CN102371128A - Apparatus for carrying out mass-transfer processes in heterogeneous systems - Google Patents

Apparatus for carrying out mass-transfer processes in heterogeneous systems Download PDF

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Publication number
CN102371128A
CN102371128A CN2011101853879A CN201110185387A CN102371128A CN 102371128 A CN102371128 A CN 102371128A CN 2011101853879 A CN2011101853879 A CN 2011101853879A CN 201110185387 A CN201110185387 A CN 201110185387A CN 102371128 A CN102371128 A CN 102371128A
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China
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container
gas
conveyance conduit
unit
equipment
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谢尔盖·亚历山德罗维奇·布奇克
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  • Devices For Dispensing Beverages (AREA)
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Abstract

The invention relates to the apparatus for carrying out mass-transfer processes and can be used for carrying out processes of gas dispersion in liquid with attendant mass-transfer processes, for example for carrying out gas-liquid reactions, absorption in food, pharmaceutical and other branches of industry. The technical result of the claimed technical solution is in increasing stable gas content in a final product and increasing productivity of the device operation during carbonization of liquids capable of foaming. The apparatus includes means for supplying the components into a container (7) under pressure, comprising a mechanism of the leakproof split connection to it a throat of the container (7) and an assembly for dispersion of the components in the container (7), a unit of control of the supplying the components into the container (7), which is connected to the means for supplying the components into the container (7) under pressure and to a channel (29 or 35 or 37) of gas bleeding from the container (7) into the atmosphere through a controllable throttle valve (9) and is made with the possibility of connecting to a pipeline (4) of the gas supply under pressure or to a pipeline (6) of the liquid supply under pressure and with the possibility of supplying to the means for supplying the components into the container (7) or gas under pressure, or liquid under pressure with simultaneous providing the gas bleeding from the filled container (7), or blocking the pipelines (4 and 6) of the gas supply under pressure and the liquid supply under pressure, respectively.

Description

Be used for carrying out the equipment of material exchange process at heterogeneous system
Technical field
Present invention relates in general to be used to carry out the equipment of material exchange process, and the present invention is used for utilizing material exchange process to dispense a gas onto liquid, particularly, is used for carrying out gas-liquid reactions and absorption in food, medicine and other industry.
Background technology
Liquid, particularly saturated water and the beverage that contains carbon dioxide or oxygen, known have a following characteristic: distinctive and pleasant taste, the effect of refreshing oneself and foaming (acutely and bubbling enduringly).Oxygen has treatment and prevention effect to histanoxia.Carbon dioxide has Anticorrosive Character, thereby has improved the shelf stable property of beverage.Carbonation method (carbonation) is through importing carbon dioxide machinery and be dissolved in the liquid (Jiu Heshui of carbonated fruit beverage, mineral water, carbonated or bubbling) or saturated naturally realization of beverage through having the carbon dioxide of being separated out by fermentation (bottled and the champagne of natural carbonation (acratophore), grape wine, applejack, beer and the bread Ge Wasi of foaming).In first method, after liquid and is removed air precooling, under the pressure of beverage in particular device (saturator, natural carbonation device (acratophores) or metal can) by carbonation.The saturation degree of carbon dioxide or oxygen reaches 5 to 10g/L in the beverage.In some cases, clarifying beer receives compulsory carbonation, the promptly saturated carbon dioxide that contains.In forcing carbonated method, edible CO 2 is ordered about through being contained in the beer in the gas-tight container under pressure.In the former Soviet Union, identical thought is implemented to be used for homemade carbonated beverage with siphon pipe.Because the pressure carbonation is very suitable for making the beer of filtration and because it has better adaptability, in the most modern winery, uses such carbon dioxide saturation process.
Known the whole bag of tricks is used to make hold-up to contain gas.A kind of method comprises carbon dioxide is supplied in a large amount of water.Carbon dioxide gas ducks in drink to generate then and rises, and gas is dissolved in the water.This method is widely used in the carbonated device that is used for feeding water (saturator automatically), and is suitable for preparing the carbonated water (one glass) of relatively small amount.Saturator comprises saturated chamber, be used for water section ground fill saturated chamber to setting height device, be used for carbon dioxide supply to saturated chamber device, be installed in be used to stir water in the saturated chamber so that this water saturation contain carbon dioxide device, be used for discharging the device of excess air pressure and the device that is used for the water of dispense either carbonated gas from saturated chamber.The designs that is used to discharge excess air pressure is the gas release valve that is connected to saturated chamber; And comprise and be connected to the device of gas noise that this gas release valve is used to reduce release (referring to WO2002/081067; IPC:B01F 3/04, open day: on October 17th, 2002).
