, is again a kind of available energy.According to statistics, the present domestic waste of China is annual to produce about more than 200,000,000 tons, and just increases with 10% speed, and China has become the heavy country of rubbish burden amount in the world, municipal wastes innoxious, subtract appearanceization and recycling treatment is extremely urgent.Municipal wastes has moisture big (moisture reaching about 30% in the rubbish), refuse thermal value is low, the characteristics of complicated component (containing hard foreign material such as porcelain, rotary head, rubble, glass, earth, metal in the rubbish).After rubbish carried out preliminary sorting, can rubbish be divided into hard foreign material such as organism, inorganics and metallic glass.At present, can be divided into three kinds to organic utilization in the rubbish: be direct regenerated using; A kind of is the modification utilization; Also having a kind of is exactly the cracking trans-utilization.But these three kinds of methods all need earlier organic matter rubbish to be carried out sorting; Waste or used plastics in the organic matter rubbish is sorted out, also need carry out pre-washing and oven dry to it, this needs a large amount of sorting costs; And the generation large amount of sewage, be unfavorable for the garbage utilization industrialization.
Summary of the invention
Technical problem to be solved by this invention provides a kind of method of utilizing organic waste refining oil fuel, and organic matter rubbish is reasonably utilized again, helps to alleviate the burden of city to rubbish; The oil fuel that produces after the treating refuse helps to solve the situation of present energy dilemma; In addition, the refuse treatment cost is low, treating processes is simple, helps scale operation.
For solving the problems of the technologies described above, technical scheme of the present invention is: a kind of method of utilizing organic waste refining oil fuel may further comprise the steps:
(1) sorting rubbish mainly is that organic waste is separated with inorganic refuse;
(2) organic waste is delivered in the reaction kettle, added catalyzer, under normal pressure, be heated to 300～400 ℃, organic waste is carried out thermocatalysis decompose, produce cinder, sewage, oil fuel, mixed oil and gas; Cinder is entered in the vapourizing furnace; Oil fuel is collected; Sewage is carried out WWT; Mixed oil and gas is sent in the catalytic tower;
(3) add catalyzer in the vapourizing furnace, cinder is carried out catalytically decomposed having under the environment of air, produce oil fuel, sewage, inflammable gas, oil fuel is collected; Sewage is carried out WWT; With gas fuel burning is the reaction kettle heat supply;
(4) add catalyzer in the catalytic tower, mixed oil and gas is carried out catalytically decomposed, a part of mixed oil and gas converts oil-water mixture to, and oil-water mixture is separated into sewage and oil fuel through water-and-oil separator, and sewage is carried out WWT; Oil fuel is collected; Another part mixed oil and gas gets into condensing tower;
(5) the mixed oil and gas part of entering condensing tower is condensed into oil-water mixture, and oil-water mixture separates into sewage and oil fuel through water-and-oil separator, and sewage is carried out WWT; Oil fuel is collected; Remaining mixed oil and gas is sent the reaction kettle burning back to and for reaction kettle heat energy is provided in the condensing tower.
As improvement, the oil fuel of collecting in said step (2)～(4) is sent into the CR tower, adds catalyzer, under normal pressure, is heated to 200～300 ℃, obtains mixed oil and gas; Mixed oil and gas is sent to condensing tower again; Part mixed oil and gas is condensed into the mixing profit, mixes profit and obtains sewage and oil fuel through behind the water-and-oil separator again, and the oil fuel stink of this part is little; Diesel oil is similar in color; Oil fuel is stored, sewage is carried out WWT, uncooled mixed oil and gas burns and is the heat supply of CR tower.
As improvement, in the said step (3), inflammable gas mainly comprises CO, methane and aromatics inflammable gas.
As improvement, said reaction kettle mainly comprises expects chamber, reaction chamber and cooling room, and organic waste is through expecting that the chamber gets into reaction chamber and reacts, and cinder is sent into vapourizing furnace after cooling off through cooling room.
As improvement, be provided with the catalytic pyrolysis chamber in the said catalytic tower, the indoor catalytic plate that is provided with of catalytic pyrolysis, below, catalytic pyrolysis chamber is provided with water-and-oil separator, is respectively equipped with water outlet and oil outlet on the said water-and-oil separator.
As improvement, be provided with condensing chamber in the said condensing tower, be provided with the cooling tube that supplies refrigerant to import in the condensing chamber, the condensing chamber below is provided with water-and-oil separator, is respectively equipped with water outlet and oil outlet on the said water-and-oil separator.
