Method and the device thereof of electric and electronic product low-temperature test proficiency testing
Technical field
The present invention relates to test capability verification technique field, be specifically related to method and the device thereof of low-temperature test proficiency testing.
Background technology
Environmental test is the research class fail-test of environment for use to material and product function and performance impact around.Temperature is as one of three large basic environmental factors, the use that affects product at all times.Research shows, 40% product field failure is relevant with temperature.
Electric and electronic product low-temperature test is the ability that uses under low temperature environment, transports or store for check element, equipment and other products.The range of application of low-temperature test is very extensive, and the electric and electronic products such as space flight, boats and ships, household electrical appliance, electronic devices and components all will carry out low-temperature test.Therefore establishing criteria (GB 2423.1) to product correct to carry out low-temperature test most important to correct assessment product ability.
Proficiency testing is to utilize comparison between laboratory to determine an activity of the calibration/detectability in laboratory or the detectability of inspection body.Ability verification refers to any for the comparison between the laboratory of evaluation experimental chamber ability and measurement audit.The activity for example being operated by the accreditation body in country or region and the supplier of cooperative association, government department or industry organization or other formal proficiency testing plan thereof.
Carry out ability verification, there is positive effect to relating to the related side of detection/calibration:
For laboratory, be that it meets ISO/IEC 17025 standards, carry out the needs that internal quality control and external ability prove;
To accreditation body, it is the important technology approach of evaluating accredited laboratory's detection/rated capacity;
To the client in laboratory, be to prove that laboratory possesses the important evidence of a certain detectability;
To responsible departments of the government, be the effective measures of supervision laboratory ability and level.
Because ability verification all has the effect of highly significant in many industries, thereby, no matter in the world still at home, all paid close attention to widely at present.
The matching requirements of functipnal capability checking meets the homogeneity that proficiency testing requires, and can in whole proficiency testing process, keep stable, is not defectively attributed between the device that functipnal capability verifies or the variability of device itself with what guarantee to occur in proficiency testing.This point is most important to whole ability verification, and it can directly have influence on the result of final activity.
In addition, the matching requirements of functipnal capability checking is convenient to transport, cost is lower, easy for operation etc., and these features all have very positive effect to the smooth running of ability verification.
The device that there is no functipnal capability checking in industry at present can be verified low-temperature test ability.In industry, only low-temperature test equipment is calibrated at present, the verification mode of generally taking is according to relevant low-temperature test equipment calibrating standard, adopts the mode of the sensor combinations such as temperature polling instrument and platinum resistance or thermopair to calibrate low-temperature experimental device.There is following shortcoming in this mode: 1) proficiency testing equipment energy characteristic point can not be set, in the application, mainly refer to operating temperature point, certain specific temperature value at place when certain action occurs device, common low-temperature test equipment Alignment device can not arrange fixing operating temperature point, cannot obtain fixing temperature and read a little, therefore cannot be to participating in the laboratory implementation ability verification of proficiency testing; 2) said apparatus exists that cost is high equally, volume is large, transport inconvenient problem, the low-temperature test equipment Alignment devices such as said temperature logging at least several thousand, up to ten thousand at most, so expensive correcting device should not be used for carrying out ability verification, common low-temperature test equipment Alignment device belongs to high-accuracy electronic equipment, be not suitable for common logistics transportation, if adopt special logistics, further can improve the cost of ability verification.
Summary of the invention
First goal of the invention of the present invention is to provide a kind of method of electric and electronic product low-temperature test proficiency testing.
Another goal of the invention of the present invention is to provide a kind of low-temperature test proficiency testing device that utilizes said method to complete low-temperature test proficiency testing.
Realizing the technical scheme that first goal of the invention of the present invention takes is: a kind of method of electric and electronic product low-temperature test proficiency testing, and it comprises the following steps:
1) operating temperature of preset temperature pick-up unit point, requires the temperature sensing medium rate temperature change≤1 ℃/min of temperature-detecting device, the temperature sensing device of temperature-detecting device is put into device to be verified inner, opens device operation cooling to be verified;
2) in the time that temperature-detecting device detects that the internal temperature of device to be verified drops to above-mentioned default operating temperature point, record device to be verified internal temperature values now, record unit temp value to be verified;
3) calculate the Z value of above-mentioned unit temp to be verified,
when |, judge that device low-temperature test ability to be verified is qualified when Z|≤the 2.