The major defect of this device comprises following aspect: need be needed the additional stirring device by for the carbonation for the liquid of more volume; Further, this device does not provide finished product is packaged into the container that is used to distribute to consumer and/or storage (transportation) with 0.5 to 3 liter amount, for example, is packaged in the PET bottle of plastics.
Another kind method comprises atomized water is ejected in the ambiance of carbon dioxide.In the method, saturated chamber is filling arbon dioxide at first, then water injection is arrived in this chamber.Carbon dioxide is dissolved in the water droplet, and these water droplets carry in the pond of carbon dioxide dissolved entering accumulation then.This saturator comprises: degasification column jecket (column), saturated column jecket and the stable column jecket installed in order, and each column jecket all has gas hollow bulb and air hollow bulb; Be used for removing the pipeline of air from the degasification column jecket; Be used to supply water to the pipeline of degasification column jecket and saturated column jecket; Be used to make water saturation to contain the unit of carbon dioxide; Be used to device that carbonated water and syrup are mixed mutually; Connecting line; Be used for carbon dioxide is supplied to the pipeline of saturation unit; Saturated column jecket and stable column jecket; Be used to shift out the pipeline of finished beverage; And (referring to Russ P No.2163081, IPC:A23L 2/54, and B01F 3/04, open day: February 20 calendar year 2001) to be installed in valve in above-mentioned each pipeline.This saturator is provided with at least one extra carbon dioxide supply pipeline; So that utilize the pump of wherein installing to carry out additional stirring; This pipeline connects the liquid hollow portion and the gas hollow bulb of saturated column jecket and/or stable column jecket; Wherein the import of pump is connected to the gas hollow bulb of relevant column jecket, and is installed in the valve that beverage shifts out in the pipeline and is designed to pressure controller.
Yet this device has complicated structure and needs independent workshop to prepare carbonated liquid; In addition, this device does not provide finished product directly is packaged into volume is 0.5 to 3 liter container, and the PET bottle of plastics for example is so that be sold to consumer and/or storage (transportation).
Become known for preparing and providing the device of cocktail (for example oxygen cocktail); This device comprises the housing, the device that foams that have the liquid reservoir that is used for foaming liquid, have supply device, the dispensing pump of air supply valve and be installed in the agitator that has power driver in the liquid reservoir (referring to Russ P No.2059401; IPC:A47J43/12, open day: on May 10th, 1996).Here, liquid reservoir is positioned on the housing with the foaming device, and dispensing pump gets into the hole through it and is connected to liquid reservoir and is connected to the foaming device through its injection orifice; This device has spring-loaded handle, and this handle is mounted to bar portion (stem) interaction with air supply valve and dispensing pump.
Yet this device has complicated structure; Further, this device does not provide finished product directly is packaged into volume is 0.5 to 3 liter container, for example is packaged into the PET bottle of plastics, so that be sold to consumer and/or storage (transportation).
A kind of device that is used to prepare carbonated water is (referring to Russ P No.2008773; IPC:A23L2/00; Open day: on March 15th, 1994) comprising: the circle tube tank of sealing, this circle tube tank had flat bottom and are used to supply with water and carbon dioxide and be used to extract the joint (nipple) of carbonated water; Be installed in the shutoff control valve on the joint; Be installed in the allocation units on the carbon dioxide supply joint; And the water that is used to supply with pressurization and carbon dioxide are also carried the device of the carbonated water that is connected to relevant joint.The saturated degree that contains carbon dioxide increases in the water in order to make; This device is provided with the device that is used to prevent that gas phase from forming, and this device is installed in the circle tube tank and comprises chamber, and wherein sidewall is made for flexible and has the folding line of collapsible type; And its end wall is made for rigidity; And this device is provided with the unit that chamber is compressed to fully zero volume, and this unit is designed to helical spring, in the bottom that this spring is attached to jar one and be connected in the end wall of chamber; To compress its sidewall through an end wall is moved towards another end wall, wherein said another end wall is attached on the bottom relative with compression unit of jar; The joint that is used for supplying with water and carbon dioxide and is used to export carbonated water is installed in this end wall of chamber; And the designs that is used to supply with pressure (hydraulic) water becomes to be used to provide enough big pressure to make it adapt to the volume of supply water to overcome helical spring power and chamber is expand into.This device is assigned to carbonated beverage in the container of threaded cap type.
