CN102680611A - Novel fully-automatic vacuum mixing and degassing device - Google Patents
Novel fully-automatic vacuum mixing and degassing device Download PDFInfo
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- CN102680611A CN102680611A CN2012101478825A CN201210147882A CN102680611A CN 102680611 A CN102680611 A CN 102680611A CN 2012101478825 A CN2012101478825 A CN 2012101478825A CN 201210147882 A CN201210147882 A CN 201210147882A CN 102680611 A CN102680611 A CN 102680611A
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Abstract
The invention provides a novel fully-automatic vacuum mixing and degassing device, which comprises a thermostat, a mixing device, an intelligent controlled heating device, a vacuumizing device, a gas intake device, an oil intake device, a filtering device, a degassing volume judgment device, a gas collecting device and a control electromagnetic valve. The novel fully-automatic vacuum mixing and degassing device disclosed by the invention can be used for automatically finishing vacuumizing, air intake, oil intake, heating, mixing, gas analysis and gas collection operations, ensuring the experimental stability and avoiding experimental errors, thereby improving the operating rate. The novel fully-automatic vacuum mixing and degassing device is simple in structure and convenient to operate.
Description
Technical field
The present invention relates to a kind of full-automatic stirring degasser, be more particularly to new automatic vacuum stirring degasser, belong to a kind of apparatus field that is used for Transformer Oil Analysis gas.
Background technology
At present, the known standard GB/T17623-1998 gas Chromatographic Determination method of oil dissolved gas " insulation " recommends to utilize head space to get the gas method transformer oil is carried out machinery concussion to outgas, and the gas that will deviate from is then sent into pick-up unit and carried out quantitative test; The process need of gas in its whole Transformer Oil Analysis: the long-range oil of getting; Transportation, the manual balance gas that adds is put into mechanical rocking equipment; And shake; Manually take out gas, the gas that manually will deviate from is at last sent into pick-up unit and is carried out quantitative test, usually through manually gas being got in the chromatograph; So complex operation, inefficiency, the factor of man's activity is too big, and is very high to the requirement of operator's technical merit simultaneously.
Summary of the invention the objective of the invention is to overcome above deficiency, provides: new automatic vacuum stirring degasser, it can improve operating rate, guarantees experiment stability, reduces experimental error.
A kind of new automatic vacuum stirring degasser; Comprise: constant temperature oven, stirring apparatus, Based Intelligent Control heating arrangement, vacuum extractor, admission gear, oil-feed device, filtration unit, judgement degassing volume device, collection gas device; Vacuum extractor connects the stirring vessel top of stirring apparatus; Admission gear connects the stirring vessel bottom of stirring apparatus, and the oil-feed device connects the stirring vessel bottom of stirring apparatus, and the inlet end of filtration unit connects the stirring vessel top of stirring apparatus; The inlet end of the outlet side connection judgment degassing volume device of filtration unit; The inlet end of judging degassing volume device is connected with pipeline with the other end, judges that the other end of degassing volume device connects control electromagnetic valve, and control electromagnetic valve connects collects gas device; The Based Intelligent Control heating arrangement is installed on the constant temperature oven, and the Based Intelligent Control heating arrangement also is installed on the stirring apparatus.
Judge that degassing volume device comprises: the control electromagnetic valve of the sealed end of pressure transducer, the control electromagnetic valve that connects the pressure transducer inlet end, connection pressure transducer.
Stirring apparatus comprises sealed stirrer ware, stirring motor, stirrer, and stirrer is arranged on and stirs in the vessel, and stirring motor is connected with stirrer.
The Based Intelligent Control heating arrangement comprises heating rod, temperature sensor probe, temperature control panel.
Vacuum extractor comprises vacuum pump, control electromagnetic valve; Vacuum pump is connected with control electromagnetic valve.
Admission gear is connected with the stirring vessel bottom of stirring apparatus through control electromagnetic valve; The oil-feed device is connected with the stirring vessel bottom of stirring apparatus through control electromagnetic valve.
The invention has the beneficial effects as follows:
The present invention can accomplish automatically and vacuumize, air inlet, oil-feed, heating, stirring, analytical gas, collection gas, guarantees experiment stability, avoids experimental error, has improved operating rate.The present invention is simple in structure, and is easy to operate.
Description of drawings
Fig. 1 is a structural representation of the present invention.
Fig. 2 is that heating rod and the sensor probe on the Based Intelligent Control heating arrangement is installed in the synoptic diagram that stirs on the vessel.
