CN102586021A - Method for recovering aroma components from solution containing aroma components - Google Patents
Method for recovering aroma components from solution containing aroma components Download PDFInfo
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- CN102586021A CN102586021A CN2012100556691A CN201210055669A CN102586021A CN 102586021 A CN102586021 A CN 102586021A CN 2012100556691 A CN2012100556691 A CN 2012100556691A CN 201210055669 A CN201210055669 A CN 201210055669A CN 102586021 A CN102586021 A CN 102586021A
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- aroma component
- macroporous adsorbent
- ethanol
- adsorbent resin
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Abstract
The invention discloses a method for recovering aroma components from solution containing the aroma components, which is characterized in that: aqueous solution of low ethanol or aqueous solution containing the aroma components is adopted as a raw material; macroporous adsorption resin is used for adsorbing the aroma components in the aqueous solution of the low ethanol or the aqueous solution; edible grade ethanol with high concentration is used for eluting; and eluent is high-concentration ethanol solution containing high-concentration aroma components. The method is effective to recover the aroma components, and the aroma components recovered by adopting the method can be directly used for wine or drinks.
Description
Technical field:
The present invention relates to fruit distillate liquor class technology and brewing technology, is a kind of method that from the solution that contains aroma component, reclaims aroma component specifically.
Background technology:
Fruit distillate liquor class development at present is very fast; Various in style; But the fragrance and the palatability of the fruit distillate liquor of brewageing are relatively poor, and its key is that aroma component is not enough, and the insufficient root of aroma component is that the aroma component loss is bigger in the still-process; These aroma components are the source of the overall fragrance of wine, also are the sources of the overall sense of taste simultaneously.
Fruit distillate liquor adopts the method for second distillation more at present; Distillation for the first time has the aroma component loss that accounts for total aroma component about 30%; Still-process has the aroma component loss that accounts for total aroma component about 35% for the second time; These compositions are present in the low alcoholic acid aqueous solution or the aqueous solution, thereby influence the overall fragrance and the mouthfeel of wine.
Summary of the invention:
The objective of the invention is to overcome the deficiency of above-mentioned prior art, and a kind of method that from the solution that contains aroma component, reclaims aroma component is provided, mainly solve existing fruit distillate liquor aroma component loss and make wine aroma and the relatively poor problem of palatability.
To achieve these goals, the present invention is achieved in that a kind of method that from the solution that contains aroma component, reclaims aroma component, and its special character is that it comprises following process step:
The activation of a resin: purpose is fully existing the revealing of all reactive sites that makes on the resin, reaches product performance; Macroporous adsorbent resin is with the food grade alcohol immersion 8-48 h of volume percent 60%-95%, and the ethanol that inclines cleans resin with above-mentioned ethanol with 1-6 BV/h speed, uses the deionized water wash resin again, and ethanol content gets final product below 10% (v/v) to the resin;
The b resin is to containing the processing of aroma component solution: the low aqueous ethanolic solution or the aqueous solution that contain aroma component are clear soln; This solution is through the activatory macroporous adsorbent resin; Solution stream is 1-10 BV/h through the speed of macroporous adsorbent resin, stops feed liquor when to the macroporous adsorbent resin effluent, containing aroma component;
The recovery of c aroma component and resin regeneration: use the food grade volume percent to be 60%-95% ethanol; Used ethanol passes through macroporous adsorbent resin with the speed of 1-6 BV/h; Wash-out is adsorbed on the aroma component on the macroporous adsorbent resin, obtains elutriant, uses the deionized water wash macroporous adsorbent resin again; Ethanol content is accomplished macroporous adsorbent resin regeneration below 10% (v/v) to the resin; Reuse again through above method regenerated resin;
The d finished product: the ethanol eluate of macroporous adsorbent resin is the product of the high alcohol concn of high aroma component concentration that obtains, and can further use, and is used to blend low wine of fragrance relative content or beverage.
A kind of method that from the solution that contains aroma component, reclaims aroma component of the present invention mainly is a resin to hocket to the low alcoholic acid aqueous solution that contains aroma component or processing and two technologies of resin regeneration of the aqueous solution.
Compared with present technology a kind of method that from the solution that contains aroma component, reclaims aroma component of the present invention has outstanding substantive distinguishing features and marked improvement; But 1, this method efficient recovery aroma component; And the aroma component that reclaims can directly be used for blended liquor or beverage; Improve the fragrance and the mouthfeel of wine or beverage, reduced the waste of aroma component; 2, method is simple, and resin is renewable, and recycling economizes in raw materials, and cost is low.
Embodiment:
In order to understand better and to implement, specify a kind of method that from the solution that contains aroma component, reclaims aroma component of the present invention below in conjunction with embodiment.