Yet; Because this device is used for the carbonated water of preparation under null-gravity state; This device comprises the unit (being provided with band fold chamber, the polybag in container for drink and some other structure member of spring) with labyrinth; Material exchange process takes place under the situation of insufficient strength, and is used for that container neck is fastened to the container that the unit of conveyance conduit do not allow just be filled and is connected to saturator apace, and separates from saturator.
Become known for making the hold-up that is contained in the container to contain the device (family expenses saturator) of gas, this device is provided with the lid that is used for container, in lid injection pipeline through unidirectional counterbalance valve be provided with the device that is used to install the Compressed Gas gas collecting jar with ground-on cover plate and combine and turn-off.This unit is included in the gas flow controller under the supply pressure effect.In this unit, the air-flow decelerator is installed, gas gets into this air-flow decelerator from gas collecting jar with ground-on cover plate.Sealing gasket is connected to said lid or unit, with the connecting portion between the injection pipeline that is used for closing cap and the outlet (referring to United States Patent(USP) No. 49991400, IPC:A23L2/00, the day for announcing is on March 12nd, 1991).
Another kind is used for the carbonated device of the liquid that is contained in container (being used for carrying out carbonated equipment through importing carbon dioxide to liquid) is comprised the closing cap on the neck that is threaded onto container; The nozzle that is used for injected gas; This nozzle passes the hole in the closing cap and is connected to gas collecting jar with ground-on cover plate through locked plug-in unit; The import of nozzle of wherein leading to the lid of sealing is sealed (referring to United States Patent(USP) No. 4927569, IPC:B 01F 3/04, the day for announcing is March 22 nineteen ninety).
The shortcoming of these devices is the wherein insufficient strength of mass exchange.This can not make the gas content in the liquid increase significantly.The container neck fastening unit can not make container neck connect apace or separate, thereby has reduced the output of this saturator.
A kind of being used for to liquid carbonation that is contained in container and the device of packing; This device comprises beaker (beaker); Closing cap is installed in the said beaker, and the gas injection nozzle is installed in the beaker and through locked plug-in unit and is connected to gas collecting jar with ground-on cover plate, it is characterized in that; Beaker is made for flexible and places on the closing cap; This closing cap is threaded onto on the neck of container so that between the bottom of the neck end of container and lid, exist and is used for gas and gets into the gap (referring to Russ P No.2065281, IPC:A23L2/00, on August 20th, 1996) in the container.The elasticity beaker is provided with lip ring (O shape ring).Be used for the slit that gas passes through and cross the inner surface that screw thread is formed on closing cap.
The shortcoming of said apparatus is, when large quantities of containers that have liquid during by carbonation, this device can not provide the output of desired carbonation fluid product and desired package reliability.Because gas is made a bet at atmospheric pressure and is mapped in the liquid mass exchange insufficient strength that takes place in this saturator.This can not make the remarkable increase of the gas content in the liquid.
Maximally related prior art is a kind of being used for liquid carbonation that is contained in container and the device of packing; This device comprises that beaker, O shape ring, gas supply pipe road and the closure means that there be closing cap the location in it are (referring to Russ P No.2167560; IPC:A23L 2/00, open day: May 27 calendar year 2001).The movable rod that beaker is provided with the attaching nut (union nut) who is used for fixing O shape ring and has the attachment that is used to catch closing cap.Beaker is provided with the guard shield between the edge that is installed in beaker and the O shape ring.Closure means be designed to be mounted to can with the interactional valve of movable rod.The gas supply pipe road is connected to beaker through joint, and the lining on the gas supply pipe road is mounted to can the rotation of solderless wrapped connection head.
The shortcoming of this device is that being designed for of saturator directs injection of the gas in the container that is filled with liquid, owing to the little contact area that forms between gas phase and the liquid phase, has reduced the possibility of a large amount of injected gases thus.The carbonated water that produces or other beverage that is mixed with carbon dioxide or oxygen can not be satisfactory aspect a lot; Unstable during their storages; And carbon dioxide is discharged from gas/aqueous mixtures relatively quickly, thus during slowly drinking most gas/aqueous mixtures air inclusion no longer all.When beverage when for example beer (its initial package carbonated) is by carbonation, owing to when container is pre-charged with beer and when gas is expelled in the beverage, produce foam, the output of this device reduces significantly.
