CN102620451B - Method for producing heat pipe type full-glass-vacuum tube through boiling exhaust technology - Google Patents

Method for producing heat pipe type full-glass-vacuum tube through boiling exhaust technology Download PDF

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CN102620451B
CN102620451B CN2012100889562A CN201210088956A CN102620451B CN 102620451 B CN102620451 B CN 102620451B CN 2012100889562 A CN2012100889562 A CN 2012100889562A CN 201210088956 A CN201210088956 A CN 201210088956A CN 102620451 B CN102620451 B CN 102620451B
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glass
inner tube
glass inner
tube
working medium
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CN102620451A (en
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许新中
程翠英
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Yinghao Yangguang Beijing Energy Saving Technology Service Co ltd
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BEIJING TIANPU SOLAR ENERGY INDUSTRY Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00Energy generation through renewable energy sources
    • Y02E10/40Solar thermal energy, e.g. solar towers
    • Y02E10/44Heat exchange systems

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Abstract

The invention discloses a method for producing a heat pipe type full-glass-vacuum tube through a boiling exhaust technology, which comprises the following steps that: a glass tube is cut into sections, and a plurality of sections of glass tubes are cleaned, then welded and processed into glass inner tubes of which one ends are sealed and the other ends are provided with filling liquid seal ports;after working media are filled into the glass inner tubes, preheated and boiled to exhaust, air in the glass inner tubes is discharged from the filling liquid seal ports; when the residual working media in the tubes reach the design index, the filling liquid seal ports are sealed; and the qualified glass inner tubes after inspection are encapsulated with glass outer tubes, vacuumized, finally sealed, baked and pinned. The full-glass-vacuum tube which is produced by the method for producing the heat pipe type full-glass-vacuum tube through the boiling exhaust technology has good reliability and safety, so the product quality is improved; and meanwhile, the production cost is also reduced, and the production efficiency is improved.

