CN102626668A - Efficient magnetic separation method for quartz sand - Google Patents
Efficient magnetic separation method for quartz sand Download PDFInfo
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- CN102626668A CN102626668A CN2012101138109A CN201210113810A CN102626668A CN 102626668 A CN102626668 A CN 102626668A CN 2012101138109 A CN2012101138109 A CN 2012101138109A CN 201210113810 A CN201210113810 A CN 201210113810A CN 102626668 A CN102626668 A CN 102626668A
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Abstract
The invention discloses a zero-emission and environmentally-friendly efficient purification method for quartz sand. In the method, two-section smashing (rough smashing and fine smashing) and ore milling with a rod mill are adopted, so that the production capacity is increased greatly, unit energy consumption is lowered, and the method is suitable for large-scale production. A method for removing weakly-magnetic minerals and intergrowth quartz with high iron content from quartz sand through advanced ore washing and weakly magnetic-high gradient strongly magnetic combined magnetic separation before ore milling is adopted, so that the purity of quartz sand is increased greatly. The method has the advantages of simple process flow, easiness for operating, low cost, high purification efficiency, stable performance and environmental friendliness of a produced product, no use of any chemical substance in an entire production process, no production of any waste water, waste residues and waste gas, true realization of zero emission, no production of waste and prevention of pollution. The method is not limited by the production scale, various quartz sand products of low, medium and high grades can be produced, the enterprise profit can be maximized, and the method has a wide application prospect on the aspect of purification of quartz sand.
Description
Technical field
The present invention relates to the method for purification of quartz sand, especially relate to a kind of efficient magnetic selection method of quartz sand.
Background technology
Quartz sand is irreplaceable basic material in national strategy property and the pillar industry development, is widely used in high-tech sectors such as glass, photovoltaic, photoelectricity and space flight.Along with developing rapidly of these fields, the demand of quartz sand is increased day by day, and good quartz mine resource is day by day exhausted along with the continuous exploitation in age.How common quartz sand resources is fully utilized through purification, just seem most important.
The tradition method of purification mainly is to realize through methods such as flotation, acidleach, traditional magnetic separation.Acidleach and flotation all will be added chemical substance in process; These chemical substances not only exist the hidden danger of environmental protection aspect; And in the quartz sand product of producing because of residual the acid or alkaline medicament that is added, can cause influence in various degree to follow-up technology and equipment, and production process receives the influence of many factors such as temperature, concentration, pH value; Production operation is poor, and not looked at by the parent of enterprise.
The tradition method of purification also adopts the various strong bar magnet of quantity (surface electric field intensity is about 0.8 tesla) to be placed in the irrigation canals and ditches manual work mostly and cleans successively; Reach the purpose of deironing; So not only workman's workload is big, and receives numerous human factors such as cleaning frequency to influence bad control in the production.Drum magnetic separator because of magnetic force little and material can not with reasons such as drum surface fully contacts, de-ferrous effect is not good yet when producing this quartz-like sand.And no matter be strong bar magnet or drum magnetic separator along with the growth of service time, all can decay to some extent in magnetic field.
In addition, traditional method of purification is because of technology imperfection and equipment backwardness, and not only production is difficult to the formation scale, and aspect purification, also is difficult to obtain positive effect.
Summary of the invention
The object of the invention just provide a kind of purity that increases substantially quartz sand, zero-emission, no waste produce, pollution-free, production capacity is high, specific energy consumption is low, be suitable for the efficient magnetic selection method of large-scale production.
The objective of the invention is to realize like this:
A kind of efficient magnetic selection method of quartz sand, characteristic is:
1, fragmentation-washup: quartz mine is slightly broken to the bulk of 5cm * 5cm through jaw crusher; Get into the carefully broken fine ore to 1cm * 1cm of gyratory crusher; With belt fine ore is delivered on the vibratory sieve; And utilize water under high pressure that the fine ore on the vibratory sieve is washed, and remove the impurity components such as clay on fine ore surface, sieve material down obtains can be used as first byproduct of simple glass raw material through the desliming of a desliming bucket, after concentrated: quartzy general sand; The overflow of a desliming bucket gets into thickening pond;
2, ore grinding-first classification: the fine ore that will wash is sent into rod mill earlier and is carried out wet milling, the ore pulp of wearing into, and getting into screen cloth is that 20 purpose cylinder roller screens carry out first classification, the material on the sieve is delivered to rod mill with belt and regrinds;
3, desliming: the ore pulp under the cylinder rotary screen gets into No. two desliming buckets, screens out mud and mica group light weight sundries in the ore pulp, and the overflow of No. two desliming buckets gets into thickening pond;
4, magnetic separation: the underflow breeze of desliming bucket is successively through cartridge type low intensity magnetic separation machine and upright ring pulsating high gradient intensity magnetic separator; The field intensity of cartridge type low intensity magnetic separation machine is 0.1~0.5 tesla; Main the background field intensity of upright ring pulsating high gradient intensity magnetic separator requires to reach 1 tesla with the mechanical iron that gets in the strongly magnetic mineral and the process that remove in the quartz sand, and medium adopts 1.5 mm rod medium; Feed ore concentration is controlled at 10~15%, with removing biotite, the Fe in the quartz sand
2O
3, TiO
2Deng weak magnetic mineral, the mine tailing that obtains behind low intensity magnetic separation and the high intensity magnetic separation is the magnetic thing, is second byproduct: non-burning brick raw sand can be used to do the non-burning brick construction material of Denging;
5, secondary classification: low intensity magnetic separation and high intensity magnetic separation mortar later carries out the secondary classification through hydraulic classifier, and the size through the sand removing hole valve of regulating the hydraulic classiciation motor spindle and the water that recoils realizes that the client is to the size fractionated product demand;
6, concentrated-dehydration: underflow mortar that obtains after the classification of hydraulic classifier secondary and overflow mortar are concentrated respectively and the high frequency shale shaker dehydration, and the underflow mortar obtains first major product and (contains SiO after concentrating, dewatering
2>=99.8%, Fe
2O
3≦ 0.007%, AL
2O
3≦ 0.2%): glass sand, the overflow mortar obtains second major product after concentrating, dewatering: quartzy washed ore, glass sand are applied to high sophisticated technology industries such as solar energy, optical-fibre communications, and quartzy washed ore is as the raw material of Ceramic glaze.