Summary of the invention
Require the technique effect that technical scheme obtained of protection to comprise: to increase the content of the stabilizing gas in the finished product, and improved the output of equipment aspect the foaming liquid carbonation.
Above-mentioned technique effect is realized in the equipment of heterogeneous system execution material exchange process through following being used for; It is characterized in that; Said equipment comprises: be used for the device of each component forced feed to container, said device comprises that the neck that is used for said container detachably is closely connected to the unit of said equipment and the unit that is used for each component is assigned to said container; Be used to control the unit of each component to said supply for receptacles; Said control module is connected to said being used for each component forced feed to the device of container and be connected to and be used for the pipeline of gas being discharged into the atmosphere from said container through controllable throttle valve; Said control module is designed to be connected to the pressurized gas supply pipe or is connected to the fluid under pressure supply pipe; So that gas-pressurized or fluid under pressure are supplied to the device that is used for each component forced feed is arrived container, can gas be discharged from the container that just is being filled simultaneously and perhaps turn-off said pressurized gas supply pipe and said fluid under pressure supply pipe.
Be used to control component can be designed to have threeway disc type cock spool (three-way disk cock cartridge) from handle control to the unit of supply for receptacles; The inlet pipeline of said threeway disc type cock spool is connected to gas supply pipe and feed tube for liquid, and the outlet conduit of said threeway disc type cock spool is connected to said container through conveyance conduit.
Saidly be used to control component and can be designed to two valves that have handle control to the unit of supply for receptacles, the inlet pipeline of said valve is connected respectively to gas supply pipe and feed tube for liquid, and the outlet conduit of said valve is connected to said container through conveyance conduit.
The said neck that is used for said container detachably is closely connected and can comprises an elastic annular sealing gasket and a spoon shape spare to the unit of said equipment; Said sealing gasket is installed around the outlet opening of said conveyance conduit coaxially; Said spoon shape spare has handle and groove; The size of said groove and bottleneck size are complementary; The cylindrical shape of its dessertspoon shape spare partly centers on said conveyance conduit arranges so that have rotation and reciprocating ability, and in the wall of conveyance conduit, has the helical groove of perforation, is attached to the wall of the cylindrical shape part of said spoon shape spare through pin in said helical groove middle roller.
The said neck that is used for said container detachably is closely connected and can comprises an elastic annular sealing gasket and a spoon shape spare to the unit of said equipment; Said sealing gasket is installed around the outlet opening of said conveyance conduit coaxially; Said spoon shape spare has handle and groove; The size of said groove and the size of bottleneck are complementary, and the cylindrical shape of wherein said spoon shape spare partly is connected to the wall of said conveyance conduit so that have reciprocating ability around said conveyance conduit layout and through threaded joints with moving.
The unit that component is assigned in the said container is designed to nozzle; The axial perforation pipeline that said nozzle has the inlet pipeline that is connected to choke valve and is used for gas is discharged into the atmosphere from container; Said nozzle has helical groove on the cylinderical surface of sidepiece, said nozzle is installed in the exit of conveyance conduit.
Said component is assigned to the pipeline that unit in the said container is designed to towards the crooked pipe of the inner surface of chamber wall and is used for gas is discharged into the atmosphere from container; The crooked pipe of said inner surface towards chamber wall is installed in the place, end of said conveyance conduit, and said being used for is connected to the pipeline that gas is discharged into the atmosphere from container the inlet pipeline of choke valve and arranges along conveyance conduit.
Said component is assigned to the pipe that unit in the said container is designed on the outer surface side of its end, have annular rim; The said pipe that has annular rim is installed in the exit of conveyance conduit and has the gap with respect to the wall of conveyance conduit, and wherein the axial perforation pipeline of pipe is used for the inlet pipeline that releases the gas into atmosphere and be connected to choke valve.
This design of equipment (saturator) can at first be arrived container with pressurized gas supply; Then through releasing the gas into atmosphere so that liquid to supply to container as these forms of distribution of the film that flows down along chamber wall; Thereby make the contact area between liquid and the gas increase significantly, and strengthened the dissolving of gas in liquid.Here, owing to formed gas pressure on the liquid mirror in equipment and in container has been eliminated foaming, this pressure is greater than the saturation pressure that is dissolved in the gas in the beverage and prevent that liquid from " boiling " occurring (boiling).The component allocation units are supplied with beverage with the form of the film on chamber wall, thereby reduce foaming.
