CN102519828A - Method for testing utilization ratio of tobacco reconstituted through rolling process - Google Patents
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 150
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 150
- 238000000034 method Methods 0.000 title claims abstract description 41
- 238000005096 rolling process Methods 0.000 title claims abstract description 34
- 238000012360 testing method Methods 0.000 title abstract 5
- 238000005070 sampling Methods 0.000 claims abstract description 18
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 12
- 238000000926 separation method Methods 0.000 claims abstract description 4
- 238000001514 detection method Methods 0.000 claims description 22
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 10
- 239000003960 organic solvent Substances 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 8
- 238000005303 weighing Methods 0.000 claims description 3
- 238000000638 solvent extraction Methods 0.000 claims 3
- 238000005192 partition Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 14
- 238000003756 stirring Methods 0.000 description 11
- 239000001087 glyceryl triacetate Substances 0.000 description 7
- 235000013773 glyceryl triacetate Nutrition 0.000 description 7
- 229960002622 triacetin Drugs 0.000 description 7
- 239000011521 glass Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000012417 linear regression Methods 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000010187 selection method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
Description
the
技术领域 technical field
本发明涉及一种再造烟叶利用率的测定方法,特别是涉及一种辊压法再造烟叶利用率的测定方法。 The invention relates to a method for measuring the utilization rate of reconstituted tobacco leaves, in particular to a method for measuring the utilization rate of reconstituted tobacco leaves by rolling method.
the
背景技术 Background technique
辊压法再造烟叶以其设备简单、能耗低、成本低,被国内大多数卷烟企业所采用,但其生产的再造烟丝因抗张强度小、耐水性差、填充性能低而使有效利用率低,影响了卷烟配方的吻合性和产品质量稳定性;同时,辊压法再造烟叶掺配比例的稳定性和配方比例的符合性也是评价卷烟生产工艺工序能力的重要指标。目前通常的做法有三种:人工挑选法、单耗比值法、填充比值法,这些方法具有工作量大、结果准确性差等缺点,且无法判断烟丝内各组分在微小单元内是否也符合设计的配方,更无法判定烟丝在立体空间内是否分布均匀。因此,建立准确测定卷烟烟丝中辊压法再造烟叶掺配比例及其转化利用率有非常重要的意义。 Roller-pressed reconstituted tobacco is adopted by most domestic cigarette companies due to its simple equipment, low energy consumption and low cost. , affecting the conformity of the cigarette formula and product quality stability; at the same time, the stability of the blending ratio of the reconstituted tobacco leaves by the rolling method and the conformity of the formula ratio are also important indicators for evaluating the capability of the cigarette production process. At present, there are three common methods: manual selection method, unit consumption ratio method, and filling ratio method. These methods have the disadvantages of heavy workload and poor accuracy of results, and it is impossible to judge whether each component in shredded tobacco meets the design requirements in the tiny unit. formula, and it is impossible to determine whether the shredded tobacco is evenly distributed in the three-dimensional space. Therefore, it is of great significance to establish an accurate determination of the blending ratio and conversion utilization rate of reconstituted tobacco leaves by rolling method in shredded cigarette tobacco.
the
发明内容 Contents of the invention
本发明正是为了克服以上技术难题而提供一种能够准确、客观的测定辊压法再造烟叶利用率的方法。 The present invention provides a method for accurately and objectively measuring the utilization rate of reconstituted tobacco leaves by roll pressing to overcome the above technical problems.