As improvement, the catalyzer in said step (2) reaction kettle comprise following composition (by weight):
Figure BDA0000155342300000031
As improvement, the catalyzer in said step (3) vapourizing furnace comprise following composition (by weight):
Figure BDA0000155342300000032
As improvement, the catalyzer in said step (4) catalytic tower comprise following composition (by weight):
Figure BDA0000155342300000041
As improvement, the catalyzer in the said CR tower comprise following composition (by weight):
Tsp 15～25%
Magnesium Trisilicate 65～75%
The artificial zeolite 5～15%.
The beneficial effect that the present invention is compared with prior art brought is:
The method of organic waste refining oil fuel of the present invention is reasonably utilized organic matter rubbish again, helps to alleviate the burden of city to rubbish; The oil fuel that produces after the treating refuse helps to solve the situation of present energy dilemma; In addition, the refuse treatment cost is low, treating processes is simple, helps scale operation.
Description of drawings
Fig. 1 is a process flow sheet of the present invention.
Fig. 2 is the reaction kettle structural representation.
Fig. 3 is the catalytic tower structural representation.
Fig. 4 is the condensing tower structural representation.
Fig. 5 is a CR tower structure synoptic diagram.
Embodiment
Below in conjunction with Figure of description the present invention is described further.
Embodiment 1
As shown in Figure 1, a kind of method of utilizing organic waste refining oil fuel comprises the following step:
(1) sorting rubbish; Sorting rubbish mainly is that organic waste is separated with inorganic refuse, carries out drying to containing the big organic waste of moisture, and other contain the few organic waste of moisture can not carry out drying;
(2) organic waste is delivered in the reaction kettle 1, added catalyzer, catalyzer comprises following composition (by weight percentage): CaO 25%, AL 2O 335%, SiO 215%, artificial zeolite 20%, water 5%; Under normal pressure, be heated to 300～400 ℃, organic waste carried out thermocatalysis decompose, produce cinder (staple is a charcoal), sewage, oil fuel, mixed oil and gas, cinder is entered in the vapourizing furnace 2; Oil fuel is collected; Sewage is carried out WWT; Mixed oil and gas is sent in the catalytic tower 3;
(3) add catalyzer in the vapourizing furnace 2, catalyzer comprises following composition (by weight percentage): CaO 45%, AL 2O 315%, iron powder 35%, water 5%; Cinder is carried out catalytically decomposed having under the environment of air, produce oil fuel, sewage, inflammable gas, oil fuel is collected; Sewage is carried out WWT; Inflammable gas mainly comprises CO, methane and aromatics inflammable gas, is reaction kettle 1 heat supply with gas fuel burning;
(4) add catalyzer in the catalytic tower 3, catalyzer comprises following composition (by weight percentage): CaO 35%, AL 2O 315%, SiO 225%, coalitenessity 15%, water 10%; Mixed oil and gas is carried out catalytically decomposed, and a part of mixed oil and gas converts oil-water mixture to, and oil-water mixture is separated into sewage and oil fuel through water-and-oil separator 7, and sewage is carried out WWT; Oil fuel is collected; Another part mixed oil and gas gets into condensing tower 4;
(5) the mixed oil and gas part of entering condensing tower 4 is condensed into oil-water mixture, and oil-water mixture separates into sewage and oil fuel through water-and-oil separator 7, and sewage is carried out WWT; Oil fuel is collected; Remaining mixed oil and gas is sent reaction kettle 1 burning back to and for reaction kettle 1 heat energy is provided in the condensing tower 4;
(6) oil fuel of collecting in step (2)～(5) is sent into CR tower 5; Add catalyzer; Catalyzer comprise following composition (by weight): tsp 15%, Magnesium Trisilicate 75%, artificial zeolite 10%; Under normal pressure, be heated to 200～300 ℃, obtain mixed oil and gas, this mixed oil and gas is delivered in another condensing tower 6;
(7) mixed oil and gas is condensed in condensing tower 6 once more; Part mixed oil and gas is condensed into the mixing profit, mixes profit and obtains sewage and oil fuel through behind the water-and-oil separator 7 again, and the oil fuel stink of this part is little; Diesel oil is similar in color; Oil fuel is sent into storage tank 8 store, sewage is carried out WWT, uncooled mixed oil and gas burns and is 5 heat supplies of CR tower.