Embodiment
Below in conjunction with accompanying drawing the present invention is elaborated
New automatic vacuum stirring degasser; Comprise: constant temperature oven 1, stirring apparatus 6, Based Intelligent Control heating arrangement, vacuum extractor 8, admission gear 9, oil-feed device 10, filtration unit 13, judgement degassing volume device 19, collection gas device 18; Vacuum extractor 8 connects stirring vessel 11 tops of stirring apparatus 6; Admission gear 9 connects stirring vessel 11 bottoms of stirring apparatus 6; Oil-feed device 10 connects stirring vessel 11 bottoms of stirring apparatus 6; The inlet end of filtration unit 13 connects stirring vessel 11 tops of stirring apparatus 6, and the inlet end of the outlet side connection judgment degassing volume device 19 of filtration unit 13 judges that the inlet end of degassing volume device 19 is connected with pipeline 20 with the other end; The other end of judging degassing volume device 19 connects control electromagnetic valve 17; Control electromagnetic valve 17 connects collects gas device 18, and the Based Intelligent Control heating arrangement is installed on the constant temperature oven 1, and the Based Intelligent Control heating arrangement also is installed on the stirring apparatus 6.
Judge that degassing volume device 19 comprises: the control electromagnetic valve 15 of the sealed end of pressure transducer 16, the control electromagnetic valve 14 that connects pressure transducer 16 inlet ends, connection pressure transducer 16.
Stirring apparatus 6 comprises sealed stirrer ware 11, stirring motor 7, stirrer 12, and stirrer 12 is arranged on and stirs in the vessel 11, and stirring motor 7 is connected with stirrer 12.On the wall of the stirring vessel 11 that heating rod 22 on the Based Intelligent Control heating arrangement and sensor probe 21 are installed in stirring apparatus 6.
The Based Intelligent Control heating arrangement comprises three heating rods 22, temperature sensor probe 21, temperature control panel.
The concrete operations step is:
1. start automatic workflow, the Based Intelligent Control heating arrangement of opening on the constant temperature oven 1 makes constant temperature oven 1 inner constant temperature.Ceaselessly heating makes constant temperature oven 1 inside remain on 60 ℃ of constant temperature through temperature sensor probe 21 in whole workflow, accomplishes up to whole lock out operation to stop.
2. vacuumize processing, open vacuum extractor 8, the vacuum probe of starting working is taken out a vacuum to whole device pipeline makes its stirring apparatus 6 be in vacuum state.Make its degreasing keep each line clear degree.
3. automatically control is opened admission gear 9 and control electromagnetic valve 4 earlier with it, gas transmission 5ml to stirring apparatus 6 in, after open oil-feed device 10 and control electromagnetic valve 5, import oil mass 10ml to stirring apparatus 6; Open the Based Intelligent Control heating arrangement on the stirring apparatus 6, to stirring apparatus 6 heating, thereby gas-oil separation is fast, and the degassing is just fast; Opening stirring motor 7 simultaneously rotates its drive stirrer 12 that runs up; Continued to open admission gear 9 and control electromagnetic valve 4 in 3-5 minute then to stirring apparatus 6 input 5ml carrier gas; Open oil-feed device 10 and control electromagnetic valve 5 again, to stirring apparatus 6 input oil mass 10ml, stirring motor 7 is rotated further and drives stirrer 12 continuation stirrings; Repeat above-mentioned action, gas is deviate from continuous 4 stirrings.
4. the filtration unit 13 that is sent to of deviating from that gas do not stopped cools off once more and its mist of oil is trapped in be unlikely to pollute chromatographic column in the filtration unit 13.
5. judgement degassing volume device 19 is judged the volume of deviating from gas; That is: open the control electromagnetic valve 14 that connects pressure transducer 16 inlet ends, the control electromagnetic valve 15 that connects the sealed end of pressure transducer 16, judge the volume of deviating from gas, calculate gas volume through software systems through pressure transducer 16.
6. open gas that control electromagnetic valve 17 will deviate from and deliver to and collect gas device 18, close the Based Intelligent Control heating arrangement on the constant temperature oven 1, the Based Intelligent Control heating arrangement on the stirring apparatus 6 this moment, and temperature control is stopped.The operation of whole stirring, the degassing, analytical gas, collection gas finishes.
7. can outgas according to the present invention, carry out the online degassing next time successively.
So the present invention can accomplish automatically and vacuumize, air inlet, oil-feed, heating, stirring, analytical gas, collection gas, guarantee experiment stability, avoid experimental error, improved operating rate.The present invention is simple in structure, and is easy to operate.
Claims (6)
1. new automatic vacuum stirring degasser, characteristic is: comprising: constant temperature oven, stirring apparatus, Based Intelligent Control heating arrangement, vacuum extractor, admission gear, oil-feed device, filtration unit, judgement degassing volume device, collection gas device, control electromagnetic valve; Vacuum extractor connects the stirring vessel top of stirring apparatus; Admission gear connects the stirring vessel bottom of stirring apparatus, and the oil-feed device connects the stirring vessel bottom of stirring apparatus, and the inlet end of filtration unit connects the stirring vessel top of stirring apparatus; The inlet end of the outlet side connection judgment degassing volume device of filtration unit; The inlet end of judging degassing volume device is connected with pipeline with the other end, judges that the other end of degassing volume device connects control electromagnetic valve, and control electromagnetic valve connects collects gas device; The Based Intelligent Control heating arrangement is installed on the constant temperature oven, and the Based Intelligent Control heating arrangement also is installed on the stirring apparatus.