Mine tailing in the thickening pond is handled: the mine tailing that No. two desliming buckets obtain in mine tailing that desliming bucket obtains in fragmentation-washup flow process and the desliming flow process all is admitted to thickening pond; Concentrate through thickening pond earlier; Filter through filter, the filter residue that obtains is as the 3rd byproduct: cement raw material again.
The present invention adopts the method for washup in advance before two sections fragmentations, the ore grinding, the strong magnetic associating of weak magnetic-high gradient magnetic separation to come purifying quartz sand, compares with traditional method of purification, and the present invention has following characteristics:
1, the present invention adopts two sections fragmentations (thick broken, thin broken) and rod mill ore grinding, has overcome the shortcoming that traditional method of purification has only thick broken one broken process, makes production capacity improve greatly, and specific energy consumption reduces, and is suitable for large-scale production.
2, on magnetic plant, except adopting cartridge type low intensity magnetic separation machine, also adopted upright ring pulsating high gradient intensity magnetic separator; Not only magnetic field intensity is big for upright ring pulsating high gradient intensity magnetic separator; Gradient is high, and key is to have disposed pulsing mechanism, and pulsing mechanism can carry out repeated screening with weak magnetic mineral in the quartz sand and the high intergrowth quartz of iron-holder; Remove to the full extent, thereby improved the purity of quartz sand.
3, the present invention has carried out reasonable processing to mine tailing, has not only practiced thrift water, and the filter residue that obtains is used as cement raw material as the 3rd byproduct, has opened up a product for enterprise's pilosity, has really accomplished zero-emission, and no waste produces, and is pollution-free; And traditional method of purification is little because of production scale, and mine tailing is not generally handled, and can pollute selecting factory and surrounding enviroment.
4, technological process of the present invention is simple, easy to operate, cost is low, purification efficiency is high, and the properties of product of being produced are stable, production environment is friendly, do not use any chemical substance in the whole process of production, also do not produce any waste water, waste residue and waste gas.
The present invention is not limited by production scale, the multiple quartz sand product such as multiple basic, normal, high that can produce, thereby can enterprise profit be maximized, having a wide range of applications aspect the purification of quartz sand.
The contrast such as the following table of the major product production target in the present invention and traditional method of purification quartz sand factory when test in Fengyang, Anhui.Visible from table, produce quartz sand with the present invention and compare with traditional method of purification, (refer to the useful component SiO in the raw ore although the original quality of raw ore is lower
2Content lower, impurity content is high), but the quartz sand concentrate quality that is obtained increases substantially SiO
2Content is promoted to 99.8% by 99.1%, objectionable impurities Fe
2O
3Reduce to 0.0063% by 0.015%, the deironing rate improves 20.73 percentage points, reaches the requirement of high most advanced and sophisticated raw materials such as solar energy, optical-fibre communications.
The specific embodiment
Below in conjunction with embodiment the present invention is done further explain.