Step 3) described in median, standard I QR value obtain in the following way: select 18 above devices to be verified carry out step 1 respectively), 2) correspondingly obtain 18 above unit temp values to be verified, calculate median and the standard I QR value of above-mentioned 18 above unit temp values to be verified.
Described temperature-detecting device is the electric temperature regulator compression-type temperature controller with fixing operating temperature point.
The present invention fully analyzes the requirement of the device to functipnal capability checking in low-temperature test ability verification, a kind of method of low-temperature test proficiency testing is provided, realize the technical breakthrough of low-temperature test being carried out to proficiency testing, enrich the quality control method in laboratory, improved laboratory ability and level.
Realizing the technical scheme that second goal of the invention of the present invention take is: a kind of low-temperature test proficiency testing device, comprise the compression-type temperature controller with fixing operating temperature point, on described temperature controller, be connected with temperature sensing device, the negative voltage input end of described temperature controller connects outside negative voltage input end by resistance, neon lamp successively, and the positive voltage input end of described temperature controller connects outside positive voltage input end.
The present invention also comprises box body, and described temperature controller is sealed in box body, and described temperature sensing device passes box body and is connected with external world's device to be verified, and described neon lamp, outside positive and negative voltage input end are arranged on box body.
Temperature controller of the present invention is the electric temperature regulator compression-type temperature controller with fixing operating temperature point, and temperature sensing medium rate temperature change≤1 of described temperature controller ℃/min.
As specific embodiments of the invention, described temperature sensing device is kapillary temperature-sensing probe.
The present invention adopts the compression-type temperature controller with fixing operating temperature point, meets the requirement of low-temperature test ability verification to matching requirements energy set temperature characteristic point; Temperature sensing medium rate temperature change≤1 ℃/min, in gradual change low-temperature test, can make response to the temperature variation of low temperature environment fast; Adopt electric temperature regulator compression-type temperature controller, can better meet the requirement of proficiency testing device to stability and repdocutbility; This apparatus structure is simple simultaneously, and volume is little, can be controlled in 0.004m
3left and right, and device inner structure is simply firm, and each components and parts also can stand common Transport Vibration, and cost is low, and convenient transportation is applicable to ability verification; Itself carries temperature indicating device compression-type temperature controller, and data read conveniently.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the present invention will be further described:
Fig. 1 is the circuit theory diagrams of low-temperature test proficiency testing device of the present invention;
Fig. 2 is the circuit theory connection layout that uses low-temperature test proficiency testing device of the present invention.
Embodiment
As shown in Figure 2, low-temperature test proficiency testing device of the present invention, comprise the compression-type temperature controller 6 with fixing operating temperature point, on described temperature controller 6, be connected with temperature sensing device 3, the negative voltage input end 2 of described temperature controller 6 connects outside negative voltage input end N by resistance R, neon lamp 4 successively, and the positive voltage input end 1 of described temperature controller 6 connects outside positive voltage input end L; Described outside negative voltage input end N is a black binding post, and outside positive voltage input end L is a red binding post; The present invention also comprises box body 5, described temperature controller 6 is sealed in box body 5, described temperature sensing device 3 passes box body 5 and is connected with external world's device to be verified, described neon lamp 4, outside positive and negative voltage input end L, N are arranged on box body 5, and the temperature sensing device in the present embodiment is kapillary temperature-sensing probe.
Temperature controller 6 selects to have the electric temperature regulator compression-type temperature controller of fixing operating temperature point, temperature sensing medium rate temperature change≤1 ℃/min.
Between the red binding post L of low-temperature test proficiency testing device of the present invention (also can select other temperature-detecting devices of the condition of defined in meeting method invention) and black post head N, load 220V ± 5%, (resistance of resistance R is R=120K Ω left and right to the alternating current of 50Hz ± 1%, circuit lead cross-sectional area: 1.0mm), as shown in Figure 2, the concrete steps of utilizing the method disclosed in the present and device to realize low-temperature test proficiency testing are:
1) the operating temperature point of the temperature controller 6 of default low-temperature test proficiency testing device is T1, the temperature range of T1 is from-10 ℃ to-70 ℃, the temperature-sensing probe 3 of low-temperature test proficiency testing device is put into device experiment case 7 to be verified, open chamber 7, start cooling from normal temperature;
2) in the time that temperature controller 6 detects that the internal temperature of chamber 7 drops to above-mentioned default operating temperature point T1, when observing neon lamp 4 and extinguishing, record neon lamp 4 and extinguish flash test case 7 internal temperature values now, record unit temp value to be verified;
3) calculate the Z value of above-mentioned unit temp to be verified,
adopt robust statistics Z than fraction method, the unit temp value to be verified of record to be processed, when |, judge that device experiment case 7 low-temperature test abilities to be verified are qualified, and then judge that validation laboratory of institute has the ability of carrying out low-temperature test when Z|≤the 2.
