CN102602912B - Synthesizing device for continuously producing carbon nano pipe with shape of crystal whisker - Google Patents
Synthesizing device for continuously producing carbon nano pipe with shape of crystal whisker Download PDFInfo
- Publication number
- CN102602912B CN102602912B CN2012100679371A CN201210067937A CN102602912B CN 102602912 B CN102602912 B CN 102602912B CN 2012100679371 A CN2012100679371 A CN 2012100679371A CN 201210067937 A CN201210067937 A CN 201210067937A CN 102602912 B CN102602912 B CN 102602912B
- Authority
- CN
- China
- Prior art keywords
- synthesizing
- valve
- bin
- furnace
- storehouse
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Crystals, And After-Treatments Of Crystals (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The invention relates to a synthesizing device for continuously producing a carbon nano pipe with a shape of a crystal whisker, which is characterized by comprising a spraying feeder, an upright synthesizing furnace, a heating device, an annular piston driven by hydraulic pressure, and valves; and the upper part of the upright synthesizing furnace is provided with a synthesizing bin, the middle of the upright synthesizing furnace is provided with a vacuum bin, the lower part of the upright synthesizing furnace is provided with a collecting bin, the atomizing feeder is installed on a cover plate at the top end of the synthesizing furnace, the cover plate is fixed at the top end of the synthesizing furnace, the heating device is installed along the outside of the position of the synthesizing bin of the upright synthesizing furnace, a first valve is installed between the synthesizing bin and the vacuum bin, a second valve is installed between the vacuum bin and the collecting bin, the vacuum bin is provided with an air exhaust hole, and the air exhaust hole is connected to a vacuum pump. The synthesizing device for the carbon nano pipe, which is disclosed by the invention, can be used for producing a very straight carbon nano pipe with the shape of a crystal whisker, so that the carbon nano pipe is easy to disperse. Therefore, a way is open for the industrialized application of the carbon nano pipe.
Description
Technical field
The invention belongs to the nano material synthesis technical field, relate to the synthesizer of carbon nanotube.
Background technology
Carbon nanotube is a kind of high performance nano material, has excellent mechanical property and electric property.In fields such as lithium ion battery, photoelectric functional material, Field Emission Display, electromagnetic shielding, absorbing material, high performance composite, be applied.But the carbon nanotube synthetic due to current carbon nanotube is very crooked, and mutually be wound around, make dispersing Nano carbon tubes become the major obstacle of application.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, a kind of synthesizer of continuous production crystal whisker-shaped carbon nanotube is provided.
Synthesizer of the present invention is comprised of spraying feeder (1), vertical synthetic furnace (3), heating unit (4), hydraulically powered annular piston (2), valve etc.
Vertically the top of synthetic furnace (3) is synthetic storehouse, centre is vacuum storehouse (8), bottom is collecting bin (7), atomization charger (1) is arranged on synthetic furnace top cover plate (10), cover plate (10) is fixed on synthetic furnace (3) top, heating unit (4) is along the vertically outside installation at the position, synthetic storehouse of synthetic furnace (3), the first valve (5) is arranged between synthetic storehouse and vacuum storehouse (8), the second valve (6) is arranged between vacuum storehouse (8) and collecting bin (7), and two valves are respectively by the hydro-cylinder opening and closing that carry.Vacuum storehouse (8) is provided with a venting hole (9), and venting hole (9) is connected to vacuum pump.It is descending that the hydraulic efficiency system that the synthetic carbon nanotube in synthetic storehouse is carried by annular piston (2) promotes annular piston (2), carbon nanotube pushed to vacuum storehouse (9), and then enter collecting bin (7).
Annular piston (2), the first valve (5) and the second valve (6) are connected respectively to the hydro-cylinder carried.
During work, five atomization chargers (1) of arranging in top spray into catalyzer and the hydrocarbon liquid that carbon source is provided in shaft furnace, after producing certain hour, produce carbon nanotube and push vacuum storehouse (8), bottom by annular piston (2), close the first storehouse valve (5), start to vacuumize, inflammable gas is discharged by venting hole (9), opens second valve (6) in vacuum storehouse (8), and then product introduction collecting bin (7), take out carbon nanotube, then valve-off (6).Annular piston (2) is promoted by the hydraulic efficiency system carried that it is descending and up, and the first valve (5) and the second valve (6) are respectively by the hydro-cylinder opening and closing that carry, but whole process service routine is controlled or manually controlled.
Apparatus for synthesizing carbon nanotubes of the present invention can be produced very straight crystal whisker-shaped carbon nanotube, makes the dispersion of carbon nanotube be easy to carry out, thereby is industrial applications carbon nanotube blaze the trail.
The accompanying drawing explanation
Fig. 1 is synthesizer schematic diagram of the present invention.Wherein 1 is atomization charger, and 2 is annular piston, and 3 is vertical synthetic furnace, and 4 is heating unit, and 5 is the first valve, and 6 is the second valve, and 7 is collecting bin, and 8 is the vacuum storehouse, and 9 is venting hole, and 10 is cover plate (spraying gun mounting plate).