本发明的目的可通过下述技术方案来实现: The purpose of the present invention can be achieved through the following technical solutions:
一种测定辊压法再造烟叶利用率方法,包括如下步骤: A method for measuring the utilization rate of reconstituted tobacco leaves by rolling method, comprising the steps of:
a、检测比例与实际比例的标准曲线的建立:预先设定实际比例xi并分别按照设定比例xi精确称量对应的多组烟丝组分、并将各组组分分别进行人工混合;将再造烟叶与烟丝其它组分分离,并用易挥发有机溶剂萃取,烘干后准确称重,计算与xi对应的辊压法再造烟叶的检测比例yi;通过多组对应的xi与yi值,建立检测比例与实际比例的标准曲线y=kx+b,其中y:为膨胀叶丝检测比例,k、b为具体拟合参数,x:为实际比例; a. The establishment of a standard curve between the detection ratio and the actual ratio: pre-set the actual ratio x i and accurately weigh the corresponding multiple groups of shredded tobacco components according to the set ratio x i respectively, and manually mix the components of each group respectively; Separating reconstituted tobacco leaves from other components of shredded tobacco, extracting them with volatile organic solvents, weighing them accurately after drying , and calculating the detection ratio y i of reconstituted tobacco leaves corresponding to x i ; i value, establish the standard curve y=kx+b of the detection ratio and the actual ratio, wherein y: is the detection ratio of expanded leaf shreds, k and b are specific fitting parameters, and x: is the actual ratio;
b、掺配后再造烟叶和其它烟丝组分的实际比例数据获取:在加香滚筒出口选取取样烟丝,将再造烟叶与烟丝其它组分分离,并用易挥发有机溶剂萃取,烘干后准确称重,得到一组取样烟丝中辊压法再造烟叶检测比例 ,分别根据步骤(a)建立的标准曲线计算取样烟丝中辊压法再造烟叶的实际比例,并计算其平均值; b. Acquisition of the actual proportion data of reconstituted tobacco leaves and other cut tobacco components after blending: select cut tobacco samples at the outlet of the flavoring drum, separate reconstituted tobacco leaves from other cut tobacco components, extract with volatile organic solvents, and weigh them accurately after drying , to obtain the detection ratio of rolled tobacco reconstituted tobacco leaves in a group of sampled cut tobacco , according to the standard curve established in step (a), calculate the actual proportion of rolled tobacco reconstituted tobacco in the sampled cut tobacco , and calculate its average ;
c、烟支中再造烟叶和其它烟丝组分的实际比例数据获取:在卷包机台上选取取样烟支并剥离烟丝,将再造烟叶与烟丝分离,并用易挥发有机溶剂萃取,烘干后准确称重,得到一组取样烟丝中辊压法再造烟叶检测比例,分别根据步骤(a)建立的标准曲线计算取样烟丝中辊压法再造烟叶的实际比例,并计算其平均值; c. Acquisition of the actual proportion data of reconstituted tobacco leaves and other cut tobacco components in cigarettes: select the sampled cigarettes on the wrapping machine and peel off the cut tobacco, separate the reconstituted tobacco leaves from the cut tobacco, extract them with volatile organic solvents, and weigh them accurately after drying Weight, to obtain a group of sampled cut tobacco in the roll-pressed reconstituted tobacco detection ratio , according to the standard curve established in step (a), calculate the actual proportion of rolled tobacco reconstituted tobacco in the sampled cut tobacco , and calculate its average ;
d、定义R为辊压法再造烟叶利用率,则R=/×100%。 d, define R as the utilization rate of reconstituted tobacco leaves by rolling method, then R= / ×100%.
式中:R:为辊压法再造烟叶利用率,:掺配后辊压法再造烟叶平均比例,:烟支中辊压法再造烟叶平均比例。 In the formula: R: the utilization rate of reconstituted tobacco leaves by rolling method, : The average proportion of reconstituted tobacco leaves by rolling method after blending, : Average proportion of rolled reconstituted tobacco leaves in a cigarette.
在本发明中,所述再造烟叶与烟丝其它组分分离的方法为,将烟丝混合物放入三醋酸甘油酯溶剂中,利用漂浮分离法,静置分离,下层为再造烟叶,上层为烟丝其它组分。 In the present invention, the method for separating the reconstituted tobacco leaves from other components of shredded tobacco is to put the shredded tobacco mixture into a triacetin solvent, and use the floating separation method to stand for separation. The lower layer is reconstituted tobacco leaves, and the upper layer is other components of shredded tobacco. point.
同时,本发明公开了人工混合烟丝量和取样烟丝量至少为5g,并且取样时要保证人工混合烟丝量和取样烟丝量的一致性。 At the same time, the invention discloses that the amount of artificially mixed shredded tobacco and the amount of sampled shredded tobacco are at least 5g, and the consistency between the amount of artificially mixed shredded tobacco and the amount of sampled shredded tobacco must be ensured during sampling.