Instance 1, the example that is recovered as so that brandy distills aroma component in the debris for the first time comprises following process step:
(1) distilling debris for the first time handles: distill debris for the first time and carry out clarifying treatment, obtain clear soln;
(2) activation of resin: with the food grade alcohol immersion 8-48h of macroporous adsorbent resin with volume percent 60%-95%; Ethanol inclines; Clean resin with above-mentioned ethanol with 1-6BV/h speed, use the deionized water wash resin again, ethanol content gets final product below 10% (v/v) to the resin;
(3) macroporous adsorbent resin is to distilling for the first time aroma component absorption in the debris: (1) step clear soln is through (2) step activatory macroporous adsorbent resin; Solution stream is 1-10 BV/h through the speed of macroporous adsorbent resin; When from the macroporous adsorbent resin effluent, containing aroma component, stop into solution;
(4) acquisition of fragrance component and macroporous absorbent resin regeneration: the regeneration of macroporous absorbent resin; Use the food grade percent by volume to be 60%-95% ethanol; Ethanol passes through the macroporous absorbent resin post with the speed of 1-6 BV/h; Wash-out is adsorbed on the fragrance component on the macroporous absorbent resin; Obtain eluent; Use the rinsed with deionized water macroporous absorbent resin again, ethanol content is at 10%(v/v to the resin) below, macroporous absorbent resin regeneration promptly accomplished;
(5) reuse: reuse again through above method regenerated resin;
(6) finished product: the ethanol eluate through macroporous adsorbent resin is the high concentration ethanol aqueous solution that contains aroma component, can be used for blending good to eat wine or beverage etc.
Embodiment 2, and with the example that is recovered as that brandy distills aroma component in the debris for the second time, it comprises following process step:
(1) distilling debris for the second time handles: distill debris for the second time and filter or do not filter based on concrete condition, obtain clear solutions;
(2) resin activation: with the food grade alcohol immersion 8-48 h of macroporous adsorbent resin with volume percent 60%-95%; Ethanol inclines; With above-mentioned ethanol with 1-6 BV/h speed washing resin; To having no peculiar smell and reaching the requirement of regulation, use the deionized water wash resin again, ethanol content is getting final product below 10% to the resin;
(3) macroporous adsorbent resin is to distilling for the second time aroma component absorption in the debris: the low alcoholic acid clear soln of step (1) is through macroporous adsorbent resin; The flow through speed of macroporous adsorbent resin of debris is 1-10 BV/h; When containing aroma component in the macroporous adsorbent resin effluent, stop into debris;
(4) acquisition of fragrance component and macroporous absorbent resin regeneration: the regeneration of macroporous absorbent resin; Use the food grade percent by volume to be 60%-95% ethanol; Used ethanol passes through the macroporous absorbent resin post with the speed of 1-6 BV/h; The fragrance component that wash-out is adsorbed on the macroporous absorbent resin obtains eluent; Use the rinsed with deionized water macroporous absorbent resin again; Ethanol content is at 10%(v/v to the resin) below, macroporous absorbent resin regeneration promptly accomplished;
(5) reuse: re-use through above method regenerated resin;
(6) finished product: obtain wash-out stream, be and contain the higher high concentration ethanol aqueous solution of aroma component, can be used for blending good to eat wine or beverage etc.
Embodiment 3, and with the example that is recovered as of aroma component among the brandy foreshot, it comprises following process step:
(1) the brandy foreshot handles: the brandy foreshot carries out clarifying treatment as the case may be, obtains clarifying liquid, is diluted to ethanol content below 10% with deionized water, also can dilute earlier and carry out clarifying treatment again;
(2) resin activation: with the food grade alcohol immersion 8-48h of macroporous adsorbent resin with volume percent 60%-95%; Ethanol inclines; With ethanol with 1-6 BV/h speed washing resin; To having no peculiar smell and reaching the requirement of regulation, use the deionized water wash resin again, ethanol content gets final product below 10% (v/v) to the resin;
(3) macroporous adsorbent resin adsorbs aroma component among the brandy foreshot after diluting: the low alcoholic acid clarified liq of (1) step is through (2) step activatory macroporous adsorbent resin; The flow through speed of macroporous adsorbent resin of clarified liq is 1-10BV/h; When containing aroma component in the macroporous adsorbent resin effluent, stop into debris;
(4) acquisition of aroma component and macroporous adsorbent resin regeneration: use the food grade volume percent to be 60%-95% ethanol, ethanol passes through macroporous adsorbent resin with the speed of 1-6 BV/h, and wash-out is adsorbed on the aroma component on the macroporous adsorbent resin, obtains elutriant; Use the rinsed with deionized water macroporous adsorbent resin again, ethanol content is promptly accomplished macroporous adsorbent resin regeneration below 10% (v/v) to the resin;
(5) reuse: re-use through above method regenerated resin;
(6) finished product: the elutriant that obtains is the high concentration ethanol aqueous solution that contains aroma component, can be used for blending good to eat wine or beverage etc.
