CN102586021B - Method for recovering aroma components from solution containing aroma components - Google Patents
Method for recovering aroma components from solution containing aroma components Download PDFInfo
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- CN102586021B CN102586021B CN 201210055669 CN201210055669A CN102586021B CN 102586021 B CN102586021 B CN 102586021B CN 201210055669 CN201210055669 CN 201210055669 CN 201210055669 A CN201210055669 A CN 201210055669A CN 102586021 B CN102586021 B CN 102586021B
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- macroporous adsorbent
- aroma component
- ethanol
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Abstract
The invention discloses a method for recovering aroma components from solution containing the aroma components, which is characterized in that: aqueous solution of low ethanol or aqueous solution containing the aroma components is adopted as a raw material; macroporous adsorption resin is used for adsorbing the aroma components in the aqueous solution of the low ethanol or the aqueous solution; edible grade ethanol with high concentration is used for eluting; and eluent is high-concentration ethanol solution containing high-concentration aroma components. The method is effective to recover the aroma components, and the aroma components recovered by adopting the method can be directly used for wine or drinks.
Description
Technical field:
The present invention relates to fruit distillate liquor class technology and brewing technology, is a kind of method that reclaims aroma component from the solution that contains aroma component specifically.
Background technology:
Fruit distillate liquor class development at present is very fast, various in style, but fragrance and the palatability of the fruit distillate liquor of brewageing are poor, its key is the aroma component deficiency, and the root of the deficiency of aroma component is that in still-process, the aroma component loss is larger, these aroma components are the source of the overall fragrance of wine, are also the sources of the overall sense of taste simultaneously.
Fruit distillate liquor adopts the method for second distillation more at present, distillation for the first time has the aroma component loss that accounts for total aroma component 30% left and right, still-process has the aroma component loss that accounts for total aroma component 35% left and right for the second time, these compositions are present in the aqueous solution or the aqueous solution of low ethanol, thereby affect overall fragrance and the mouthfeel of wine.
Summary of the invention:
The objective of the invention is to overcome the deficiency of above-mentioned prior art, and a kind of method that reclaims aroma component from the solution that contains aroma component is provided, mainly solve existing fruit distillate liquor aroma component loss and make wine aroma and the poor problem of palatability.
To achieve these goals, the present invention is achieved in that a kind of method that reclaims aroma component from the solution that contains aroma component, and its special character is that it comprises following processing step:
The activation of a resin: purpose is the fully existing dew of all reactive sites made on resin, reaches product performance; The food grade alcohol immersion 8-48 h of volume percent 60%-95% for macroporous adsorbent resin, the ethanol that inclines, with 1-6 BV/h speed cleaning resin, then use the deionized water washing resin with above-mentioned ethanol, to ethanol content in resin at 10%(v/v) below get final product;
The processing of b resin to containing aroma component solution: the low aqueous ethanolic solution that contains aroma component or the aqueous solution are clear soln, this solution is through the macroporous adsorbent resin of overactivation, solution stream is 1-10 BV/h through the speed of macroporous adsorbent resin, stops feed liquor when containing aroma component in the macroporous adsorbent resin effluent liquid;
The recovery of c aroma component and resin regeneration: using the food grade volume percent is 60%-95% ethanol, ethanol used passes through macroporous adsorbent resin with the speed of 1-6 BV/h, wash-out is adsorbed on the aroma component on macroporous adsorbent resin, obtain elutriant, use again the deionized water wash macroporous adsorbent resin, to ethanol content in resin at 10%(v/v) below, complete macroporous adsorbent resin regeneration; Resin through above method regeneration is reused again;
The d finished product: the ethanol eluate of macroporous adsorbent resin is the product of the high alcohol concn of obtained high fragrance constituent concentration, can further use, for blending wine or the beverage that the fragrance relative content is low.
A kind of method that reclaims aroma component from the solution that contains aroma component of the present invention is mainly resin to hocket to the aqueous solution of the low ethanol that contains aroma component or processing and two techniques of resin regeneration of the aqueous solution.
Compared with the prior art a kind of method that reclaims aroma component from the solution that contains aroma component of the present invention has outstanding substantive distinguishing features and marked improvement, but 1, the method efficient recovery aroma component, and the aroma component reclaimed can be directly used in blended liquor or beverage, improve fragrance and the mouthfeel of wine or beverage, reduced the waste of aroma component; 2, method is simple, and resin is renewable, and recycling, economize in raw materials, and cost is low.
Embodiment:
For Comprehension and Implementation better, below in conjunction with embodiment, describe a kind of method that reclaims aroma component from the solution that contains aroma component of the present invention in detail.