Above-mentioned steps 3) described in median, standard I QR value obtain in the following way: select the device to be verified of 18 above (being generally more than 20) carry out step 1 respectively), 2) correspondingly obtain 18 above unit temp values to be verified, median and the standard I QR value of calculating above-mentioned 18 above unit temp values to be verified, standard I QR value is standardization interquartile range.
Be the experimental data of low-temperature test proficiency testing device of the present invention below:
The uniformity testing report of device
According to the designing requirement of this device, each 100 of customized 1# sample (low-temperature test proficiency testing device) and 2# sample, therefrom randomly draw respectively 12 for uniformity testing, totally 24 samples, each sample repeated test 2 times.
Sample homogeneity assay data:
1# sample:
Sample number into spectrum |
Test value 1 (℃) |
Test value 2 (℃) |
1 |
-15.31 |
-15.46 |
2 |
-15.00 |
-15.00 |
3 |
-15.43 |
-15.34 |
4 |
-15.28 |
-15.25 |
5 |
-15.53 |
-15.46 |
6 |
-15.40 |
-14.93 |
7 |
-15.46 |
-14.93 |
8 |
-15.25 |
-15.56 |
9 |
-15.34 |
-15.65 |
10 |
-15.65 |
-15.45 |
11 |
-15.43 |
-15.32 |
12 |
-15.46 |
-15.64 |
2# sample:
Sample number into spectrum |
Test value 1 (℃) |
Test value 2 (℃) |
1 |
-23.37 |
-23.09 |
2 |
-23.49 |
-23.15 |
3 |
-23.38 |
-23.28 |
4 |
-22.85 |
-23.07 |
5 |
-23.49 |
-23.77 |
6 |
-22.72 |
-23.15 |
7 |
-23.43 |
-23.65 |
8 |
-23.43 |
-23.15 |
9 |
-23.87 |
-23.21 |
10 |
-23.81 |
-23.34 |
11 |
-23.09 |
-22.81 |
12 |
-23.15 |
-23.06 |
Sample homogeneity check analysis result:
1# sample one-way analysis of variance result
1.69<F
0.05(11,12)=2.72
The F statistics value calculating is less than F critical value, shows in the time of 0.05 level of significance, and low-temperature test testing cassete 1# sample operating temperature is uniform.
2# sample one-way analysis of variance result
2.24<F
0.25(11,12)=2.72
The F statistics value calculating is less than F critical value, shows in the time of 0.05 level of significance, and low-temperature test testing cassete 2# sample operating temperature is uniform.
Conclusion: low-temperature test proficiency testing device of the present invention meets uniformity requirement.
The test of low-temperature test proficiency testing device of the present invention to chamber, seemingly tests about the requirement of " test Ab: the low-temperature test of non heat dissipating specimen temperature gradual change " in standard according to GB/T 2423.1-2008 " electric and electronic product environmental test part 2: test method test A: low temperature ", IEC 60068-2-1:2007 " Environmental testing-Part 2-1:Tests-Test A:Cold " (Chinese is " environmental test-2-1 part: test-test A: low temperature ") or other associated class.
The service condition of low-temperature test proficiency testing device of the present invention:
Use this device to carry out CNAS T0436 and T0530 totally 2 ability verifications, there are respectively 123 and 170 laboratories to participate in proficiency testing, shown in specifically seeing the following form, median and the uniformity testing test value of all chamber test results of participating in the experiment are basically identical, prove that this device has good practicality.
CNAS T0436 statistics
CNAS T0530 statistics
Apparatus of the present invention are simple in structure, and reusable more than 200,000 times cost is low, and volume is little, and convenient transportation is very suitable for various ability verifications.
The above embodiment of the present invention is not limiting the scope of the present invention; embodiments of the present invention are not limited to this; according to foregoing of the present invention; according to ordinary skill knowledge and the customary means of this area; do not departing under basic fundamental thought prerequisite of the present invention; modification, replacement or the change of other various ways that said structure of the present invention is made, within all dropping on protection scope of the present invention.