本发明还同时公开了人工混合烟丝量和取样烟丝量均为5~10g。同时也要保证人工混合烟丝量和取样烟丝量的一致性,即人工混合烟丝量和取样烟丝量的要尽量接近。根据一般的数据统计常识,由于取样量增大,其数据更加丰富,检测的准确性也越高,所以本发明特别公开了5~10g的取样范围,从而可以同时保证检测数据的准确性和检测成本。 The invention also discloses that both the amount of shredded tobacco for artificial mixing and the amount of shredded tobacco for sampling are 5-10 g. At the same time, the consistency of the amount of artificially mixed shredded tobacco and the amount of sampled shredded tobacco should be ensured, that is, the amount of artificially mixed shredded tobacco and the amount of shredded tobacco sampled should be as close as possible. According to common knowledge of data statistics, due to the increase of sampling volume, the data will be more abundant and the accuracy of detection will be higher. Therefore, the present invention particularly discloses the sampling range of 5-10g, so that the accuracy of detection data and detection accuracy can be guaranteed at the same time. cost.
本发明还公开了所述烘干为在80~95℃的温度条件中烘干30分钟。 The invention also discloses that the drying is at a temperature of 80-95° C. for 30 minutes.
在本发明中所述的易挥发有机溶剂是指化学领域内的易挥发有机溶剂(如乙醇),在本发明的实际应用中可以结合低毒、低成本的要求具体选用。 The volatile organic solvent mentioned in the present invention refers to the volatile organic solvent (such as ethanol) in the chemical field, which can be specifically selected in combination with the requirements of low toxicity and low cost in the practical application of the present invention.
本发明的有益效果是:解决了目前卷烟企业辊压法再造烟叶利用率检测难题,为准确、客观检测辊压法再造烟叶利用率提供了一种可行方法,提供了可靠的技术参数和检测数据,对于控制生产过程稳定性、配方吻合性及烟支质量指标都具有重要意义。 The invention has the beneficial effects of: solving the problem of detecting the utilization rate of reconstituted tobacco leaves by rolling method in cigarette enterprises at present, providing a feasible method for accurate and objective detection of the utilization rate of reconstituted tobacco leaves by rolling method, and providing reliable technical parameters and detection data , which is of great significance to control the stability of the production process, the consistency of the formula and the quality indicators of cigarettes.
the
附图说明 Description of drawings
图1为实际比例与检测比例的标准曲线。 Fig. 1 is the standard curve of actual ratio and detection ratio.
the
具体实施方式 Detailed ways
实施例1 Example 1
a、检测比例与实际比例的标准曲线的建立:将辊压法再造烟叶分别按4%、6%、8%、10%、12%、14%、16%、18%、20%、22%的设定比例和其他烟丝组分精确称量、混合,每组混合烟丝约10g,放入1000ml装有三醋酸甘油酯溶剂的烧杯中用玻璃棒搅拌,静置2分钟后,分别取下层辊压法再造烟叶和上层烟丝其它组分,用95%乙醇浸泡并搅拌1分钟后过滤,放入90℃左右的烘箱中烘干30分钟后分别称重,计算辊压法再造烟叶在混合烟丝中的检测比例对应为3.8%、5.7%、7.8%、9.8%、11.8%、13.6%、15.8%、17.8%、20.4%、22.3%,得到检测比例与设定比例的线性回归方程y=1.0264x-0.0049,其标准曲线如图1所示。 a. The establishment of the standard curve between the detection ratio and the actual ratio: the rolling method reconstituted tobacco leaves are respectively 4%, 6%, 8%, 10%, 12%, 14%, 16%, 18%, 20%, 22% Precisely weigh and mix the set ratio and other cut tobacco components. Each group of mixed cut tobacco is about 10g, put it into a 1000ml beaker filled with triacetin solvent and stir it with a glass rod. After standing for 2 minutes, remove the lower layer and roll it The reconstituted tobacco leaves and other components of the upper layer of shredded tobacco were soaked in 95% ethanol and stirred for 1 minute, then filtered, dried in an oven at about 90°C for 30 minutes, and then weighed to calculate the content of reconstituted tobacco leaves in the mixed shredded tobacco. The detection ratio corresponds to 3.8%, 5.7%, 7.8%, 9.8%, 11.8%, 13.6%, 15.8%, 17.8%, 20.4%, 22.3%, and the linear regression equation y=1.0264x- 0.0049, and its standard curve is shown in Figure 1.