Example 1, the example that is recovered as of distilling for the first time aroma component in debris with brandy comprises following processing step:
(1) distilling for the first time debris processes: distill for the first time debris and carry out clarifying treatment, obtain clear soln;
(2) activation of resin: the food grade alcohol immersion 8-48h by macroporous adsorbent resin with volume percent 60%-95%, ethanol inclines, clean resin with above-mentioned ethanol with 1-6BV/h speed, then use the deionized water washing resin, to ethanol content in resin at 10%(v/v) below get final product;
(3) macroporous adsorbent resin is to distilling for the first time aroma component absorption in debris: (1) step clear soln is through the macroporous adsorbent resin of (2) step activation, solution stream is 1-10 BV/h through the speed of macroporous adsorbent resin, when from the macroporous adsorbent resin effluent liquid, containing aroma component, stop into solution;
(4) acquisition of aroma component and macroporous adsorbent resin regeneration: the regeneration of macroporous adsorbent resin, using the food grade volume percent is 60%-95% ethanol, ethanol passes through macroporous adsorptive resins with the speed of 1-6 BV/h, wash-out is adsorbed on the aroma component on macroporous adsorbent resin, obtain elutriant, use again the rinsed with deionized water macroporous adsorbent resin, to ethanol content in resin at 10%(v/v) below, complete macroporous adsorbent resin regeneration;
(5) reuse: the resin through above method regeneration is reused again;
(6) finished product: the ethanol eluate through macroporous adsorbent resin is the high concentration ethanol aqueous solution that contains aroma component, can be used for blending good to eat wine or beverage etc.
Embodiment 2, distill for the second time the example that is recovered as of aroma component in debris with brandy, and it comprises following processing step:
(1) distilling for the second time debris processes: distill for the second time debris and filtered as the case may be or do not filter, obtain clear soln;
(2) resin activation: the food grade alcohol immersion 8-48 h by macroporous adsorbent resin with volume percent 60%-95%, ethanol inclines, with above-mentioned ethanol with 1-6 BV/h speed washing resin, to without any peculiar smell and reach the requirement of regulation, use again the deionized water washing resin, getting final product below 10% to ethanol content in resin;
(3) macroporous adsorbent resin is to distilling for the second time aroma component absorption in debris: the clear soln of the low ethanol of step (1) is through macroporous adsorbent resin, the flow through speed of macroporous adsorbent resin of debris is 1-10 BV/h, while in the macroporous adsorbent resin effluent liquid, containing aroma component, stop into debris;
(4) acquisition of aroma component and macroporous adsorbent resin regeneration: the regeneration of macroporous adsorbent resin, using the food grade volume percent is 60%-95% ethanol, ethanol used passes through macroporous adsorptive resins with the speed of 1-6 BV/h, the aroma component that wash-out is adsorbed on macroporous adsorbent resin obtains elutriant, use again the rinsed with deionized water macroporous adsorbent resin, to ethanol content in resin at 10%(v/v) below, complete macroporous adsorbent resin regeneration;
(5) reuse: the resin through above method regeneration re-uses;
(6) finished product: obtain wash-out stream, be and contain the high concentration ethanol aqueous solution that aroma component is higher, can be used for blending good to eat wine or beverage etc.
Embodiment 3, and with the example that is recovered as of aroma component in the brandy foreshot, it comprises following processing step:
(1) the brandy foreshot processes: the brandy foreshot carries out clarifying treatment as the case may be, obtains the liquid of clarification, with deionized water, is diluted to ethanol content below 10%, also can first dilute and carry out clarifying treatment again;
(2) resin activation: the food grade alcohol immersion 8-48h by macroporous adsorbent resin with volume percent 60%-95%, ethanol inclines, with ethanol with 1-6 BV/h speed washing resin, to without any peculiar smell and reach the requirement of regulation, use again the deionized water washing resin, to ethanol content in resin at 10%(v/v) below get final product;
(3) macroporous adsorbent resin adsorbs aroma component in the brandy foreshot after diluting: the clarified liq of the low ethanol of (1) step is through the macroporous adsorbent resin of (2) step activation, the flow through speed of macroporous adsorbent resin of clarified liq is 1-10BV/h, while in the macroporous adsorbent resin effluent liquid, containing aroma component, stop into debris;
(4) acquisition of aroma component and macroporous adsorbent resin regeneration: using the food grade volume percent is 60%-95% ethanol, and ethanol passes through macroporous adsorbent resin with the speed of 1-6 BV/h, and wash-out is adsorbed on the aroma component on macroporous adsorbent resin, obtains elutriant; Use again the rinsed with deionized water macroporous adsorbent resin, to ethanol content in resin at 10%(v/v) below, complete macroporous adsorbent resin regeneration;
(5) reuse: the resin through above method regeneration re-uses;
(6) finished product: the elutriant obtained is the high concentration ethanol aqueous solution that contains aroma component, can be used for blending good to eat wine or beverage etc.