Being used for detachably the be closely connected unit of equipment of neck with container provides fast a kind of and reliably container has been connected or spaced manner, thereby has improved the output of saturator equipment.
Description of drawings
This device will be illustrated through accompanying drawing.
Fig. 1 shows the sketch map that is used for carrying out at heterogeneous system the equipment of material exchange process, and wherein control module is embodied as two vent pathway (vents).
Fig. 2 shows the sketch map that is used for carrying out at heterogeneous system the equipment of material exchange process, and wherein control module is designed to threeway disc type cock spool, and allocation units are designed to helical member.
Fig. 3 shows the sketch map that is used for carrying out at heterogeneous system the equipment of material exchange process, and wherein control module is designed to threeway disc type cock spool, and allocation units are designed to have and are used for the pipe of flow of liquid towards the edge of chamber wall deflection.
Fig. 4 shows the sketch map that is used for carrying out at heterogeneous system the equipment of material exchange process, and wherein control module is designed to threeway disc type cock spool, and allocation units are designed for the bend pipe unit of flow of liquid towards chamber wall deflection.
Fig. 5 shows the A-A cross section among Fig. 1, and it is the cross section of passing the neck and the unit that equipment detachably is closely connected that are used to make container.
Fig. 6 shows the B-B cross section among Fig. 1, and it is to pass another cross section that is used to make the neck of container and the unit that equipment detachably is closely connected.
The specific embodiment
The equipment that is used for carrying out at heterogeneous system material exchange process comprises: housing 1, this housing have conveyance conduit 2, be connected to pipe 4 so that from the pipeline 3 of gas collecting jar with ground-on cover plate supply gas and be connected to pipe 6 so that supply with the pipeline 5 of beverage from equipressure tank; Be used for the device of each component forced feed to container 7, this device comprises the unit of the outlet of the conveyance conduit 2 that is used for the equipment that detachably is closely connected, and this unit is installed on the housing 1 around the sidewall 8 of the conveyance conduit 2 of the neck of container 7; Be used for each component is assigned to the unit of said vesse 7; And be installed in the housing 1 and have the choke valve 9 of inlet hole 10.The unit that is used for each component is assigned to container 7 is installed in the conveyance conduit 2.Be used for controlling each component in first embodiment of the unit that container 7 is supplied with (shown in Fig. 1); The pipeline 3 and 5 that is connected to gas supply pipe 4 and beverage supplying pipe 6 is connected to conveyance conduit 2 through independent vent pathway 11 and 12 respectively, and said vent pathway 11 and 12 is installed in the hollow bulb 13 in the housing 1 of equipment.Here, for example, pipeline 3 is connected to hollow bulb 13 through vent pathway 11, and pipeline 5 is connected to hollow bulb 13 (Fig. 1) through vent pathway 12.
Be used for controlling each component in second embodiment of the unit that container 7 is supplied with (Fig. 2); The pipeline 3 and 5 that is connected to gas supply pipe 4 and beverage supplying pipe 6 is connected to conveyance conduit 2 through threeway disc type cock spool 14 respectively, and said threeway disc type cock spool is installed in the housing 1 of equipment.Three-way cock 14 comprises manual operating handle 15, and said manual operating handle is connected to the upper movable dish 16 of cock (cock).Here, for example, pipeline 3 is connected to the inlet hole of cock 14, and pipeline 5 is connected to the inlet hole 18 of this cock, and conveyance conduit 2 is connected to the outlet opening (not shown go out) of cock 14 (Fig. 2).
Being used for the unit (Fig. 1,2) that neck and equipment with container 7 detachably is closely connected comprising: elastic annular sealing gasket 19, and the sealing pad is attached coaxially around the outlet opening of conveyance conduit 2; And; The spoon shape spare 20 that has joystick 21 and groove 22; This groove has the size that the size with the neck of container 7 is complementary; The cylindrical shape part 23 of its dessertspoon shape spare centers on the sidewall 8 of conveyance conduit 2 arranges so that can move back and forth, and has the helical groove of in this wall, processing that does not connect 24, and roller 25 is installed in the wall that is attached to the cylindrical shape part 23 of spoon shape spare 20 in this helical groove and through pin 26.The groove 22 of spoon shape spare is arranged in the front (Fig. 5 and 6) of the outlet opening of conveyance conduit 2.In second embodiment of this unit (Fig. 3), the cylindrical shape part 23 of spoon shape spare 20 is connected to above-mentioned wall around sidewall 8 layouts of conveyance conduit 2 and through threaded portion 27 with moving.