As shown in Figure 2, said reaction kettle 1 mainly comprises expects chamber 11, reaction chamber 12 and cooling room 13, and reaction chamber 13 bottoms are provided with heating unit 13, and reaction chamber 12 tops are provided with gas tube 15 and catalyzer ingress pipe 14.Reaction chamber 12 is a sealed state, and organic waste is through expecting that chamber 11 gets into reaction chambers 12 and reacts, and reacted cinder is discharged to cooling room 13 earlier, enters vapourizing furnace 2 again after waiting cooling.Catalyzer enters in the reaction kettle 1 through the catalyzer ingress pipe 14 of reactor top; The mixed oil and gas that reaction kettle 1 is produced gets in the catalytic tower 3 through gas tube 15.Reaction chamber 12 bottoms also are provided with water shoot 17.
As shown in Figure 3; Said catalytic tower 3 tops are provided with catalytic tower lid 31 and tank 32; Inside is provided with catalytic pyrolysis chamber 36, and catalytic pyrolysis chamber 36 is provided with inlet mouth 33 and air outlet 34, is provided with catalytic plate 35 in the catalytic pyrolysis chamber 36; 36 belows, catalytic pyrolysis chamber are provided with water-and-oil separator 7, and water-and-oil separator 7 is provided with water outlet 73 and oil outlet 72.Reaction kettle 1 imports mixed oil and gas through gas tube 15 in the catalytic pyrolysis chamber 36 of catalytic tower 3 and reacts; The mixing profit that produces falls into water-and-oil separator 7 to be separated; CR tower 5 is derived and delivered to isolated oil fuel from oil outlet 72, and WWT is derived and sent to sewage from water outlet 73.
As shown in Figure 4; Said condensing tower 4 tops are provided with condensation Tata lid 41 and tank 42; Be provided with condensing chamber 46 in the said condensing tower 4; Be provided with the spiral tube 45 that is used to load refrigerant in the condensing chamber 46, condensing chamber 46 belows are provided with water-and-oil separator 7, and water-and-oil separator 7 is connected with oil outlet 72 with water outlet 73 respectively.A mixed oil and gas part that gets into condensing tower 4 is condensed into oil-water mixture; Oil-water mixture separates into sewage and oil fuel through water-and-oil separator 7; Sewage is carried out WWT; Oil fuel is delivered to CR tower 5, and remaining mixed oil and gas is sent reaction kettle 1 burning back to and for reaction kettle 1 heat energy is provided in the condensing tower 4.
As shown in Figure 5, be provided with storing chamber 54 in the said CR tower 5, the CR tower 5 outer thermal insulation layers 53 that are provided with; Be provided with whisking appliance 56 in the storing chamber 54, the top is provided with oil-feed S pipe 51 and air outlet 52, and the below is provided with combustion unit 55.The oil fuel that reaction draws in reaction kettle 1, vapourizing furnace, catalytic tower 3 and the condensing tower 4 gets into CR tower 5 through oil-feed S pipe 51; Carry out in the catforming process at oil fuel, the residual air that combustion unit 55 burnings are provided by condensing tower 4,56 pairs of oil fuel of whisking appliance stir; Accelerated reaction; The mixed oil and gas that produces gets into the condensing tower 6 of next stage through air outlet 52, and the reaction principle of next stage condensing tower the same with before no longer is described in detail.
The survey report of the oil fuel that draws is following:
Figure BDA0000155342300000071
The method of organic waste refining oil fuel of the present invention is reasonably utilized organic matter rubbish again, helps to alleviate the burden of city to rubbish; The oil fuel that produces after the treating refuse helps to solve the situation of present energy dilemma; In addition, the refuse treatment cost is low, treating processes is simple, helps scale operation.
Embodiment 2
Different is that the catalyzer in the reaction kettle 1 comprises following composition (by weight percentage): CaO 30%, AL with embodiment 1 2O 330%, SiO 210%, artificial zeolite 20%, water 10%;
Catalyzer in the vapourizing furnace 2 comprises following composition (by weight percentage): CaO 50%, AL 2O 310%, iron powder 30%, water 10%;
Catalyzer in the catalytic tower 3 comprises following composition (by weight percentage): CaO 40%, AL 2O 310%, SiO 220%, coalitenessity 20%, water 10%;
Catalyzer in the CR tower 5 comprises following composition (by weight percentage): tsp 20%, Magnesium Trisilicate 70%, artificial zeolite 10%.
The survey report of the oil fuel that draws is following:
Figure BDA0000155342300000081
Embodiment 3
Different is that the catalyzer in the reaction kettle 11 comprise following composition (by weight percentage): CaO 35%, AL with embodiment 1 2O 325%, SiO 25%, artificial zeolite 25%, water 10%;
Catalyzer in the vapourizing furnace 2 comprises following composition (by weight percentage): CaO 55%, AL 2O 35%, iron powder 25%, water 15%;
Catalyzer in the catalytic tower 3 comprises following composition (by weight percentage): CaO 45%, AL 2O 35%, SiO 215%, coalitenessity 25%, water 10%;
Catalyzer in the CR tower 5 comprises following composition (by weight percentage): tsp 25%, Magnesium Trisilicate 65%, artificial zeolite 10%.