b、在A牌号加香滚筒出口用托盘接取混合烟丝3次,每次取样约10g,将烟丝混合物放入1000ml装有三醋酸甘油酯溶剂的烧杯中用玻璃棒搅拌,静置2分钟后,分别取下层辊压法再造烟叶和上层烟丝其它组分,用95%乙醇浸泡并搅拌1分钟后过滤,放入90℃左右的条件下的烘箱中烘干30分钟后称重,计算取样烟丝中辊压法再造烟叶检测比例15.80%、15.85%、15.82%,根据步骤(a)中建立的标准曲线计算取样烟丝中辊压法再造烟叶的实际比例15.87%、15.92%、15.89%,计算其平均值=15.89%。 b. Use a tray to pick up the mixed cut tobacco at the outlet of the flavoring drum of brand A for 3 times, and take a sample of about 10g each time. Put the cut tobacco mixture into a 1000ml beaker filled with triacetin solvent and stir it with a glass rod. After standing for 2 minutes, Remove the lower layer of reconstituted tobacco leaves and other components of the upper layer of shredded tobacco respectively, soak them in 95% ethanol and stir for 1 minute, then filter, put them in an oven at about 90°C for 30 minutes, weigh them, and calculate the sampled shredded tobacco. The detected proportions of reconstituted tobacco leaves by rolling method are 15.80%, 15.85%, and 15.82%. According to the standard curve established in step (a), the actual proportions of reconstituted tobacco leaves by rolling method in the cut tobacco are calculated as 15.87%, 15.92%, and 15.89%, and the average value =15.89%.
c、在A牌号同批次包装机上取样3次,每次15支(烟丝含量约0.7g/支),分别剥离烟丝约10g,将烟丝混合物放入1000ml装有三醋酸甘油酯溶剂的烧杯中用玻璃棒搅拌,静置2分钟后,分别取下层辊压法再造烟叶和上层烟丝其它组分,用95%乙醇浸泡并搅拌1分钟后过滤,放入90℃左右的条件下的烘箱中烘干30分钟后称重,计算取样烟丝中辊压法再造烟叶检测比例14.47%、14.56%、14.62%,根据步骤(a)建立的标准曲线计算取样烟丝中辊压法再造烟叶的实际比例14.58%、14.66%、14.72%,计算其平均值=14.65%。 c. Sampling 3 times on the packaging machine of the same batch of brand A, 15 pieces each time (tobacco content is about 0.7g/piece), peeling off about 10g of shredded tobacco respectively, and putting the shredded tobacco mixture into a 1000ml beaker with triacetin solvent for use Stir with a glass rod, let stand for 2 minutes, remove the lower layer of reconstituted tobacco leaves and other components of the upper layer of shredded tobacco, soak them in 95% ethanol and stir for 1 minute, then filter, and put them in an oven at about 90°C for drying Weigh after 30 minutes, and calculate the detected proportions of rolled tobacco reconstituted tobacco leaves in the sampled shredded tobacco as 14.47%, 14.56%, and 14.62%, and calculate the actual proportions of the rolled tobacco reconstituted tobacco leaves in the sampled tobacco cuts as 14.58%, 14.56%, and 14.62% according to the standard curve established in step (a). 14.66%, 14.72%, calculate the average =14.65%.
d、计算辊压法再造烟叶利用率:R=/×100%=92.20%。 d. Calculate the utilization rate of reconstituted tobacco leaves by rolling method: R= / ×100%=92.20%.
the
实施例2 Example 2
a、将辊压法再造烟叶分别按4%、6%、8%、10%、12%、14%、16%、18%、20%、22%的设定比例和其他烟丝组分精确称量、混合,每组混合烟丝约5g,放入500ml装有三醋酸甘油酯溶剂的烧杯中用玻璃棒搅拌,静置2分钟后,分别取下层辊压法再造烟叶和上层烟丝其它组分,用95%乙醇浸泡并搅拌1分钟后过滤,放入90℃左右的烘箱中烘干30分钟后分别称重,计算辊压法再造烟叶在混合烟丝中的检测比例对应为3.8%、5.7%、7.8%、9.8%、11.8%、13.6%、15.8%、17.8%、20.4%、22.3%,得到检测比例与设定比例的线性回归方程y=1.0264x-0.0049,其标准曲线如图1所示。 a. Accurately weigh the reconstituted tobacco leaves by rolling method according to the set proportions of 4%, 6%, 8%, 10%, 12%, 14%, 16%, 18%, 20%, 22% and other shredded tobacco components Measure and mix, about 5g of mixed shredded tobacco for each group, put it into a 500ml beaker filled with triacetin solvent and stir it with a glass rod. Soak in 95% ethanol and stir for 1 minute, then filter, dry in an oven at about 90°C for 30 minutes, and weigh them respectively. Calculate the detection ratios of reconstituted tobacco leaves in the blended shredded tobacco as 3.8%, 5.7%, and 7.8% respectively. %, 9.8%, 11.8%, 13.6%, 15.8%, 17.8%, 20.4%, 22.3%, the linear regression equation y=1.0264x-0.0049 of the detected ratio and the set ratio is obtained, and the standard curve is shown in Figure 1.