The unit (Fig. 1 and 2) that is used for each component is assigned to container 7 is designed to nozzle 28; This nozzle has and is used for axial perforation pipeline 29 that gas is discharged into the atmosphere from container 7; Should axially connect the inlet pipeline 30 that pipeline is connected to choke valve 9; Nozzle has helical groove 31 on the cylinderical surface of its sidepiece, and is installed in the exit of conveyance conduit 2.
(Fig. 3) in another embodiment; Be used for the unit that each component is assigned to container 7 is designed on the outer surface side of its end, have the pipe 32 of annular rim 33; This pipe is installed in the exit of conveyance conduit; And the wall with respect to conveyance conduit has gap 34, and the axial pipeline 35 of wherein managing is used for releasing the gas into atmosphere and is connected to the inlet pipeline 30 of choke valve 9.
In the 3rd embodiment (Fig. 4); Be used for the unit that each component is assigned to container 7 is designed to towards the crooked pipe 36 and the pipeline 37 that is used for gas is discharged into the atmosphere from container 7 of inner surface of the wall of container 7; This pipe 36 is installed in the place, end of conveyance conduit 2, and said pipeline 37 is connected to the inlet pipeline 30 of choke valve 9 and is arranged near the conveyance conduit 2.
This is used for operating as follows at the equipment of heterogeneous system execution material exchange process.
Container 7 is set to the groove 22 of the spoon shape spare 20 that is used for making the neck of container 7 and the unit that equipment detachably is closely connected, and fits closely to the end of conveyance conduit 2 by means of elastic annular sealing gasket 19 through rotary handle 21.Now, choke valve 9 cuts out.Be used for each component forced feed to the vent pathway 11 of first embodiment (Fig. 1) of the device of container 7 and 12 and be used for each component forced feed all in the closed position to the handle 15 of the three-way cock 14 of second embodiment (Fig. 2) of the device of container 7.Then, open vent pathway 11 (Fig. 1) so that gas supply pipe line 4 is communicated with the inner space of container 7 through pipeline 3, hollow bulb 13, conveyance conduit 2 and helical groove 31; The upper disc 16 that perhaps makes handle 15 and three-way cock 14 (Fig. 2) is (counterclockwise) rotation 45 degree together, so that inlet hole 17 and outlet opening, conveyance conduit 2 and helical groove 31 that gas line 4 passes through pipeline 3, cock 14 are communicated with the inner space of container 7.At this moment, gas (for example carbon dioxide or oxygen) gets into container 7, and the pressure in the pressure in container and the isobaric storage tank (not shown go out) equates.Then, vent pathway 11 is closed and vent pathway 12 is opened (Fig. 1), so that liquid line 6 is communicated with the inner space of container 7 through pipeline 5, hollow bulb 13, conveyance conduit 2 and helical groove 31; Perhaps with the upper disc 16 of handle 15 and three-way cock 14 (Fig. 2) together in opposite direction (counterclockwise) revolve and turn 90 degrees so that inlet hole 18 and outlet opening, conveyance conduit 2 and helical groove 31 that beverage line 6 is passed through pipeline 5, cock 14 are communicated with the inner space of container 7.Because the pressure in the container 7 equates that with the pressure in the isobaric storage tank liquid does not get into said vesse 7.When choke valve 9 was opened, gas (carbon dioxide or oxygen) got in the atmosphere through the hole 10 compelled containers 7 that leave that axial gas discharges pipeline 29 (Fig. 1 and 2) or axial gas release pipeline 35 (Fig. 3) or gas discharge tube road 37 (Fig. 4) and choke valve 9.The pressure reduction that produces between isobaric storage tank and the container 7 makes liquid get into container 7 and filling containers.At liquid under the situation of the helical groove 31 (Fig. 1 and 2) through joint 28; Liquid through the centrifugal force feeding in case on the wall of the neck of container 7, form cone shape film or liquid through annular rim 33 (Fig. 3) deflection or liquid through bend pipe 36 (Fig. 4) deflection towards the inner surface of container 7, saturatedly then contain gas and do not flow down reposefully along wall of a container with not foaming.Through in allocation units, going up gas pressure (about 1.5 to 3.5 atmospheric pressure that form with the liquid mirror (liquid mirror) of container 7; On the order of 1.5-3.5at) further eliminate foaming, this pressure is greater than the saturation pressure that is dissolved in the gas in the beverage.After the liquid that