A kind of quartz sand process for effectively purifying of Zero-discharge non-pollution, concrete steps are following:
1, fragmentation-washup: quartz mine is slightly broken to the bulk of 5cm * 5cm through jaw crusher; Get into the carefully broken fine ore to 1cm * 1cm of gyratory crusher; With belt fine ore is delivered on the vibratory sieve; And utilize water under high pressure that the fine ore on the vibratory sieve is washed, and remove the impurity components such as clay on fine ore surface, sieve material down obtains can be used as first byproduct of simple glass raw material through the desliming of a desliming bucket, after concentrated: quartzy general sand; The overflow of a desliming bucket gets into thickening pond;
2, ore grinding-first classification: the fine ore that will wash is sent into rod mill earlier and is carried out ore grinding, the ore pulp of wearing into, and getting into screen cloth is that 20 purpose cylinder roller screens carry out first classification, the material on the cylinder roller screen is delivered to rod mill with belt and regrinds;
3, desliming: the ore pulp under the cylinder rotary screen gets into No. two desliming buckets, screens out mud and mica group light weight sundries in the ore pulp, and the overflow of No. two desliming buckets gets into thickening pond;
4, magnetic separation: the underflow breeze of desliming bucket is successively through cartridge type low intensity magnetic separation machine and upright ring pulsating high gradient intensity magnetic separator; The field intensity of cartridge type low intensity magnetic separation machine is 0.1~0.5 tesla; Main the background field intensity of upright ring pulsating high gradient intensity magnetic separator requires to reach 1 tesla with the mechanical iron that gets in the strongly magnetic mineral and the process that remove in the quartz sand, and medium adopts 1.5 mm rod medium; Feed ore concentration is controlled at 10~15%, with removing biotite, the Fe in the quartz sand
2O
3, TiO
2Deng weak magnetic mineral, the mine tailing that obtains behind low intensity magnetic separation and the high intensity magnetic separation is the magnetic thing, is second byproduct: non-burning brick raw sand can be used to do the non-burning brick construction material of Denging;
5, secondary classification: low intensity magnetic separation and high intensity magnetic separation mortar later carries out the secondary classification through hydraulic classifier, and the size through the sand removing hole valve of regulating the hydraulic classiciation motor spindle and the water that recoils realizes that the client is to the size fractionated product demand;
6, concentrated-dehydration: underflow mortar that obtains after the classification of hydraulic classifier secondary and overflow mortar are concentrated respectively and the high frequency shale shaker dehydration, and the underflow mortar obtains first major product and (contains SiO after concentrating, dewatering
2>=99.8%, Fe
2O
3≦ 0.007%, AL
2O
3≦ 0.2%): glass sand, the overflow mortar obtains second major product after concentrating, dewatering: quartzy washed ore, glass sand are applied to high sophisticated technology industries such as solar energy, optical-fibre communications, and quartzy washed ore is as the raw material of Ceramic glaze.
Mine tailing in the thickening pond is handled: the mine tailing that No. two desliming buckets obtain in mine tailing that desliming bucket obtains in fragmentation-washup flow process and the desliming flow process all is admitted to thickening pond; Concentrate through thickening pond earlier; Filter through filter, the filter residue that obtains is as the 3rd byproduct: cement raw material again.
Claims (2)
1. the quartz sand process for effectively purifying of a Zero-discharge non-pollution is characterized in that:
(1), fragmentation-washup: quartz mine is slightly broken to the bulk of 5cm * 5cm through jaw crusher; Get into the carefully broken fine ore to 1cm * 1cm of gyratory crusher; With belt fine ore is delivered on the vibratory sieve; And utilize water under high pressure that the fine ore on the vibratory sieve is washed, and remove the impurity components such as clay on fine ore surface, sieve material down obtains can be used as first byproduct of simple glass raw material through the desliming of a desliming bucket, after concentrated: quartzy general sand; The overflow of a desliming bucket gets into thickening pond;
(2), ore grinding-first classification: the fine ore that will wash is sent into rod mill earlier and is carried out wet milling, and getting into screen cloth is that 20 purpose cylinder roller screens carry out first classification, and the material on the sieve is delivered to rod mill with belt and regrinds;
(3), desliming: the ore pulp under the cylinder rotary screen gets into No. two desliming buckets, screens out mud and mica group light weight sundries in the ore pulp, and the overflow of No. two desliming buckets gets into thickening pond;
(4), magnetic separation: the underflow breeze of desliming bucket is successively through cartridge type low intensity magnetic separation machine and upright ring pulsating high gradient intensity magnetic separator; The field intensity of cartridge type low intensity magnetic separation machine is 0.1~0.5 tesla; The background field intensity of upright ring pulsating high gradient intensity magnetic separator requires to reach 1 tesla, and medium adopts 1.5 mm rod medium, and feed ore concentration is controlled at 10~15%; The mine tailing that obtains behind low intensity magnetic separation and the high intensity magnetic separation is the magnetic thing, is second byproduct: non-burning brick raw sand;
(5), secondary classification: low intensity magnetic separation and high intensity magnetic separation mortar later carries out the secondary classification through hydraulic classifier, and the size through the sand removing hole valve of regulating the hydraulic classiciation motor spindle and the water that recoils realizes that the client is to the size fractionated product demand;
(6), concentrated-dehydration: underflow mortar that obtains after the classification of hydraulic classifier secondary and overflow mortar are concentrated respectively and the high frequency shale shaker dehydration, and the underflow mortar obtains containing SiO after concentrating, dewatering
2>=99.8%, Fe
2O
3≦ 0.007%, AL
2O
3≦ 0.2% first major product: glass sand, overflow mortar obtain second major product after concentrating, dewatering: quartzy washed ore.
2. quartz sand process for effectively purifying according to claim 1; It is characterized in that: mine tailing in the thickening pond is handled: the mine tailing that No. two desliming buckets obtain in mine tailing that desliming bucket obtains in fragmentation-washup flow process and the desliming flow process all is admitted to thickening pond; Concentrate through thickening pond earlier; Filter through filter, the filter residue that obtains is as the 3rd byproduct: cement raw material again.
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