CN102433737A - Histidine-lysine combination strengthening method of rotten silk fabrics - Google Patents
Histidine-lysine combination strengthening method of rotten silk fabrics Download PDFInfo
- Publication number
- CN102433737A CN102433737A CN2011102378764A CN201110237876A CN102433737A CN 102433737 A CN102433737 A CN 102433737A CN 2011102378764 A CN2011102378764 A CN 2011102378764A CN 201110237876 A CN201110237876 A CN 201110237876A CN 102433737 A CN102433737 A CN 102433737A
- Authority
- CN
- China
- Prior art keywords
- histidine
- lysine
- aqueous solution
- rotten
- silk goods
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004472 Lysine Substances 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000004744 fabric Substances 0.000 title claims abstract description 16
- 238000005728 strengthening Methods 0.000 title abstract description 4
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000007864 aqueous solution Substances 0.000 claims abstract description 14
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 claims abstract description 14
- 230000002787 reinforcement Effects 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 10
- 239000002131 composite material Substances 0.000 claims description 9
- 239000007921 spray Substances 0.000 claims description 5
- 239000000126 substance Substances 0.000 abstract description 4
- 238000005507 spraying Methods 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 1
- HNDVDQJCIGZPNO-YFKPBYRVSA-N L-histidine Chemical compound OC(=O)[C@@H](N)CC1=CN=CN1 HNDVDQJCIGZPNO-YFKPBYRVSA-N 0.000 description 11
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 description 11
- 229960002885 histidine Drugs 0.000 description 10
- 235000018977 lysine Nutrition 0.000 description 9
- 108010022355 Fibroins Proteins 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 235000019766 L-Lysine Nutrition 0.000 description 1
- 229940024606 amino acid Drugs 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000413 hydrolysate Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000012460 protein solution Substances 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000001771 vacuum deposition Methods 0.000 description 1
Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a histidine-lysine combination strengthening method of rotten silk fabrics, comprising the following steps: A), flatting a rotten silk fabric, then uniformly spraying a histidine aqueous solution having a concentration of 0.5-2 wt% on the surface of the rotten silk fabric until the silk fabric is uniformly drenched through with the histidine aqueous solution to drip; B), at 10 min after completing the step A), spraying a lysine aqueous solution having a concentration of 0.5-2 wt% on the surface of the silk fabric until the silk fabric is uniformly drenched through with the lysine aqueous solution, naturally drying to strengthen the rotten silk fabric. Compared with the prior art, the invention has the advantage of convenient operation; because of no need of other chemical auxiliaries except for histidine and lysine, the strength of the fabrics can be effectively increased, and the original characteristics of the fabrics are not affected.
Description
Technical field
The present invention relates to a kind of silk historical relic's protection method, particularly a kind of histidine-lysine composite reinforcement method of poor rotten silk goods.
Background technology
At present; Both at home and abroad the reinforcement means to poor rotten silk goods mainly contain chucking method, mount the holder method, resin method for strengthening, silk gum method for strengthening, Pai Lalun Vacuum Coating method, grafting copolymerization process etc.; But all there is certain defective in these methods, and it is used and has also received great restriction.Silk-fibroin reinforcing project by Institutes Of Technology Of Zhejiang cooperates with the China Silk Museum has been developed the research that fibroin albumen is reinforced fragile silk; But cumbersome and difficult storage of the preparation of silk fibroin protein solution and transportation, people's expectation simultaneously has the reinforcement means without other chemical assistant.
Summary of the invention
The object of the present invention is to provide a kind of histidine-lysine composite reinforcement method of poor rotten silk goods, is a kind of reinforcement means efficiently that has easily and effectively, and this reinforcement means is simple to operate, and is low to environment requirement, and room temperature condition gets final product down.It is reinforcement material that the present invention selects the hydrolysate amino acid of protein for use, at ambient temperature the silk historical relic is reinforced, and through experimental study repeatedly, the compound of L-histidine and L-lysine has significant consolidation effect.The present invention does not need other chemical assistant except that histidine-lysine, the ultimate strength and the elongation at break of the fragile silk behind this composite reinforcement of process all are significantly improved, and to the almost not influence of silk goods primary characteristic.A kind of histidine-lysine composite reinforcement method of poor rotten silk goods is characterized in that adopting following steps:
A) will be pickled with grains or in wine after rotten silk goods divide, evenly spray mass percentage concentration on its surface and be 0.5%～2% the histidine aqueous solution, evenly drenched by the histidine aqueous solution and till dripping to silk goods;
B) completing steps A) behind the 10min, the sprinkling mass percentage concentration is 0.5%～2% lysine solution on fabric, and is evenly drenched by lysine solution to silk goods, air dry, and poor rotten silk goods obtain to reinforce.
