CN102490228B - Method for processing fireproof flame retardant bamboo, wood, hemp and grass and curtain made of fireproof flame retardant bamboo, wood, hemp and grass - Google Patents
Method for processing fireproof flame retardant bamboo, wood, hemp and grass and curtain made of fireproof flame retardant bamboo, wood, hemp and grass Download PDFInfo
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- CN102490228B CN102490228B CN201110413917.0A CN201110413917A CN102490228B CN 102490228 B CN102490228 B CN 102490228B CN 201110413917 A CN201110413917 A CN 201110413917A CN 102490228 B CN102490228 B CN 102490228B
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Abstract
The invention discloses a method for processing fireproof flame retardant bamboo, wood, hemp and grass and a curtain made of the fireproof flame retardant bamboo, wood, hemp and grass. The method comprises the following steps of: processing the bamboo and the wood into a threadlike or strip-type structure; performing bleaching treatment; performing first drying treatment; performing flame retardant treatment; performing second drying treatment; and performing a flame retardant experiment, wherein a finished product is used as a manufacturing material of the curtain after the experiment is qualified. The invention also discloses the bamboo and the wood which are prepared by the method for processing the fireproof flame retardant bamboo and wood, and a bamboo and wood curtain and door curtain which are made of the bamboo and the wood. The invention has the advantages that: in the flame retardant treatment process, a flame retardant is fully invaded into the inside of the bamboo through repeated pressurization, constant pressure and pressure reduction treatment; and a hard flame retardant layer is formed on a surface layer, so that the flame retardant performance of the curtain is greatly improved. By combining the two drying processes before and after flame retardant treatment, guarantee is provided for the invasion of the flame retardant and the coagulation of the flame retardant on the surface layer. Dyeing and the bleaching treatment before the dyeing step are performed after the first drying treatment step, so that colors of the curtain are bright and can be kept for a long time; and the long-lasting performance of fire safety is further improved through the flame retardant treatment after the dyeing step.
Description
Technical field
The present invention relates to a kind of fire protection flame retarding bamboo and wood, fiber crops, the processing method of grass and curtain for door or window, curtain or the decorative curtain be made up of this bamboo and wood, fiber crops, grass, and floor or bed, chair surface, pad etc.
Background technology
The living standard of present people is more and more higher, house is the demand of people's rigidity, anyone can have this demand, but house is when finishing, use chemical substance more and more, can distribute a series of chemical element in these chemical substance use procedures, these elements belong to pollution-free a bit.But some really belongs to high pollution, therefore people start to focus on environmental protection, focus on the product using environmental protection.Bamboo wood fiber crops wait product to belong to natural prodcuts, do not have radiation, also can not distribute pollution element, belong to a kind of environmental protection article, and people can also be allowed to produce a kind of sensation of access expansion, the product that these raw materials are made has used a lot of place, such as curtain, floor or bed chair etc.But this this product itself all belongs to combustibles, fire hazardous is held in improper use at home, and the article that special curtain and so on is thinner, the possibility of igniting is higher.Therefore, when this series products of making, the fire resistance of product be considered.Patent Office of the People's Republic of China discloses a CN1457964A document on November 26th, 2003, name is called a kind of flame-retardant shaped bamboo material and production method thereof, first bamboo wood deep-sawing is become bamboo chip, again every sheet bamboo chip is placed in that anticorrisive agent leaching is full carries out boiling preservative treatment, then dried bamboo chip is cutd open well-thought-out plan silk, then bamboo silk is placed in the fire resistant fluid be made into by phosphoric acid ester, boric acid or borax soaks.Then carry out dehydration to drain, the bamboo silk of drying afterwards containing fire resistant fluid is placed in waterproof binding agent immersion, drying; Dry bamboo wire material containing fire resistant fluid is placed in mould and carries out compression sizing, then mould is placed in dry kiln, the demoulding after overcuring cooling and shaping.This process is through multiprogramming, exist and cut open system twice, and preservative treatment generally can form anticorrosive coat on bamboo chip surface, but differ and penetrate into bamboo chip inside surely, like this bamboo chip after preservative treatment is made bamboo silk, just may make inside do not have preservative treatment to position be exposed to outside completely, then this position preservative treatment formation hot spot not in place when making product, may be caused, thus the performance that impact is overall.
The curtain made with bamboo and wood, fiber crops, grass or door curtain, owing to drawing materials extensively, super quality and competitive price, both artistic and practical, and be used widely.Be subject to the inflammability the subject of knowledge and the object of knowledge limit of material, must combustion-supporting process be carried out, to improve the performance of its fire-retardant fireproof.Due to flame-proof treatment method Problems existing, the fire resistance of the material that existing bamboo and wood, fiber crops, straw screen or mat adopt is poor, limits it to a certain extent and applies.