Claims (1)
1. method that from the solution that contains aroma component, reclaims aroma component is characterized in that it comprises following process step:
The activation of a resin: macroporous adsorbent resin is with the food grade alcohol immersion 8-48 h of volume percent 60%-95%; Ethanol inclines; Clean resin with above-mentioned ethanol with 1-6 BV/h speed, use the deionized water wash resin again, ethanol content gets final product below 10% (v/v) to the resin;
The b resin is to containing the processing of aroma component solution: the low aqueous ethanolic solution or the aqueous solution that contain aroma component are clear soln; This solution is through the activatory macroporous adsorbent resin; Solution stream is 1-10 BV/h through the speed of macroporous adsorbent resin, stops feed liquor when to the macroporous adsorbent resin effluent, containing aroma component;
The recovery of c aroma component and resin regeneration: use the food grade volume percent to be 60%-95% ethanol; Used ethanol passes through macroporous adsorbent resin with the speed of 1-6 BV/h; Wash-out is adsorbed on the aroma component on the macroporous adsorbent resin, obtains elutriant, uses the deionized water wash macroporous adsorbent resin again; Ethanol content is accomplished macroporous adsorbent resin regeneration below 10% (v/v) to the resin;
The d finished product: the ethanol eluate of macroporous adsorbent resin is the product of the high alcohol concn of high intensity fragrance composition that obtains.
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| CN 201210055669 CN102586021B (en) | 2012-03-06 | 2012-03-06 | Method for recovering aroma components from solution containing aroma components |
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| CN 201210055669 CN102586021B (en) | 2012-03-06 | 2012-03-06 | Method for recovering aroma components from solution containing aroma components |
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| CN102586021A true CN102586021A (en) | 2012-07-18 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104403795A (en) * | 2014-10-29 | 2015-03-11 | 湖北中烟工业有限责任公司 | Cigarette-use yellow rice wine extract preparation method, and application method of cigarette-use yellow rice wine extract in cigarette |
| CN105066590A (en) * | 2015-07-22 | 2015-11-18 | 大闽食品（漳州）有限公司 | Methods for adsorbing fragrance volatiles of grapefruit fresh flowers and drying grapefruit fresh flowers at low temperature |
| CN106028835A (en) * | 2014-01-10 | 2016-10-12 | Wia红酒公司 | Device and method for producing a dealcoholized beverage |
| CN106190556A (en) * | 2016-07-22 | 2016-12-07 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette fermented type blackberry extractum flavor components |
| CN106221909A (en) * | 2016-07-22 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Fructus Pruni extractum flavor components |
| CN108244427A (en) * | 2017-12-20 | 2018-07-06 | 烟台大学 | A kind of method for improving fruit juice or fruit wine quality |
| CN108660037A (en) * | 2018-05-22 | 2018-10-16 | 贵州省生物研究所 | A kind of method and perfume compounding method of the enrichment of Blueberry brandy fruity |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106028835A (en) * | 2014-01-10 | 2016-10-12 | Wia红酒公司 | Device and method for producing a dealcoholized beverage |
| US11230687B2 (en) | 2014-01-10 | 2022-01-25 | Wia Wine Ag | Device and method for producing a dealcoholized beverage |
| CN104403795A (en) * | 2014-10-29 | 2015-03-11 | 湖北中烟工业有限责任公司 | Cigarette-use yellow rice wine extract preparation method, and application method of cigarette-use yellow rice wine extract in cigarette |
| CN104403795B (en) * | 2014-10-29 | 2017-03-08 | 湖北中烟工业有限责任公司 | A kind of application with the preparation method of yellow wine extraction thing and its in Medicated cigarette for cigarette |
| CN105066590A (en) * | 2015-07-22 | 2015-11-18 | 大闽食品（漳州）有限公司 | Methods for adsorbing fragrance volatiles of grapefruit fresh flowers and drying grapefruit fresh flowers at low temperature |
| CN106190556A (en) * | 2016-07-22 | 2016-12-07 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette fermented type blackberry extractum flavor components |
| CN106221909A (en) * | 2016-07-22 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Fructus Pruni extractum flavor components |
| CN108244427A (en) * | 2017-12-20 | 2018-07-06 | 烟台大学 | A kind of method for improving fruit juice or fruit wine quality |
| CN108660037A (en) * | 2018-05-22 | 2018-10-16 | 贵州省生物研究所 | A kind of method and perfume compounding method of the enrichment of Blueberry brandy fruity |
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| CN102586021B (en) | 2013-12-25 |
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Effective date of registration: 20190813 Address after: 264000 No. 56 Dama Road, Zhifu District, Yantai City, Shandong Province Patentee after: Zhangyu Wine Making Co., Ltd., Yantai City Address before: 264000 Airport Road, Zhifu, Shandong, No. 1, No. Patentee before: Yantai Zhongyu Group Co., Ltd. |
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