contains dissolved gases therein is filled in the container 7, further supply with for stop liquid, close vent pathway 12 (Fig. 1) or make handle 17 and the upper disc 16 (Fig. 2) of three-way cock 14 together (counterclockwise) rotation 45 spend to get back to its initial position.Residual gas in container 7 necks is through the axial perforation pipeline 29 of nozzle 28, the inlet pipeline 30 and the outlet opening 10 (Fig. 1 and 2) of choke valve 9; Perhaps discharge the inlet pipeline 30 and the outlet opening 10 (Fig. 3) of pipeline 35, choke valve 9 through axial gas; Perhaps pass through the inlet pipeline 30 and the outlet opening 10 of gas discharge tube road 37, choke valve 9, and be discharged in the atmosphere.Pressure in container 7 is with after atmospheric pressure equates, handle 21 along opposite direction rotation so that the neck of the end of conveyance conduit 2 and container 7 separate; Container is removed from equipment (saturator), and plug is good also to be consigned to the consumer or send to storage.The gas saturation of liquid is the 6-9 grams per liter.Oxygen cocktail, carbonated beverage, carbonated mineral water and carbonation drinking water and carbonation beer all can be produced by this way.
Therefore; The present invention has obtained beyond thought technique effect; Promptly owing to compare the saturation conditions of formation container 7 under high pressure (1.5 to 3.5 atmospheric pressure) more with existing equipment; Improved the content of the stabilizing gas in the finished product, and made the mode of the film that the liquid that has gas flows down with the inner surface along container 7 supply to container 7 by means of the component allocation units, this has increased the contact area between liquid and the gas phase significantly and has strengthened the dissolving of gas in liquid significantly.Owing to form gas pressure in equipment and on the liquid mirror in the container greater than the saturation pressure that is dissolved in the gas in the beverage; Eliminate foaming further and prevent liquid " boiling ", the equipment that makes is improved in the output aspect the carbonation of foaming liquid.Be used for the neck of container is connected container fast with unit that equipment detachably is closely connected or separates, thereby this has further improved the output of saturator equipment.

Claims (8)

1. equipment that is used for carrying out material exchange process at heterogeneous system; Said equipment comprises: be used for the device of each component forced feed to container (7), said device comprises that the neck that is used for container (7) detachably is closely connected to the unit of said equipment and the unit that is used for each component is assigned to container (7); Be used to control the unit of each component to container (7) supply; Saidly be used to control each component and be connected to said being used for each component forced feed to the device of container (7) and be connected to and be used for the pipeline (29 of gas being discharged into the atmosphere from said container (7) through controllable throttle valve (9) to the unit that container (7) is supplied with; 35; 37); Saidly be used to control each component and be designed to be connected to pressurized gas supply pipe (4) or be connected to fluid under pressure supply pipe (6) to the unit that container (7) is supplied with; So that gas-pressurized or fluid under pressure are supplied to the device that is used for each component is supplied to said container (7), can gas be discharged from the container (7) that just is being filled simultaneously and perhaps turn-off said pressurized gas supply pipe (4) or said fluid under pressure supply pipe (6) respectively.
2. equipment as claimed in claim 1; It is characterized in that; Saidly be used to control each component is designed to have threeway disc type cock spool (14) from joystick (15) to the unit that container (7) is supplied with; Said threeway disc type cock spool is connected to gas supply pipe (4) and feed tube for liquid (6) by its inlet pipeline (3 and 5) respectively, and is connected to said container (7) by its outlet conduit through conveyance conduit (2).
3. equipment as claimed in claim 1; It is characterized in that; Saidly be used to control each component is designed to have two vent pathway (11 and 12) from joystick to the unit that container (7) is supplied with; Said two vent pathway are connected to gas supply pipe line (4) and feed tube for liquid line (6) by inlet pipeline (3 and 5) respectively, and are connected to said container (7) by the hollow bulb (13) and the conveyance conduit (2) of outlet conduit through housing (1).