Summary of the invention
The curtain that the present invention aims to provide a kind of fire protection flame retarding bamboo and wood, fiber crops, careless processing method and makes thus, with the problem that the fire resistance solving the bamboo wood that prior art exists is poor.
Technical scheme of the present invention is: the processing method of a kind of fire protection flame retarding bamboo and wood, fiber crops, grass, is characterized in that, comprise the following steps:
(1), bamboo wood is processed into thread or banded structure;
(2), first time dry process;
(3), flame treatment: material is put in the stainless steel tank of the sealing filling fire retardant, the pressure gradually in raising groove, and step-down after keeping pressure time enough;
(4), the dry process of second time;
(5), carry out fire-retardant experiment, test the qualified rear making material as curtain.
After described step (1), carry out bleaching, the bleaching agent that this bleaching uses is hydrogen peroxide, and the concentration mixed with water is 12-20mol/l, and water temperature is 60-95 DEG C, bleaching time 30-90min.
After described step (1) or bleaching, carry out dyeing process, be first added in water by dyestuff, the temperature of aqueous dye solutions controls at 50-130 DEG C, is immersed by material in dye solution, and the time of immersion determines according to the requirement to shade.
Described flame treatment step (3), is immersed in 24-36 hour in retardant solution by material at ambient pressure.
When carrying out described flame treatment step (3), the pressure gradually in raising groove is to 0.08-0.1MPa, and pressure rising time is 35-45min, and maintenance pressure time is 50-70min, and the time of step-down is 10-15min.
The process of described boosting-maintenance pressure-step-down is carried out 1-3 time.
Described first time, the method for operating of dry treatment step (2) was: by the bamboo of bleach wood in layer place on the top of the shelf, be separated from each other between layers, the temperature of drying controls at 45-70 DEG C, and the residual moisture of drying controls at 8%-12%.
The method of operating of described fire-retardant experimental procedure (5) is: be 45o angle by the bamboo wood after process with flame, and keep 5cm with flame, burning time is 120s, and the diameter in the region of burning that bamboo wood burns is not more than 50mm.
In flame treatment and dried material surface scribbles japanning.
A kind of described processing method prepare bamboo and wood, fiber crops, grass.
A kind of described bamboo and wood, fiber crops, the grass curtain made by more than one material wherein and door curtain.
Advantage of the present invention is: in flame retardant treatment process, adopts repetitious pressurization, constant voltage and step-down process, makes fire retardant invade the inside of bamboo wood fully, and forms firm flame-retardant layer on top layer, substantially increase its fire resistance.In conjunction with twice dry run before and after flame treatment, for the intrusion of fire retardant with on top layer, cohesion provides guarantee.Dye after first time dry process, and bleaching before, make painted bright-coloured, permanent, flame treatment thereafter further increases painted permanence.
It is the product meeting security against fire requirement.
Accompanying drawing explanation
Fig. 1 is the process chart of the first embodiment of the present invention;
Fig. 2 is the process chart of the second embodiment of the present invention;
Fig. 3 is the process chart of the third embodiment of the present invention;
Fig. 4 is the process chart of the fourth embodiment of the present invention.
Detailed description of the invention
See Fig. 1-Fig. 4, the processing method of a kind of fire protection flame retarding bamboo of the present invention wood, is characterized in that, comprise the following steps:
1, first raw material are processed into filament, size after processing meets the size of curtain processing, the dimensions length of such as bamboo chip is 160,190,260 or 320mm, generous is 6mm × 1.2mm, 7mm × 1.8mm, 12mm × 1.8mm, the length of bamboo silk is 130mm, 160mm, 190mm, 260mm, 320mm, bamboo filament diameter is 2.5,1.8 or 1.2mm, and wooden louvres sheet width 2.5-5mm.These sizes are determined according to the size of curtain, generally according to thickness and the width of curtain, considers that the width of bamboo is to form various striped simultaneously; These materials also can be timber, grass (rope) or fiber crops material.
2, bleaching (material very white for quality or need to retain the material of primary colors also can save this step, see Fig. 1 and Fig. 3); Bleaching is carried out to the material after above-mentioned processing, bleaching is to be processed into by bamboo wood material not containing the material of natural pigments, simultaneously by bleaching the sugared part can removed former bamboo and produce in growth course, or remove the foreign material being attached to bamboo material surface, keep bamboo wood material consistency of colour and clean.