2. new automatic vacuum stirring degasser according to claim 1 is characterized in that: judge that degassing volume device comprises: the control electromagnetic valve of the sealed end of pressure transducer, the control electromagnetic valve that connects the pressure transducer inlet end, connection pressure transducer.
3. new automatic vacuum stirring degasser according to claim 1, it is characterized in that: stirring apparatus comprises sealed stirrer ware, stirring motor, stirrer, and stirrer is arranged on and stirs in the vessel, and stirring motor is connected with stirrer.
4. new automatic vacuum stirring degasser according to claim 1, it is characterized in that: the Based Intelligent Control heating arrangement comprises heating rod, temperature sensor probe, temperature control panel.
5. new automatic vacuum stirring degasser according to claim 1, it is characterized in that: vacuum extractor comprises vacuum pump, control electromagnetic valve; Vacuum pump is connected with control electromagnetic valve.
6. new automatic vacuum stirring degasser according to claim 1 is characterized in that: admission gear is connected with the stirring vessel bottom of stirring apparatus through control electromagnetic valve; The oil-feed device is connected with the stirring vessel bottom of stirring apparatus through control electromagnetic valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101478825A CN102680611A (en) | 2012-05-13 | 2012-05-13 | Novel fully-automatic vacuum mixing and degassing device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101478825A CN102680611A (en) | 2012-05-13 | 2012-05-13 | Novel fully-automatic vacuum mixing and degassing device |
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| CN102680611A true CN102680611A (en) | 2012-09-19 |
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| CN2012101478825A Pending CN102680611A (en) | 2012-05-13 | 2012-05-13 | Novel fully-automatic vacuum mixing and degassing device |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105223297A (en) * | 2015-11-20 | 2016-01-06 | 江苏有能电力自动化有限公司 | The degasser that a kind of novel transformer oil chromatography on-Line Monitor Device is special |
| CN115201388A (en) * | 2022-08-01 | 2022-10-18 | 哈尔滨理工大学 | Intelligent sampling analysis system and sampling analysis method for methanol in transformer oil |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101650353A (en) * | 2009-09-01 | 2010-02-17 | 福建省福州电业局 | Desaeration process of full desaeration system of chromatogram high-performance total analysis on-line monitoring device and desaeration system |
| CN201425590Y (en) * | 2009-06-05 | 2010-03-17 | 许坤 | Vacuum degassing device for insulating oil on-line chromatographic analysis |
| CN102125772A (en) * | 2010-12-30 | 2011-07-20 | 天津开发区利达科技发展有限公司 | Degasser |
| CN102198340A (en) * | 2011-04-08 | 2011-09-28 | 胡志敏 | Electronic-magnetic-stirring-based oil-gas separation device |
| CN202757945U (en) * | 2012-05-13 | 2013-02-27 | 江苏有能电力自动化有限公司 | Novel full-automatic vacuum mixing degasser |
-
2012
- 2012-05-13 CN CN2012101478825A patent/CN102680611A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201425590Y (en) * | 2009-06-05 | 2010-03-17 | 许坤 | Vacuum degassing device for insulating oil on-line chromatographic analysis |
| CN101650353A (en) * | 2009-09-01 | 2010-02-17 | 福建省福州电业局 | Desaeration process of full desaeration system of chromatogram high-performance total analysis on-line monitoring device and desaeration system |
| CN102125772A (en) * | 2010-12-30 | 2011-07-20 | 天津开发区利达科技发展有限公司 | Degasser |
| CN102198340A (en) * | 2011-04-08 | 2011-09-28 | 胡志敏 | Electronic-magnetic-stirring-based oil-gas separation device |
| CN202757945U (en) * | 2012-05-13 | 2013-02-27 | 江苏有能电力自动化有限公司 | Novel full-automatic vacuum mixing degasser |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105223297A (en) * | 2015-11-20 | 2016-01-06 | 江苏有能电力自动化有限公司 | The degasser that a kind of novel transformer oil chromatography on-Line Monitor Device is special |
| CN105223297B (en) * | 2015-11-20 | 2017-07-18 | 江苏有能电力自动化有限公司 | A kind of special degasser of novel transformer oil chromatography on-Line Monitor Device |
| CN115201388A (en) * | 2022-08-01 | 2022-10-18 | 哈尔滨理工大学 | Intelligent sampling analysis system and sampling analysis method for methanol in transformer oil |
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Application publication date: 20120919 |