4. equipment as claimed in claim 1; It is characterized in that; The said neck that is used for container (7) detachably is closely connected and comprises elastic annular sealing gasket (19) and spoon shape spare (20) to the unit of said equipment; Said sealing gasket is attached to the wall (8) of said conveyance conduit coaxially around the outlet opening of said conveyance conduit (2); Said spoon shape spare has joystick (21) and groove (22), and the neck size of the size of said groove and container (7) is complementary, and the cylindrical shape part (23) of wherein said spoon shape spare (20) centers on said conveyance conduit (2) layout and can rotate and move back and forth; And in the wall (8) of conveyance conduit, have the helical groove (24) that does not connect, roller (25) is installed in the wall that is attached to the cylindrical shape part (23) of said spoon shape spare (20) in the said helical groove and through pin (26).
5. equipment as claimed in claim 1; It is characterized in that; The said neck that is used for container detachably is closely connected and comprises elastic annular sealing gasket (19) and spoon shape spare (20) to the unit of said equipment; Said sealing gasket is attached coaxially around the outlet opening of conveyance conduit (2); Said spoon shape spare (20) has joystick (21) and groove (22), and the neck size of the size of said groove (22) and said container (7) is complementary, and the wall (8) that the cylindrical shape part (23) of wherein said spoon shape spare (20) is connected to said conveyance conduit around said conveyance conduit (2) layout and through threaded joints (27) with moving is so that can rotate and move back and forth.
6. equipment as claimed in claim 1; It is characterized in that; The said unit that is used for each component is assigned to container (7) is designed to nozzle (28); The axial perforation pipeline (29) that said nozzle has the inlet pipeline (30) that is connected to choke valve (9) and is used for gas is discharged into the atmosphere from said container (7), said nozzle has helical groove (31) on the cylinderical surface of sidepiece, and said nozzle is installed in the exit of conveyance conduit (2).
7. equipment as claimed in claim 1; It is characterized in that; The said pipeline (37) that the unit that each component is assigned to container (7) is designed to towards the crooked pipe (36) of the inner surface of chamber wall and is used for gas is discharged into the atmosphere from container (7) of being used for; The crooked pipe (36) of said inner surface towards chamber wall is installed in the place, end of conveyance conduit (2), and said being used for is connected to the pipeline (37) that gas is discharged into the atmosphere from container (7) inlet pipeline (30) of choke valve (9) and is provided with along said conveyance conduit (2).
8. equipment as claimed in claim 1; It is characterized in that; The said pipe (32) that is used for the unit that each component is assigned to container (7) is designed on outer surface side to have at its place, end annular rim (33); The said pipe (32) that has annular rim is installed in the exit of conveyance conduit (2) and has gap (34) with respect to the wall of conveyance conduit, and the wherein said axial pipeline (35) that has the pipe of annular rim is used for releasing the gas into atmosphere and is connected to the inlet pipeline (30) of choke valve (9).
CN2011101853879A 2010-07-12 2011-07-04 Apparatus for carrying out mass-transfer processes in heterogeneous systems Pending CN102371128A (en)

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EA201001054A EA014813B1 (en) 2010-07-12 2010-07-12 Apparatus for carrying out mass-transfer processes in heterogeneous systems
EA201001054 2010-07-12

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RU2694494C2 (en) * 2017-09-11 2019-07-15 Закрытое Акционерное Общество "Ленпродмаш" Saturator activated

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CA1092507A (en) * 1976-10-25 1980-12-30 Peter F. Haythornthwaite Carbonating apparatus
WO1990011122A1 (en) * 1989-03-29 1990-10-04 The Coca-Cola Company Buoyant tank carbonator pump control for post-mix beverage apparatus
WO1997025130A1 (en) * 1996-01-04 1997-07-17 International Home Beverage Supply Co., Inc. Carbonated beverage making apparatus and method
CA2261560A1 (en) * 1998-02-10 1999-08-10 Kautz, Peter Device for the impregnation of liquids with gases
DE19825559A1 (en) * 1998-06-08 1999-12-16 Privatbrauerei M C Wieninger G Oxygenation and carbonation of potable water, table water and mineral water
FR2799137A1 (en) * 1999-10-05 2001-04-06 Air Liquide Carbonation of beverage includes filling container with liquid at atmospheric pressure and carbonating it using solid carbon dioxide
EP1162167A1 (en) * 2000-06-09 2001-12-12 KHS Maschinen- und Anlagenbau Aktiengesellschaft Method and device for filling bottles, cans and similar containers with a liquid product

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EA201001054A1 (en) 2011-02-28
EA014813B1 (en) 2011-02-28

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Application publication date: 20120314