Bleaching agent uses hydrogen peroxide, and the time standby temperature of bleaching is the water of 60-95 DEG C, and the time of bleaching will be kept to be 50-90min simultaneously.Hydrogen peroxide is used to make bleaching, play the effect of oxidation bleaching, simultaneously still a kind of preservative treatment, prevent final products because the reason of former bamboo itself is easily mouldy, keeping the clean of curtain, using when bleaching the water with uniform temperature to be sugared part in order to remove former bamboo inside.The concentration of the hydrogen peroxide used during bleaching controls at 12-20mol/l.It is suitable that the concentration of hydrogen peroxide will control, and concentration is too high, and easily by the fiber destruction of former bamboo inside, the too low effect can not playing again bleaching oxidation of concentration, the concentration of hydrogen peroxide also can change according to the age difference of former bamboo to some extent.
3, first time dry process; Carried out drying (water content 8-12%) by material after bleaching, in layer put on the top of the shelf by the bamboo wood material after bleaching, be separated from each other between layers, dry temperature controls at 45-70 DEG C, and dry residual moisture controls at 8%-12%.Time dry, by bamboo layers of material, make to be separated from each other between layers, fully dry, can not dead angle be left, ensure dry effect.
4, before drying and flame treatment, carrying out dyeing process (needs the material retaining primary colors also can save this step, see Fig. 1 and Fig. 2), first deployed pigment is added in water, water temperature controls at 50-130 DEG C, be immersed in pigment water by the material after bleaching (drying), the time of immersion determines according to the requirement to shade.Need primary drying after dyeing process, drying means is dry identical with first time.
5, again the material of oven dry is carried out flame treatment: put into by the material of oven dry and fill in the stainless steel locked groove of fire retardant, apply pressure with height gradually, and keep enough time step-down; The pressure of closed container inside is improved gradually, then pressurize step-down again.After this process, the fire retardant in closed cell penetrates into bamboo material internal under the effect of the pressure, thus improves the fire resistance of bamboo wood material, improves flame retardant effect.The osmotic effect of fire retardant can be improved by the increase of pressure, make the thickness of the permeable formation of fire retardant comparatively large, thus ensure the fire resistance of final products; The fire retardant used has more selection, and can be domestic product, also can be external product, or can be the product mix of multiple different flame retardant or catalyst, and this generally selects according to the thickness of bamboo or the performance that will reach.
During flame treatment, raised pressure is to 2-4.5MPa gradually, and the time controling of boosting is at 35-45min, and the time controling of pressurize is at 50-79min, and the time controling of last step-down is at 10-15min.The pressure of pressurize, time determine according to the size of bamboo chip or bamboo silk, and the surface area of bamboo chip is larger, the pressure of use can higher while pressurize time also can proper extension.
The process of 1-3 boosting-pressurize-step-down is carried out in flame treatment.Repeatedly repeat this process, be the thickness of the permeable formation in order to deepen fire retardant as far as possible, or form a kind of stacked flame-retardant layer structure on the surface of bamboo wood material.
It is phosphorus-nitrogen (Phospphorus-nitrogen) compound that fire retardant adopts from a kind of chemical name of Japanese import, and trade name is NON-NEN 984.Another kind of chemical name is Sulfer-halogen compound, and trade name is NON-NEN R028-8.Manufacturer is MARUBISHI OIL CHEMICAL CO.LTD(manufacturer address: 2-11 RINKAI-CHO IZUMIOTSU-SHI OSAKA JAPAN).
5, second time drying method is dry identical with first time.
6, fire-retardant experiment is carried out:
Dried material carries out fire retardancy test, and described fire-retardant experimental procedure is: the material after process is made curtain, and be 45o angle with flame, and keep 5cm with flame, burning time is 120s, and the diameter in the region of bamboo wood burning or turning white is not more than 50mm.This is the mode of experiment and the data of requirement of experiment, and reaching these objects is exactly qualified products.If do not meet the requirements of data, need to re-start fire retardant infiltration process.
The bamboo and wood of said method process, fiber crops, grass is adopted conventionally to prepare series connection or are woven into curtain, door curtain or other articles for use.