Description

A kind of method of boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe
Technical field
The present invention relates to the solar energy utilization technique field, especially a kind of boiling and exhaust technology prepares the method for heat pipe type full-glass vacuum pipe.
Background technology
According to the operation principle of all-glass vacuum tube, vacuum tube can be divided into from top to bottom can be divided into evaporator section, condensation segment successively.At present, Chang Yong heat pipe type full-glass vacuum pipe has two kinds of structures:
A kind of is at common all-glass vacuum tube inner tube mouth place's welding condenser pipe, only need get final product by secondary welding vacuum tube on common all-glass vacuum tube, and processing is simple.In case but welding is defective, will cause scrapping of whole vacuum tube.And near the selective coating the vacuum tube welding port is damaged easily; The inwall out-of-flatness at welding end seam place, thus the backflow of working medium in the all-glass vacuum tube influenced.
Another kind of structure is that condensation segment and evaporator section are one, as shown in Figure 1.This structure has multiple processing technology: the one, and the interior pipe of the vacuum tube that inner and outer pipes sealing-in is good vacuumizes, and when vacuum reaches specification requirement, manages the quantitative working medium of can again in vacuum tube, last sealing-in.The one,, and then vacuumize sealing-in when the vacuum plating reaches specification requirement at first to the quantitative working medium of interior pipe can of the vacuum tube that sealing-in is good.Though, can overcome condenser pipe and the common irregular defective of all-glass vacuum tube weld, its processing technology still can not realize the higher vacuum of pipe in the vacuum tube, solves the technical problem of glass tube walls and working medium on-condensible gas discharging.And its processing technology has been introduced new technical problem again: the former needs accurate working medium filling apparatus, and is very strict to the sealing requirements of the filling weight valve of working medium, the equipment investment height, and product cost is higher; And production efficiency is lower.The product vacuum that the latter produces does not reach specification requirement, and the product hot property is lower, and production efficiency is low.Simultaneously, when vacuumizing, vavuum pump is intake easily, has increased the maintenance of equipment.
Summary of the invention
For the existing production technology production cost height that solves the heat pipe type full-glass vacuum pipe, the product hot property is lower, production efficiency is low, problems such as equipment investment is big, the invention provides the method that a kind of boiling and exhaust technology prepares the heat pipe type full-glass vacuum pipe, to remedy above-mentioned weak point, thereby improve the quality of products, reduce production costs, minimizing equipment drops into, and being conducive to energy-saving and emission-reduction is the industrialization production proposition feasibility embodiment of heat pipe type full-glass vacuum pipe.
In order to solve the problems of the technologies described above, the invention provides a kind of method of boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe, may further comprise the steps:
(a) blanking and cleaning: glass tube is cut into pieces, and cleans up;
(b) welding processing: clean glass tube is made end sealing, and an end is provided with the glass inner tube of irritating the fluid-tight interface, at the intersection welding glass ring of evaporator section and condensation segment;
(c) can working medium: the glass inner tube setting is emitted on the transfer station, and the working medium injector that is positioned at the transfer station top is injected into each glass inner tube with working medium respectively by irritating the fluid-tight interface;
(d) preheating: glass inner tube is sent into the exhaust station preheating;
(e) boiling and exhaust: the glass inner tube of preheating is sent to exhaust station below jet-burner the working medium in the glass inner tube is heated to boiling, the steam of working medium is taken over a mouthful discharge with the air in the glass inner tube from irritating fluid-tight;
(f) seal: after the amount of remaining working medium in the glass inner tube reached production standard, the fluid-tight interface was irritated in sealing-in;
(g) check: detect glass inner tube, qualified glass inner tube enters step (h) and continues processing;
(h) encapsulation: clean the glass inner tube outer wall, outer wall to glass inner tube passes through the magnetron sputtering selective coating, the glass outer tube of in vacuum glass, packing into after the pipe assembling getter, pipe and vacuum glass outer tube in the vacuum glass are passed through the glass ring welding, and vacuumize last sealing-in, roasting pin between the tube wall with glass inner tube and glass outer tube.
Preferably, the specification of the glass tube described in the described step (a) is Φ 47mm * 1.6~2.0mm or Φ 37mm * 1.6~2.0mm, and the length of cutting is 1800mm~2000mm.
Preferably, the working medium of injecting glass inner tube in the described step (c) is water, 0~30% aqueous solution of propylene glycol or 0~20% inorganic acid, saline solution, and described inorganic acid, saline solution are the aqueous solution or the aqueous solution of potassium bichromate, potassium sulfate, ammonium sulfate and ammonium phosphate or the aqueous solution of potassium bichromate, potassium sulfate, sulfuric acid, phosphoric acid, ammonium sulfate and ammonium phosphate of potassium bichromate, potassium sulfate, sulfuric acid and phosphoric acid.