The survey report of the oil fuel that draws is following:
Figure BDA0000155342300000092

Claims (10)

1. a method of utilizing organic waste refining oil fuel is characterized in that, may further comprise the steps:
(1) sorting rubbish mainly is that organic waste is separated with inorganic refuse;
(2) organic waste is delivered in the reaction kettle, added catalyzer, under normal pressure, be heated to 300～400 ℃, organic waste is carried out thermocatalysis decompose, produce cinder, sewage, oil fuel, mixed oil and gas; Cinder is entered in the vapourizing furnace; Oil fuel is collected; Sewage is carried out WWT; Mixed oil and gas is sent in the catalytic tower;
(3) add catalyzer in the vapourizing furnace, cinder is carried out catalytically decomposed having under the environment of air, produce oil fuel, sewage, inflammable gas, oil fuel is collected; Sewage is carried out WWT; With gas fuel burning is the reaction kettle heat supply;
(4) add catalyzer in the catalytic tower, mixed oil and gas is carried out catalytically decomposed, a part of mixed oil and gas converts oil-water mixture to, and oil-water mixture is separated into sewage and oil fuel through water-and-oil separator, and sewage is carried out WWT; Oil fuel is collected; Another part mixed oil and gas gets into condensing tower;
(5) the mixed oil and gas part of entering condensing tower is condensed into oil-water mixture, and oil-water mixture separates into sewage and oil fuel through water-and-oil separator, and sewage is carried out WWT; Oil fuel is collected; Remaining mixed oil and gas is sent the reaction kettle burning back to and for reaction kettle heat energy is provided in the condensing tower.
2. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that:
The oil fuel of collecting in said step (2)～(5) is sent into the CR tower, adds catalyzer, under normal pressure, is heated to 200～300 ℃, obtains mixed oil and gas; Mixed oil and gas is sent to condensing tower again; Part mixed oil and gas is condensed into the mixing profit, mixes profit and obtains sewage and oil fuel through behind the water-and-oil separator again, and oil fuel is stored; Sewage is carried out WWT, and uncooled mixed oil and gas burns and is the heat supply of CR tower.
3. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that:
In the said step (3), inflammable gas mainly comprises CO, methane and aromatics inflammable gas.
4. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that:
Said reaction kettle mainly comprises expects chamber, reaction chamber and cooling room, and organic waste is through expecting that the chamber gets into reaction chamber and reacts, and cinder is sent into vapourizing furnace after cooling off through cooling room.
5. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that:
Be provided with the catalytic pyrolysis chamber in the said catalytic tower, the indoor catalytic plate that is provided with of catalytic pyrolysis, below, catalytic pyrolysis chamber is provided with water-and-oil separator, and said water-and-oil separator is respectively equipped with water outlet and oil outlet.
6. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that:
Be provided with condensing chamber in the said condensing tower, be provided with the cooling tube that supplies refrigerant to import in the condensing chamber, the condensing chamber below is provided with water-and-oil separator, and said water-and-oil separator is respectively equipped with water outlet and oil outlet.
7. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that: the catalyzer in said step (2) reaction kettle comprise following composition (by weight):
Figure FDA0000155342290000021
8. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that: the catalyzer in said step (3) vapourizing furnace comprise following composition (by weight):
Figure FDA0000155342290000022
Figure FDA0000155342290000031
9. the method for utilizing organic waste refining oil fuel according to claim 1 is characterized in that:
Catalyzer in said step (4) catalytic tower comprise following composition (by weight):
Figure FDA0000155342290000032
10. the method for utilizing organic waste refining oil fuel according to claim 2 is characterized in that:
Catalyzer in the said CR tower comprise following composition (by weight):
Tsp 15～25%
Magnesium Trisilicate 65～75%
The artificial zeolite 5～15%.
CN201210118613.6A 2012-04-20 2012-04-20 Refining method of fuel oil by organic refuse Expired - Fee Related CN102703105B (en)

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CN103849408A (en) * 2014-03-20 2014-06-11 芜湖昌能环保技术有限公司 Method and system for producing fuel oil from garbage

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CN103849408A (en) * 2014-03-20 2014-06-11 芜湖昌能环保技术有限公司 Method and system for producing fuel oil from garbage
CN103849408B (en) * 2014-03-20 2016-04-27 芜湖昌能环保技术有限公司 The method and system of fuel oil produced by rubbish

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