Claims (2)
1. a processing method for fire protection flame retarding bamboo and wood, fiber crops, grass, is characterized in that, comprise the following steps:
(1), bamboo and wood, fiber crops, grass are processed into thread or banded structure;
(2), first time dry process;
(3), flame treatment: material is put in the stainless steel tank of the sealing filling fire retardant, the pressure gradually in raising groove, and step-down after keeping pressure time enough;
(4), the dry process of second time;
(5), carry out fire-retardant experiment, test the qualified rear making material as curtain;
When carrying out described flame treatment step (3), the pressure gradually in raising groove is to 2-4.5 MPa, and pressure rising time is 35-45min, and maintenance pressure time is 50-70min, and the time of step-down is 10-15min;
The process of described boosting-maintenance pressure-step-down is carried out 1-3 time;
After described step (1), carry out bleaching, the bleaching agent that this bleaching uses is hydrogen peroxide, and the concentration mixed with water is 12-20mol/l, and water temperature is 60-95 DEG C, bleaching time 30-90min;
After bleaching, carry out dyeing process, be first added in water by dyestuff, the temperature of aqueous dye solutions controls at 50-130 DEG C, is immersed by material in dye solution, and the time of immersion determines according to the requirement to shade;
Described first time, the method for operating of dry treatment step (2) was: by bamboo and wood bleach, fiber crops, careless in layer place on the top of the shelf, be separated from each other between layers, dry temperature controls at 45-70 DEG C, and dry residual moisture controls at 8%-12%;
The method of operating of described fire-retardant experimental procedure (5) is: be 45o angle by the bamboo and wood after process, fiber crops, grass and flame, and keep 5cm with flame, burning time is 120s, and the diameter in the region of burning that material burns is not more than 50mm;
In flame treatment and dried material surface scribbles japanning.
2. the bamboo and wood prepared by processing method according to claim 1, fiber crops, a grass, and curtain made by this bamboo and wood, fiber crops, grass more than one material wherein and door curtain.
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CN201110413917.0A CN102490228B (en) | 2011-12-13 | 2011-12-13 | Method for processing fireproof flame retardant bamboo, wood, hemp and grass and curtain made of fireproof flame retardant bamboo, wood, hemp and grass |
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CN201110413917.0A CN102490228B (en) | 2011-12-13 | 2011-12-13 | Method for processing fireproof flame retardant bamboo, wood, hemp and grass and curtain made of fireproof flame retardant bamboo, wood, hemp and grass |
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CN102490228A CN102490228A (en) | 2012-06-13 |
CN102490228B true CN102490228B (en) | 2015-01-07 |
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CN201110413917.0A Expired - Fee Related CN102490228B (en) | 2011-12-13 | 2011-12-13 | Method for processing fireproof flame retardant bamboo, wood, hemp and grass and curtain made of fireproof flame retardant bamboo, wood, hemp and grass |
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CN104015241B (en) * | 2014-06-25 | 2017-02-15 | 湖北楚风竹韵科技有限公司 | Production method of mould-proof, anti-bacterial and flame-retardant wall decoration bamboo curtain |
CN107336310B (en) * | 2017-07-07 | 2019-04-05 | 戴海泉 | Bamboo and wood fireproof treatment method |
CN110973970A (en) * | 2019-12-27 | 2020-04-10 | 杭州富阳望月竹制品有限公司 | Non-joint bamboo curtain and its making process |
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CA2217086A1 (en) * | 1996-10-22 | 1998-04-22 | Masahiro Funato | Method of impregnating wood with liquid |
CN1730254A (en) * | 2005-07-31 | 2006-02-08 | 戴海泉 | Making and treating method for bamboo splint for fabricating bamboo rolling screen |
CN1864956A (en) * | 2006-06-15 | 2006-11-22 | 庄启程 | Method for manufacturing flame-retardant recombined decorative material |
CN101637352A (en) * | 2008-07-31 | 2010-02-03 | 蔡范恩 | Bamboo curtain and preparation process thereof |
CN102102228A (en) * | 2010-12-29 | 2011-06-22 | 戴海泉 | Method for processing fibers used for curtain |
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Publication number | Priority date | Publication date | Assignee | Title |
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JP2557780B2 (en) * | 1993-01-19 | 1996-11-27 | 株式会社マキノン | Method and apparatus for injecting treatment liquid into wood and porous inorganic material, and method for breaking radial soft cell wall and closed wall pores of wood |
CN101327606A (en) * | 2008-07-16 | 2008-12-24 | 赵盛源 | Method for processing five-prevention lumber |
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Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2217086A1 (en) * | 1996-10-22 | 1998-04-22 | Masahiro Funato | Method of impregnating wood with liquid |
CN1730254A (en) * | 2005-07-31 | 2006-02-08 | 戴海泉 | Making and treating method for bamboo splint for fabricating bamboo rolling screen |
CN1864956A (en) * | 2006-06-15 | 2006-11-22 | 庄启程 | Method for manufacturing flame-retardant recombined decorative material |
CN101637352A (en) * | 2008-07-31 | 2010-02-03 | 蔡范恩 | Bamboo curtain and preparation process thereof |
CN102102228A (en) * | 2010-12-29 | 2011-06-22 | 戴海泉 | Method for processing fibers used for curtain |
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