b、在B牌号加香滚筒出口用托盘接取混合烟丝3次,每次取样约5g,将烟丝混合物放入500ml装有三醋酸甘油酯溶剂的烧杯中用玻璃棒搅拌,静置2分钟后,分别取下层辊压法再造烟叶和上层烟丝其它组分,用95%乙醇浸泡并搅拌1分钟后过滤,放入90℃左右的条件下的烘箱中烘干30分钟后称重,计算取样烟丝中辊压法再造烟叶检测比例3.23%、3.24%、3.19%,根据步骤(a)中建立的标准曲线计算取样烟丝中辊压法再造烟叶的实际比例3.62%、3.63%、3.59%,计算其平均值=3.61%。 b. Use a tray to pick up the mixed cut tobacco at the outlet of the flavoring drum of brand B for 3 times, and take a sample of about 5g each time. Put the cut tobacco mixture into a 500ml beaker filled with triacetin solvent and stir it with a glass rod. After standing for 2 minutes, Remove the lower layer of reconstituted tobacco leaves and other components of the upper layer of shredded tobacco respectively, soak them in 95% ethanol and stir for 1 minute, then filter, put them in an oven at about 90°C for 30 minutes, weigh them, and calculate the sampled shredded tobacco. The detected proportions of reconstituted tobacco leaves by rolling method were 3.23%, 3.24%, and 3.19%. According to the standard curve established in step (a), the actual proportions of 3.62%, 3.63%, and 3.59% of reconstituted tobacco leaves by rolling method in the cut tobacco were calculated, and the average value =3.61%.
c、在B牌号同批次包装机上取样3次,每次7支(烟丝含量约0.7g/支),分别剥离烟丝,将烟丝混合物放入500ml装有三醋酸甘油酯溶剂的烧杯中用玻璃棒搅拌,静置2分钟后,分别取下层辊压法再造烟叶和上层烟丝其它组分,用95%乙醇浸泡并搅拌1分钟后过滤,放入85℃左右的条件下的烘箱中烘干30分钟后称重,计算取样烟丝中辊压法再造烟叶检测比例2.92%、2.95%、2.93%,根据步骤(a)建立的标准曲线计算取样烟丝中辊压法再造烟叶的实际比例3.32%、3.35%、3.33%,计算其平均值=3.33%。 c. Sampling 3 times on the packaging machine of the same batch of B brand, 7 pieces each time (tobacco content is about 0.7g/piece), peel off the shredded tobacco respectively, put the shredded tobacco mixture into a 500ml beaker with triacetin solvent and use a glass rod Stir and let stand for 2 minutes, remove the lower layer of reconstituted tobacco leaves and other components of the upper layer of shredded tobacco respectively, soak them in 95% ethanol and stir for 1 minute, then filter, put them in an oven at about 85°C for 30 minutes After weighing, calculate the detection ratios of 2.92%, 2.95%, and 2.93% of the reconstituted tobacco leaves by rolling method in the cut tobacco, and calculate the actual proportions of 3.32% and 3.35% of the reconstituted tobacco leaves by rolling method in the cut tobacco samples according to the standard curve established in step (a) , 3.33%, calculate the average =3.33%.
d、计算辊压法再造烟叶利用率:R=/×100%=92.24%。 d. Calculate the utilization rate of reconstituted tobacco leaves by rolling method: R= / ×100%=92.24%.
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CN1885003A (en) * | 2006-06-30 | 2006-12-27 | 中国烟草总公司郑州烟草研究院 | Method for determining tobacco shred ratio in cigarette |
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CN1885003A (en) * | 2006-06-30 | 2006-12-27 | 中国烟草总公司郑州烟草研究院 | Method for determining tobacco shred ratio in cigarette |
CN1885004A (en) * | 2006-06-30 | 2006-12-27 | 中国烟草总公司郑州烟草研究院 | Method for determining expansion shred doping ratio in tobacco shred |
CN101581648A (en) * | 2009-06-19 | 2009-11-18 | 中国烟草总公司郑州烟草研究院 | Method for testing tobacco flakes mixing ratio of cut tobacco blend |
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