Preferably, the glass tube that is placed in the described step (c) on the transfer station is 10 * N root, and per 10 is one group, and N is positive integer.
Preferably, the amount of the working medium of can is 1 ‰ of glass inner tube capacity~2 ‰ in the described step (c).
Preferably, the working medium of can is 6~12g in the described step (c).
Preferably, the working medium of injecting glass inner tube in the described step (c) is water, and the temperature of described step (d) preheating is 90~105 ℃.
Preferably, when residue working medium was 3~6g in the described step (f), the fluid-tight interface was irritated in sealing-in.
Preferably, in the described step (f) with the filling fluid-tight interface of glass inner tube by flame sealing.
The present invention adopts the production method of boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe and the difference of existing production method to be mainly following 4 aspects:
1, in the method for boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe provided by the invention, the processing of described glass inner tube is independently to finish, and after check, has only qualified glass inner tube just to enter next process.And be when finishing the inner and outer pipes welding of glass-vacuum tube in the prior art, pipe end welding condenser pipe is made heat pipe.Whether qualified the key technical indexes is: the sealing of glass inner tube and the amount of interior intraductal working medium and weigh all-glass vacuum tube, so prior art is had relatively high expectations to production equipment, production has high input, and production method provided by the present invention does not have extra high requirement to the working medium filling apparatus, so investment in production equipment is low, reduced production cost indirectly.
2, the present invention and the existing core that goes up the difference of product method are that exhaust process is to adopt boiling and exhaust technology, are about to working medium and are heated to boiling, and the working medium vaporized gas can be discharged the on-condensible gas that evaporates in the gas in the glass tube and the working medium.After the glass inner tube sealing-in, the steam of coagulable working medium is condensed into liquid state again, makes glass inner tube have higher vacuum.
3, in the production method that the present invention adopts, temperature is higher than the serviceability temperature of glass heat pipe during owing to vacuum exhaust, does not go wrong in process of production, and this product does not just have glass tube explosion problem when using.Improved reliability and the security of product when hot operation greatly.
4, evaporator section, the condensation segment of the interior pipe of the all-glass vacuum tube produced of method of the present invention are one, thereby have avoided weld inwall out-of-flatness in the two-part structure and influence the problem that working medium refluxes.
In addition, the production method that the present invention adopts is applicable to mobile automatic production line, also is applicable to fixedly exhaust station equipment.Every all-glass vacuum tube vacuumizing and exhausting approximately needs 10min in the existing production technology, and every all-glass vacuum tube boiling and exhaust only needs about 1min in the production method of the present invention, and its production efficiency is higher than existing production method far away.
In sum, reliability and the security of the all-glass vacuum tube that the method for boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe provided by the present invention is produced are good, have improved product quality; Simultaneously, also reduce production cost, improved production efficiency.
Description of drawings
Fig. 1 is described heat pipe type full-glass vacuum duct ligation composition.
Fig. 2 is the process chart of the method for boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe of the present invention.
Fig. 3 is the state diagram of described glass inner tube can working medium.
Fig. 4 is the state diagram of described glass inner tube boiling and exhaust.
Description of reference numerals is as follows:
1-working medium, the 2-evaporator section, the 3-condensation segment, the 4-getter, 5-glass outer tube, the 6-glass inner tube, the 7-selective coating, the 8-vacuum layer, the 9-glass ring, 11-irritates fluid-tight interface, 12-working medium injector, 13-exhaust station, 14-flame.
The specific embodiment
The present invention is further illustrated below in conjunction with accompanying drawing and specific embodiment, but protection scope of the present invention is not limited to this.
As shown in Figure 2, the method for boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe of the present invention may further comprise the steps:
(a) blanking and cleaning: glass tube is cut into pieces, and cleans up.
(b) welding processing: clean glass tube is made end sealing, and an end is provided with the glass inner tube 6 of irritating fluid-tight interface 11, at the intersection welding glass ring 9 of evaporator section 2 and condensation segment 3.
(c) can working medium 1: glass inner tube 6 settings are emitted on the transfer station, and the working medium injector 12 that is positioned at the transfer station top is injected into each glass inner tube 6 with working medium 1 respectively by irritating fluid-tight interface 11.
