CN1025429C - Composite heat-insulating silicate shapes and production process - Google Patents

Composite heat-insulating silicate shapes and production process Download PDF

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Publication number
CN1025429C
CN1025429C CN 91111471 CN91111471A CN1025429C CN 1025429 C CN1025429 C CN 1025429C CN 91111471 CN91111471 CN 91111471 CN 91111471 A CN91111471 A CN 91111471A CN 1025429 C CN1025429 C CN 1025429C
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China
Prior art keywords
water
silicate
alumina
sepiolite
chrysotile
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Expired - Fee Related
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CN 91111471
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Chinese (zh)
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CN1063474A (en
Inventor
游绍龙
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SANXIA ENERGY SAVING PRODUCTS FACTORY DIANJIANG COUNTY SICHUAN PROV
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Application filed by SANXIA ENERGY SAVING PRODUCTS FACTORY DIANJIANG COUNTY SICHUAN PROV filed Critical SANXIA ENERGY SAVING PRODUCTS FACTORY DIANJIANG COUNTY SICHUAN PROV
Priority to CN 91111471 priority Critical patent/CN1025429C/en
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Abstract

The present invention relates to a composite heat insulation silicate sectional material which belongs to heat insulation materials for buildings, etc. The present invention is a fibrous reticular elastic material rich in sealed micropores, and has the offwhite appearance and the density between 220 and 250 kg/m<3>. The present invention is composed of serpentine asbestos, alumina-silicate ceramic fiber, dioctyl succinate sulfonate, sepiolite, expanded perlite and water, is manufactured by processes such as heat preservation soaking, agitation pulping and cast drying, is widely used for heat preservation and cold preservation engineering with the medium temperature between-40 and 700 DEG C, such as equipment, pipelines, kilns, buildings, cold storage, freezing (boxes) vehicles, etc., and has the characteristics of good performance, convenient operation, economy and practicality.