Fig. 2 is synthesizer of the present invention top cover plate schematic diagram.Wherein 1 is atomization charger, and 10 is cover plate.
Fig. 3 is synthesizer annular piston vertical view of the present invention.
Embodiment
The present invention will be described further by following examples.
The top of the described vertical synthetic furnace 3 of the present embodiment is synthetic storehouse, centre is vacuum storehouse 8, bottom is collecting bin 7, atomization charger 1 is arranged on synthetic furnace top cover plate 10, cover plate 10 is fixed on vertical synthetic furnace 3 tops, and heating unit 4 is along the vertically outside installation at the position, synthetic storehouse of synthetic furnace 3, and the first valve 5 is arranged between synthetic storehouse and vacuum storehouse 8, the second valve 6 is arranged between vacuum storehouse 8 and collecting bin 7, and two valves are respectively by the hydro-cylinder opening and closing that carry.Vacuum storehouse 8 is provided with a venting hole 9, and venting hole 9 is connected to vacuum pump.It is descending that the hydraulic efficiency system that the synthetic carbon nanotube in synthetic storehouse is carried by annular piston 2 promotes annular piston 2, carbon nanotube pushed to vacuum storehouse 9, and then enter collecting bin 7.
With reference to Fig. 1.Heating unit 4 energisings are heated to assigned temperature (1200 ℃).By atomization charger 1, pass into nitrogen and discharge the interior air of vertical synthetic furnace 3, then change by atomization charger 1 and pass into nitrogen and hydrogen mixed gas, to import atomization charger 1 by pump of constant delivery type by the catalyzer than the row configuration and hydrocarbon liquid solution through atomization charger 1 simultaneously, under the effect of gas, after solution atomization, spray in synthetic storehouse.After continuing for some time, annular piston 2 moves downward carbon nanotube is pushed to vacuum storehouse 9, annular piston 2 returns, and the first valve 5 is closed, and starts the second cyclic production.The second valve 6 is in closing condition.Start to vacuumize, the interior gas in vacuum storehouse 9 is emptying by venting hole 9, and the second valve 6 is opened, and carbon nanotube falls into collecting bin 7.Then the second valve 6 is closed, and vacuumizes, and after vent gas, the first valve 5 is opened, and enters next discharging circulation.
Claims (2)
1. produce continuously the synthesizer of crystal whisker-shaped carbon nanotube, it is characterized in that being formed by spraying feeder (1), vertical synthetic furnace (3), heating unit (4), hydraulically powered annular piston (2), valve; Vertically the top of synthetic furnace (3) is synthetic storehouse, centre is vacuum storehouse (8), bottom is collecting bin (7), atomization charger (1) is arranged on synthetic furnace top cover plate (10), cover plate (10) is fixed on synthetic furnace (3) top, heating unit (4) is along the vertically outside installation at the position, synthetic storehouse of synthetic furnace (3), the first valve (5) is arranged between synthetic storehouse and vacuum storehouse (8), the second valve (6) is arranged between vacuum storehouse (8) and collecting bin (7), vacuum storehouse (8) is provided with a venting hole (9), and venting hole (9) is connected to vacuum pump.
2. synthesizer according to claim 1, is characterized in that annular piston (2), the first valve (5) and the second valve (6) are connected respectively to the hydro-cylinder carried.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100679371A CN102602912B (en) | 2012-03-15 | 2012-03-15 | Synthesizing device for continuously producing carbon nano pipe with shape of crystal whisker |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100679371A CN102602912B (en) | 2012-03-15 | 2012-03-15 | Synthesizing device for continuously producing carbon nano pipe with shape of crystal whisker |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102602912A CN102602912A (en) | 2012-07-25 |
| CN102602912B true CN102602912B (en) | 2013-12-04 |
Family
ID=46520784
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012100679371A Active CN102602912B (en) | 2012-03-15 | 2012-03-15 | Synthesizing device for continuously producing carbon nano pipe with shape of crystal whisker |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102602912B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE1027066B1 (en) * | 2019-06-21 | 2020-09-11 | Nanocarbon Co Ltd | System and method for the automatic production of carbon nanomaterial |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103011123B (en) * | 2012-08-24 | 2014-04-09 | 南昌大学 | Fully-automatic synthesis device for continuously producing whisker-shaped carbon nano tube |
| CN104045558A (en) * | 2013-03-15 | 2014-09-17 | 江苏天成生化制品有限公司 | Methyl acetoacetate production mass transfer process |
| CN103395774B (en) * | 2013-07-24 | 2015-05-27 | 中国石油大学(北京) | Reaction device and method for producing graphene or carbon nanotubes |
| CN103435026B (en) * | 2013-08-05 | 2015-08-12 | 南昌大学 | A kind of continuous synthesis carbon receives the device of material |
| KR102047370B1 (en) * | 2016-07-14 | 2019-11-22 | 주식회사 엘지화학 | Apparatus for drying and collecting carbon nanotube product and process for preparing carbon nanotubes |