Further, in this step in the glass inner tube 6 working medium 1 of institutes' can be for water, mass concentration less than 30% aqueous solution of propylene glycol or mass concentration less than 20% inorganic acid, saline solution, described inorganic acid, saline solution are the aqueous solution or the aqueous solution of potassium bichromate, potassium sulfate, ammonium sulfate and ammonium phosphate or the aqueous solution of potassium bichromate, potassium sulfate, sulfuric acid, phosphoric acid, ammonium sulfate and ammonium phosphate of potassium bichromate, potassium sulfate, sulfuric acid and phosphoric acid.The amount of the working medium 1 of institute's can is 1 ‰~2 ‰ of glass inner tube 6 capacity, is 2~3 times of the amount of the working medium 1 of production standard.
(d) preheating: glass inner tube 6 is sent into exhaust station 13 preheatings, as shown in Figure 4.
(e) boiling and exhaust: the glass inner tube 6 of preheating is sent to exhaust station 13 below jet-burners the working medium 1 in the glass inner tube 6 are heated to boiling, the steam of working medium 1 is taken over a mouthful discharge with the air in the glass tube from irritating fluid-tight;
(f) seal: after the amount of remaining working medium 1 in the glass inner tube 6 reached production standard, fluid-tight interface 11 was irritated in sealing-in;
(g) check: detect glass inner tube 6, qualified glass inner tube 6 enters step (h) and continues processing;
(h) encapsulation: the outer wall that cleans glass inner tube 6, outer wall to glass inner tube 6 passes through magnetron sputtering spraying plating selective coating 7, the pipe 6 assemblings glass outer tube 5 of packing into after the getters 4 in vacuum glass, pipe 6 and vacuum glass outer tube in the vacuum glass are passed through glass ring 9 weldings, and will vacuumize last sealing-in, roasting pin between glass inner tube 6 and glass outer tube 5 tube walls.
Exhaust air technique of the present invention carries out at heated condition, and glass inner tube 6 vacuums guarantee that easily the on-condensible gas in the glass inner tube 6 is discharged easily.The hot property of the glass heat pipe of making is better, and service life is longer.And the production method that the present invention adopts is applicable to mobile automatic production line, also is applicable to fixedly exhaust station 13 equipments.Every all-glass vacuum tube vacuumizing and exhausting approximately needs 10min in the existing production technology, and every all-glass vacuum tube boiling and exhaust only needs about 1min in the production method of the present invention, and its production efficiency is higher than existing production method far away.
In concrete operating process, consider the specification of existing solar water heater, be the glass tube of Φ 47mm * 1.6~2.0mm or Φ 37mm * 1.6~2.0mm with specification, after cleaning, the length that cuts into is the glass tube of 1800mm~2000mm.The clean glass tube of well cutting carries out welding processing then, makes end sealing, and an end is provided with the glass inner tube 6 of irritating fluid-tight interface 11, at the intersection welding glass ring 9 of evaporator section 2 and condensation segment 3.In order to enhance productivity, be convenient to management, 6 settings of 10 * N root glass inner tube are placed on the transfer station, per 10 is one group, as shown in Figure 3.Working medium 1 injector that is positioned at the transfer station top is injected into each glass inner tube 6 with 6~12 gram working medium 1 respectively from irritating fluid-tight interface 11.
Then, there is the glass inner tube 6 of working medium 1 to carry out preheating and boiling and exhaust processing to filling.At first glass inner tube 6 is served exhaust station 13, carry out preheating, the temperature of preheating should be near the boiling point of the working medium 1 of institute's can, and when the working medium 1 of institute's can was water, the temperature of preheating this moment should be above 105 ℃.After the preheating glass inner tube 6 is sent to exhaust station 13 below jet-burners the working medium 1 in the glass inner tube 6 is heated to boiling, the steam of working medium 1 is taken over a mouthful discharge with the air in the glass tube from irritating fluid-tight; Working medium 1 remaining in glass inner tube 6 reaches design objective, and when being 3~6g, fluid-tight interface 11 is irritated in flame sealing.
Detect the amount of the working medium 1 in the glass inner tube 6 and the hot property of glass inner tube 6, the qualified product that will meet production standard flows into next process, and glass inner tube 6 and glass outer tube 5 are encapsulated.Before encapsulation, at first clean glass inner tube 6 outer walls, to the outer wall of glass inner tube 6 by magnetron sputtering selective coating 7.Then, the pipe 6 assemblings glass outer tube of packing into after the getters 4 in vacuum glass.At last, glass inner tube 6 and glass outer tube 5 are passed through glass ring 9 weldings, and will vacuumize between glass inner tube 6 and glass outer tube 5 tube walls, last sealing-in, roasting pin.
The above specific embodiment only is indivedual embodiment of the present invention, the present invention is not limited to above-mentioned embodiment, under the situation that does not deviate from flesh and blood of the present invention, any distortion that it may occur to persons skilled in the art that, improvement, replacement all fall into scope of the present invention.