Description

Composite heat-insulating silicate shapes and production process
The invention belongs to used thermal insulation material and production methods thereof such as equipment, buildings.
Immediate with the present invention in the existing insulation cold insulation material is that application number is that 87101962(1988 is open March 30) patent application disclosed " composite silicate heat insulation material ".This lagging material is with its superior performance, and good energy-saving effect has been brought into play in widespread use in Industry Branch.Existing nearly this lagging material of various schools of thinkers plant produced in the existing whole nation.But, because this lagging material is pasty state, take the mode of brushing layer by layer, construction to need under heated condition, treat the priming paint moisture evaporation during application, can the brushing last layer after the drying.Medium temperature is not high, ambient moisture is bigger if run into, and then the engineering time will be very long.For the equipment that does not have heating condition, buildings, freezer etc., just can not use at all.
The purpose of this invention is to provide a kind of high-performance that can keep composite silicate heat insulation material, again a kind of novel thermal insulation material that can under heating or the condition that does not heat, can both use.
Theme of the present invention is not found identical with product component of the present invention or proximate public technology through the Chongqing branch update search of Chinese science and technology Institute of Social Science Information.
Product of the present invention is the fibrous web-like resilient material that is rich in closed porosity that is made of the multiple light body non-metallic minerals that contains silicate, appearance off-white, density 220~250kg/m 3Its component and content (weight percent) are: chrysotile 15.15~20.00, alumina-silicate ceramic fibre 3.79~10.00, pearlstone 7.58~13.33, sepiolite 2.27~4.67, dioctyl succinate acid sodium 2.27~4.67, surplus are water.
The production method of product of the present invention is: make the composition silicate paste-like material earlier, make section bar again.Raw material and the consumption (weight percent) of producing this product are: chrysotile 3.71~4.62, alumina-silicate ceramic fibre 0.92~2.31, pearlstone 1.85~3.08, sepiolite 0.55~1.08, dioctyl sodium sulfosuccinate 0.55~1.08, surplus are water.Production stage is: (one) raw material is handled: chrysotile, the alumina-silicate ceramic fibre impurity elimination is loosened, and sepiolite is pulverized below 2 millimeters; (2) by prescription metering respectively; (3) soak: 40~60% dioctyl sodium sulfosuccinate of chrysotile, alumina-silicate ceramic fibre, formula ratio is added 40~60% boiling water of Total Water, and insulation was soaked about 24 hours; (4) stir: add the normal-temperature water of the difference of the dioctyl sodium sulfosuccinate of surplus and Total Water and boiling water amount, stir more than 20 minutes,, add sepiolite, pearlstone, stirring 3~5 minutes then to sparing to becoming the foam pasty state; (5) make section bar: pasty state is cast in the mould the dry back demoulding under 100~110 ℃ of temperature.
Product of the present invention detects through Chongqing Building Science Inst., its salient features such as following table: (table is seen the literary composition back)
Product of the present invention and common lagging material salient features relatively see the following form: (table is seen the literary composition back)
Be not difficult to find out that by last table The comprehensive performance of the present invention is better than other lagging materials.Compare with former " composite silicate heat insulation material ", product of the present invention has been done very big change on prescription, make its performance more perfect, and Application Areas enlarges.Simultaneously, because 1 cubic metre of section bar can be equivalent to nearly 2 cubic metres of liquid coating, and price is significantly less than the latter, has reduced transport charge and packing charge again, so use product of the present invention more economical.
Product of the present invention is applicable to insulation cold insulation engineerings such as the equipment of medium temperature in-40~700 ℃ of scopes, pipeline, kiln, freezer, buildings, freezing (Tibetan) case (car).Can be according to different insulation cold insulation object adjustment prescriptions, the section bar product of making different shapes, density and thickness.Only needing during use that this product is wrapped in dielectric surface gets final product.
Example formulations: (table is seen the literary composition back)
Production method is ditto described.
Project unit's indication test method
Dry state density kg/m 3231
Void content % 45.59
Water-intake rate g/cm 30.95
Rate of moisture absorption % 7.97
Thermal conductivity w/mk 0.034 impulse method, 17.5 ℃ of test temperatures
Resistance toheat is ℃ indeformable, do not ftracture, 600 ℃ of constant temperature of not efflorescence hour
Water resistance is indeformable, do not ftracture, not efflorescence tap water
Oil resistance is indeformable, do not ftracture, not efflorescence machine oil
Acid resistance is indeformable, do not ftracture, not efflorescence 1.0M hydrochloric acid
Alkaline resistance properties is indeformable, do not ftracture, not efflorescence 1.0 sodium hydroxide
Bonding strength MPa 1.6 * 10 -2
Ultimate compression strength MPa viscous deformation test specimen 100 * 100 * 80mm
Frost resistance does not ftracture, not efflorescence, average weightless 3.5%
Appearance off-white sheet material
Dry density normal temperature thermal conductivity heat resisting temperature
Material (kg/m 3) (W/mk) performance such as (≤℃) anti-water, anti-corruption
Antivibration, anti-water, acid and alkali-resistance, nothing
Product 231 0.034 700 dust of the present invention, the not needle-holding hand of no burn into
The ultra-fine glass of alkali is arranged
Cotton no fat felt 60-80 0.035 400 not water-fast, not oil resistant, the needle-holding hand of glass
The ultra-fine glass of alkali-free
Not oil resistant, needle-holding hand of the cotton no fat felt 70-80 0.035 600 of glass
Litaflex felt 70-95 0.044-0.050 500 water resisting property are poor
Pure aluminium silicate is fire-resistant
0.093(700 ℃ of fibre product 150-200) poor, the needle-holding hand of 1000-1100 water resisting property
Microporous calcium silicate
Goods 200-250 0.056 600 water resisting property is poor, acid and alkali-resistance not
Hard 550
Soft 230 thermotolerances of asbestos product 80-140 0.041-0.051 and water resisting property are poor, needle-holding hand
Rigid poly urethanes
Porous plastics 50-70 0.023-0.037 130 poor heat resistance
Material name specification dosage (weight %)
Chrysotile 5-65 4.21
Alumina-silicate ceramic fibre secondary 1.52
Dioctyl sodium sulfosuccinate proportion 1.04 0.84
95~100 ℃ 45.00 of boiling water
Normal-temperature water 45.07
Sepiolite 0.84
Pearlstone one-level 2.52

Claims (2)