| CN109758812B (en) * | 2019-03-22 | 2021-06-22 | 上海诺净环保科技有限公司 | Intelligent integrated sewage treatment equipment |
| CN112225178A (en) * | 2020-11-10 | 2021-01-15 | 内蒙古乌海化工有限公司 | Synthetic furnace door structure |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100732516B1 (en) * | 2005-12-16 | 2007-06-27 | 세메스 주식회사 | Apparatus and method for collection carbon nano tube |
| JP4811690B2 (en) * | 2007-07-06 | 2011-11-09 | 独立行政法人産業技術総合研究所 | Carbon nanotube film forming method and film forming apparatus |
| RU2010110470A (en) * | 2007-12-26 | 2012-02-10 | Никкисо Ко., Лтд. (Jp) | DEVICE FOR MANUFACTURE OF CARBON NANOTUBES OR CARBON NANO FIBERS AND DEVICE FOR THEIR ISOLATION |
| US9061909B2 (en) * | 2009-09-10 | 2015-06-23 | The University Of Tokyo | Method for simultaneously producing carbon nanotubes and hydrogen, and device for simultaneously producing carbon nanotubes and hydrogen |
| CN202519030U (en) * | 2012-03-15 | 2012-11-07 | 南昌大学 | Synthesizing device for continuously producing whisker-shaped carbon nano tube |
-
2012
- 2012-03-15 CN CN2012100679371A patent/CN102602912B/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE1027066B1 (en) * | 2019-06-21 | 2020-09-11 | Nanocarbon Co Ltd | System and method for the automatic production of carbon nanomaterial |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102602912A (en) | 2012-07-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102602912B (en) | Synthesizing device for continuously producing carbon nano pipe with shape of crystal whisker | |
| CN103638950B (en) | A kind of CuS nanosheet photocatalytic material and preparation method | |
| CN102544499A (en) | Method for preparing lithium ferrous phosphate (LiFePO4) and carbon nano tube composite cathode material for lithium battery | |
| CN102921951A (en) | Nano-powder and graded preparation device of dispersing liquid thereof | |
| CN203678371U (en) | Device for preparing nano powder by using ultrasonic atomization-microwave pyrolysis combined method | |
| CN202519030U (en) | Synthesizing device for continuously producing whisker-shaped carbon nano tube | |
| CN104401966A (en) | Continuous type production equipment and method of carbon nano tube | |
| CN114852962A (en) | Hydrogen production system and method for decomposing alcohols by microwave plasma under normal pressure | |
| CN204171361U (en) | A kind of novel electric-explosion metal-nanometer | |
| CN202323024U (en) | Deposition chamber for chemical vapor deposition | |
| CN202940070U (en) | System for recovering scrap wires and cables | |
| CN103011123B (en) | Fully-automatic synthesis device for continuously producing whisker-shaped carbon nano tube | |
| CN103435026B (en) | A kind of continuous synthesis carbon receives the device of material | |
| CN202785662U (en) | Synthesis device for fully-automatic and continuous production of whisker-shaped carbon nanometer tube | |
| CN109248637B (en) | Heat treatment equipment for continuous lithium ion battery cathode material and use method | |
| CN102139374B (en) | Method for preparing metal zinc nanometer wire | |
| CN202201355U (en) | Resin pot with pressurized discharging mechanism | |
| CN202440314U (en) | Preparation device for graphene | |
| CN210711403U (en) | Microwave pyrolysis atmosphere furnace and coal hydrogenation microwave pyrolysis system | |
| CN103936009B (en) | A kind of thermal decomposition of silane produces the device and method of nano level high-purity silicon powder | |
| CN202527134U (en) | Multi-pole magnetic ring spray granulator | |
| CN106477556A (en) | A kind of automatic carbon nano material continuous producing apparatus and production method | |
| CN203781853U (en) | Device for continuously synthesizing carbon nano-tubes by virtue of flame method | |
| CN105498644A (en) | Electrically controlled mechanical equipment for chemical synthesis | |
| CN202876822U (en) | Moisturizing and cooling mechanism of vortex reaction kettle synthesizer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160713 Address after: 330103 Nanchang Changleng Industrial Park in Jiangxi Province Huang Xi Road Patentee after: Nanchang Weisike Nano Technology Co. Ltd. Address before: 999 No. 330031 Jiangxi province Nanchang Honggutan University Avenue Patentee before: Nanchang University |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20180213 Address after: 330052 Jiangxi city of Nanchang province Nanchang County Blue Economic and Technological Development Zone Jinsha Road West, three Toyama Road South Patentee after: Jiangxi Kelaiwei carbon nano materials Co. Ltd. Address before: 330103 Nanchang Changleng Industrial Park in Jiangxi Province Huang Xi Road Patentee before: Nanchang Weisike Nano Technology Co. Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190628 Address after: 452470 Henan Xinbo Mine Equipment Technology Co., Ltd. (Jiaohe Village, Zhongyue District) Patentee after: Henan Calway nano carbon materials Co., Ltd. Address before: 330052 Nanchang County Xiaolan economic and Technological Development Zone, Nanchang County, Nanchang, Jiangxi, west of Jinsha three road, south of Toyama Patentee before: Jiangxi Kelaiwei carbon nano materials Co. Ltd. |
|
| TR01 | Transfer of patent right |