Claims (9)

1. the method for a boiling and exhaust explained hereafter heat pipe type full-glass vacuum pipe is characterized in that, may further comprise the steps:
(a) blanking and cleaning: glass tube is cut into pieces, and cleans up;
(b) welding processing: clean glass tube is made end sealing, and an end is provided with the glass inner tube (6) of irritating fluid-tight interface (11), at the intersection welding glass ring (9) of evaporator section (2) and condensation segment (3);
(c) can working medium (1): glass inner tube (6) setting is emitted on the transfer station, working medium (1) is injected into respectively in each glass inner tube (6) by irritating fluid-tight interface (11);
(d) preheating: glass inner tube (6) is sent into exhaust station (13) preheating;
(e) boiling and exhaust: the glass inner tube (6) of preheating is sent to exhaust station (13) below jet-burner, working medium (1) in the glass inner tube (6) is heated to boiling, and the steam of working medium (1) is discharged the air in the glass inner tube (6) from irritating fluid-tight interface (11);
(f) seal: after the amount of remaining working medium (1) in the pipe reached production standard, fluid-tight interface (11) was irritated in sealing-in;
(g) check: detect glass inner tube (6), qualified glass inner tube (6) enters step (h) and continues processing;
(h) encapsulation: clean glass inner tube (6) outer wall, outer wall to glass inner tube (6) passes through magnetron sputtering selective coating (7), the glass outer tube (5) of after glass inner tube (6) assembling getter (4), packing into, glass inner tube (6) and glass outer tube (5) are passed through glass ring (9) welding, and will vacuumize last sealing-in, roasting pin between glass inner tube (6) and glass outer tube (5) tube wall.
2. production method according to claim 1 is characterized in that, the specification of the glass tube described in the described step (a) is Φ 47mm * 1.6~2.0mm or Φ 37mm * 1.6~2.0mm, and the length of cutting is 1800mm~2000mm.
3. production method according to claim 1, it is characterized in that, the working medium (1) of injecting glass inner tube (6) in the described step (c) is water, mass concentration less than 30% aqueous solution of propylene glycol or mass concentration less than 20% inorganic acid, saline solution, and described inorganic acid, saline solution are the aqueous solution or the aqueous solution of potassium bichromate, potassium sulfate, ammonium sulfate and ammonium phosphate or the aqueous solution of potassium bichromate, potassium sulfate, sulfuric acid, phosphoric acid, ammonium sulfate and ammonium phosphate of potassium bichromate, potassium sulfate, sulfuric acid and phosphoric acid.
4. production method according to claim 2 is characterized in that, the glass tube that is placed in the described step (c) on the transfer station is 10 * N root, and per 10 is one group, and N is positive integer.
5. production method according to claim 4 is characterized in that, the amount of the working medium (1) of can is 1 ‰~2 ‰ of glass inner tube (6) capacity in the described step (c).
6. production method according to claim 3 is characterized in that, the working medium (1) of can is 6~12g in the described step (c).
7. production method according to claim 5 is characterized in that, the working medium (1) of injecting glass inner tube (6) in the described step (c) is water, and the temperature of described step (d) preheating is 90~105 ℃.
8. production method according to claim 7 is characterized in that, when residue working medium (1) was 3~6g in the described step (f), fluid-tight interface (11) was irritated in sealing-in.
9. according to the described production method of each claim of claim 1-8, it is characterized in that, in the described step (f) with the filling fluid-tight interface (11) of glass inner tube (6) by flame sealing.
CN2012100889562A 2012-03-29 2012-03-29 Method for producing heat pipe type full-glass-vacuum tube through boiling exhaust technology Active CN102620451B (en)

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CN103090570B (en) * 2013-02-28 2014-08-06 北京金阳科创太阳能技术有限公司 Manufacturing method of heat-tube-type evacuated collector tube
CN106112420A (en) * 2016-07-21 2016-11-16 吴金成 A kind of copper tube production technology

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JPS5687742A (en) * 1979-12-19 1981-07-16 Sanyo Electric Co Ltd Heat pipe type solar heat collector
CN1021844C (en) * 1990-11-20 1993-08-18 北京市太阳能研究所 Method and equipment for thermal pipe vacuum tube air exhaust
CN202013029U (en) * 2010-11-25 2011-10-19 大连熵立得传热技术有限公司 Heat transfer device for heat pipe type solar heat collector

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Patentee after: YINGHAO YANGGUANG (BEIJING) ENERGY SAVING TECHNOLOGY SERVICE CO.,LTD.

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Patentee before: BEIJING TIANPU SOLAR ENERGY INDUSTRY Co.,Ltd.