Claims (1)
1. a method that reclaims aroma component from the solution that contains aroma component is characterized in that it comprises following processing step:
The activation of a resin: the food grade alcohol immersion 8-48 h of volume percent 60%-95% for macroporous adsorbent resin, ethanol inclines, clean resin with above-mentioned ethanol with 1-6 BV/h speed, then use the deionized water washing resin, to ethanol content in resin at 10%(v/v) below get final product;
The processing of b resin to containing aroma component solution: the low aqueous ethanolic solution that contains aroma component or the aqueous solution are clear soln, this solution is that brandy distills for the first time debris, brandy and distills for the second time debris or brandy foreshot, macroporous adsorbent resin through overactivation, solution stream is 1-10 BV/h through the speed of macroporous adsorbent resin, stops feed liquor when containing aroma component in the macroporous adsorbent resin effluent liquid;
The recovery of c aroma component and resin regeneration: using the food grade volume percent is 60%-95% ethanol, ethanol used passes through macroporous adsorbent resin with the speed of 1-6 BV/h, wash-out is adsorbed on the aroma component on macroporous adsorbent resin, obtain elutriant, use again the deionized water wash macroporous adsorbent resin, to ethanol content in resin at 10%(v/v) below, complete macroporous adsorbent resin regeneration;
The d finished product: the ethanol eluate of macroporous adsorbent resin is the product of the high alcohol concn of obtained high intensity fragrance composition.
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| CN 201210055669 CN102586021B (en) | 2012-03-06 | 2012-03-06 | Method for recovering aroma components from solution containing aroma components |
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| CN 201210055669 CN102586021B (en) | 2012-03-06 | 2012-03-06 | Method for recovering aroma components from solution containing aroma components |
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| CN102586021A CN102586021A (en) | 2012-07-18 |
| CN102586021B true CN102586021B (en) | 2013-12-25 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| EP2893817B1 (en) * | 2014-01-10 | 2017-07-19 | Wia Wine AG | Device and method for producing of a de-alcoholised beverage |
| CN104403795B (en) * | 2014-10-29 | 2017-03-08 | 湖北中烟工业有限责任公司 | A kind of application with the preparation method of yellow wine extraction thing and its in Medicated cigarette for cigarette |
| CN105066590B (en) * | 2015-07-22 | 2017-03-29 | 大闽食品（漳州）有限公司 | A kind of method of absorption grapefruit flower fragrant volatile of fresh flowers and low temperature drying shaddock fresh flower |
| CN106190556A (en) * | 2016-07-22 | 2016-12-07 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette fermented type blackberry extractum flavor components |
| CN106221909A (en) * | 2016-07-22 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Fructus Pruni extractum flavor components |
| CN108244427A (en) * | 2017-12-20 | 2018-07-06 | 烟台大学 | A kind of method for improving fruit juice or fruit wine quality |
| CN108660037A (en) * | 2018-05-22 | 2018-10-16 | 贵州省生物研究所 | A kind of method and perfume compounding method of the enrichment of Blueberry brandy fruity |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102100721A (en) * | 2011-01-26 | 2011-06-22 | 安徽协和成药业饮片有限公司 | Method for producing total flavonoids of chrysanthemum |
| CN102178207A (en) * | 2011-04-25 | 2011-09-14 | 天宁香料（江苏）有限公司 | Wallace melon essence and preparation method thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102100721A (en) * | 2011-01-26 | 2011-06-22 | 安徽协和成药业饮片有限公司 | Method for producing total flavonoids of chrysanthemum |
| CN102178207A (en) * | 2011-04-25 | 2011-09-14 | 天宁香料（江苏）有限公司 | Wallace melon essence and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| 邢其毅，金声，林祖铭，王显仑等.荔枝香气化学成分的研究.《北京大学学报(自然科学版)》.1995,第31卷(第02期), * |
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Effective date of registration: 20190813 Address after: 264000 No. 56 Dama Road, Zhifu District, Yantai City, Shandong Province Patentee after: Zhangyu Wine Making Co., Ltd., Yantai City Address before: 264000 Airport Road, Zhifu, Shandong, No. 1, No. Patentee before: Yantai Zhongyu Group Co., Ltd. |