Compared with prior art, advantage of the present invention has: 1) easy to operate; 2) the present invention does not need other chemical assistant except that histidine lysine, can effectively improve fabric intensity, to the almost not influence of silk goods primary characteristic.
The specific embodiment
Embodiment 1:
A kind of histidine-lysine composite reinforcement method of poor rotten silk goods is characterized in that adopting following steps:
A) will be pickled with grains or in wine after rotten silk goods divide, evenly spray mass percentage concentration on its surface and be 0.5% the histidine aqueous solution, evenly drenched by the histidine aqueous solution and till dripping to silk goods;
B) completing steps A) behind the 10min, the sprinkling mass percentage concentration is 2% lysine solution on fabric, and is evenly drenched by lysine solution to silk goods, air dry, and poor rotten silk goods obtain to reinforce.
Embodiment 2:
A kind of histidine-lysine composite reinforcement method of poor rotten silk goods is characterized in that adopting following steps:
A) will be pickled with grains or in wine after rotten silk goods divide, evenly spray mass percentage concentration on its surface and be 2% the histidine aqueous solution, evenly drenched by the histidine aqueous solution and till dripping to silk goods;
B) completing steps A) behind the 10min, the sprinkling mass percentage concentration is 0.5% lysine solution on fabric, and is evenly drenched by lysine solution to silk goods, air dry, and poor rotten silk goods obtain to reinforce.
Embodiment 3:
A kind of histidine-lysine composite reinforcement method of poor rotten silk goods is characterized in that adopting following steps:
A) will be pickled with grains or in wine after rotten silk goods divide, evenly spray mass percentage concentration on its surface and be 1.3% the histidine aqueous solution, evenly drenched by the histidine aqueous solution and till dripping to silk goods;
B) completing steps A) behind the 10min, the sprinkling mass percentage concentration is 1.3% lysine solution on fabric, and is evenly drenched by lysine solution to silk goods, air dry, and poor rotten silk goods obtain to reinforce.
Claims (1)
1. histidine-lysine composite reinforcement the method for poor rotten silk goods is characterized in that adopting following steps:
A) will be pickled with grains or in wine after rotten silk goods divide, evenly spray mass percentage concentration on its surface and be 0.5%～2% the histidine aqueous solution, evenly drenched by the histidine aqueous solution and till dripping to silk goods;
B) completing steps A) behind the 10min, the sprinkling mass percentage concentration is 0.5%～2% lysine solution on fabric, and is evenly drenched by lysine solution to silk goods, air dry, and poor rotten silk goods obtain to reinforce.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110237876 CN102433737B (en) | 2011-08-18 | 2011-08-18 | Histidine-lysine combination strengthening method of rotten silk fabrics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110237876 CN102433737B (en) | 2011-08-18 | 2011-08-18 | Histidine-lysine combination strengthening method of rotten silk fabrics |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102433737A true CN102433737A (en) | 2012-05-02 |
| CN102433737B CN102433737B (en) | 2013-07-10 |
Family
ID=45982074
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110237876 Expired - Fee Related CN102433737B (en) | 2011-08-18 | 2011-08-18 | Histidine-lysine combination strengthening method of rotten silk fabrics |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102433737B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05171568A (en) * | 1991-12-24 | 1993-07-09 | Agency Of Ind Science & Technol | Fixing of sericin of raw silk fiber |
| CN101338516A (en) * | 2008-07-28 | 2009-01-07 | 浙江理工大学 | Fibroin atomization strengthening method for fragile silk fabrics |
| CN101424042A (en) * | 2008-11-03 | 2009-05-06 | 浙江理工大学 | Fibroin reinforcement process of fragile silk |
| CN101487189A (en) * | 2008-11-03 | 2009-07-22 | 浙江理工大学 | Fibroin reinforcement process of fragile silk |
-
2011
- 2011-08-18 CN CN 201110237876 patent/CN102433737B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05171568A (en) * | 1991-12-24 | 1993-07-09 | Agency Of Ind Science & Technol | Fixing of sericin of raw silk fiber |
| CN101338516A (en) * | 2008-07-28 | 2009-01-07 | 浙江理工大学 | Fibroin atomization strengthening method for fragile silk fabrics |
| CN101424042A (en) * | 2008-11-03 | 2009-05-06 | 浙江理工大学 | Fibroin reinforcement process of fragile silk |
| CN101487189A (en) * | 2008-11-03 | 2009-07-22 | 浙江理工大学 | Fibroin reinforcement process of fragile silk |
Non-Patent Citations (1)
| Title |
|---|
| 郑海玲等: "丝素蛋白/戊二醛对脆弱丝绸织物加固的工艺条件研究", 《蚕业科学》, no. 3, 15 September 2009 (2009-09-15), pages 576 - 582 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102433737B (en) | 2013-07-10 |
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