1, composite heat-insulating silicate shapes, it is a kind of fibrous web-like resilient material that is rich in closed porosity, it is characterized in that component and content (weight percent) are: chrysotile 15.15~20.00, alumina-silicate ceramic fibre 3.79~10.00, pearlstone 7.58~13.33, sepiolite 2.27~4.67, dioctyl sodium sulfosuccinate 2.27~4.67, surplus are water.
2, the production method of product according to claim 1 is characterized in that:
(1) feed composition and consumption (weight percent) are: chrysotile 3.71~4.62, alumina-silicate ceramic fibre 0.92~2.31, pearlstone 1.85~3.08, sepiolite 0.55~1.08, dioctyl sodium sulfosuccinate 0.55~1.08, surplus are water;
(2) production stage is:
1. raw material is handled: chrysotile, alumina-silicate ceramic fibre impurity elimination, loosen, sepiolite is pulverized below 2 millimeters,
2. measure by prescription,
3. soak: 40~60% dioctyl sodium sulfosuccinate of chrysotile, alumina-silicate ceramic fibre, formula ratio is added 40~60% boiling water of Total Water, and insulation was soaked about 24 hours,
4. stir: the normal-temperature water of the dioctyl sodium sulfosuccinate of adding surplus and the difference of Total Water and boiling water amount, stir more than 20 minutes, to becoming foam lake shape, add sepiolite, pearlstone then, stir 3~5 minutes to even,
5. make section bar: thickener is cast in the mould the dry back demoulding under 100~110 ℃ of temperature.
CN 91111471 1991-12-03 1991-12-03 Composite heat-insulating silicate shapes and production process Expired - Fee Related CN1025429C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 91111471 CN1025429C (en) 1991-12-03 1991-12-03 Composite heat-insulating silicate shapes and production process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 91111471 CN1025429C (en) 1991-12-03 1991-12-03 Composite heat-insulating silicate shapes and production process

Publications (2)

Publication Number Publication Date
CN1063474A CN1063474A (en) 1992-08-12
CN1025429C true CN1025429C (en) 1994-07-13

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 91111471 Expired - Fee Related CN1025429C (en) 1991-12-03 1991-12-03 Composite heat-insulating silicate shapes and production process

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105924126B (en) * 2016-05-11 2018-08-21 临沂洪恩节能环保制品有限公司 A kind of nanocages metallic high temperature anti-corrosive thermal insulation material
CA3005556A1 (en) 2017-05-24 2018-11-24 Relborgn Pty Ltd Method of limiting permeability of a matrix to limit liquid and/or gas inflow

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C14 Grant of patent or utility model
GR01 Patent grant
C53 Correction of patent for invention or patent application
CB03 Change of inventor or designer information

Inventor after: You Zhilong

Inventor after: Zhou Longchi

Inventor before: You Zhilong

COR Change of bibliographic data

Free format text: CORRECT: INVENTOR; FROM: YOU ZHILONG TO: YOU ZHILONG; ZHOU LONGCHI

CP02 Change in the address of a patent holder

Address after: Chongqing Longteng Industrial and Trading Company

Address before: Sanxia Energy Saving Products Factory, Dianjiang County, Sichuan Prov.

ERR Gazette correction

Free format text: CORRECT: BIBLIOGRAPHIC CHANGE; FROM: ADDRESS SICHUAN THREE GORGES ENERGY-SAVING PRODUCTS FACTORY TO: APPLICANT CHONGQING CITY LONGTENG INDUSTRY AND TRADE CO., LTD.

CI01 Correction of invention patent gazette

Correction item: Description item change

Correct: Chongqing Longteng Industrial and Trading Company

False: Address Sanxia Energy Saving Products Factory, Dianjiang County, Sichuan Prov.

Number: 15

Page: 197

Volume: 12

C53 Correction of patent for invention or patent application
COR Change of bibliographic data

Free format text: CORRECT: PATENTEE; FROM: CHONGQING CITY LONGTENG INDUSTRY AND TRADE CO., LTD. TO: YOU SHAOLONG

CP03 Change of name, title or address

Address after: 401147 No. 178 Jinlong Road, Longxi Town, Chongqing, Yubei District

Co-patentee after: Dianjiang Chongqing County Education Committee Jia Bao thermal insulation material factory

Patentee after: You Shaolong

Address before: Longxi Town, Yubei District, Chongqing

Patentee before: Chongqing Longteng Industrial and Trading Company

C15 Extension of patent right duration from 15 to 20 years for appl. with date before 31.12.1992 and still valid on 11.12.2001 (patent law change 1993)
OR01 Other related matters
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee