CN102337196A - Haematococcus alcoholic drink and preparation method thereof - Google Patents
Haematococcus alcoholic drink and preparation method thereof Download PDFInfo
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- CN102337196A CN102337196A CN2011102650091A CN201110265009A CN102337196A CN 102337196 A CN102337196 A CN 102337196A CN 2011102650091 A CN2011102650091 A CN 2011102650091A CN 201110265009 A CN201110265009 A CN 201110265009A CN 102337196 A CN102337196 A CN 102337196A
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- haematococcus pulvialis
- haematococcus
- astaxanthin
- pulvialis
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Abstract
The invention discloses a haematococcus alcoholic drink, which is characterized in that: haematococcus serves as a substrate of the alcoholic drink, and has the particle size of 1,000-3,000 meshes, the wall breaking rate of 75-95 percent and the astaxanthin content of 0.05-4.0 percent. The invention further discloses a preparation method of the haematococcus alcoholic drink. The haematococcus alcoholic drink has the advantages of keeping the bouquet, protecting an organism from being damaged by alcohol by using the contained natural astaxanthin substance and protecting health.
Description
Technical field
The present invention relates to nourishing function property Wine, specifically relate to a kind of haematococcus pulvialis Wine and preparation method thereof.
Background technology
Haematocoocus Pluvialls (
Haematococcus pluvialis) be a kind of common vetch algae of being rich in nutritive value and pharmaceutical use of after tenaculat Habenaria, chlorella, finding.Contain a large amount of Phycocyanins, C-s, β-Hu Luobusu in the Haematocoocus Pluvialls, wherein the content of astaxanthin accounts for 1.5%～3.0% of dried cell weight, is counted as " concentrate " of natural astaxanthin.Because natural astaxanthin has superpower anti-oxidant activity, its resistance of oxidation is 550～1000 times of vitamin E, is called as " super vitamin E ", also has anti-inflammatory properties simultaneously, is described as " hormone of being free from side effects ".
China Ministry of Health regulation was classified Haematocoocus Pluvialls as new resource food in 2010, can quantity-unlimitingly eat.Current research shows that natural astaxanthin is having outstanding effect aspect protection liver and the neural system, has the effect of the immunity regulated, alleviating fatigue.But do not see with the Haematocoocus Pluvialls to be the report of feedstock production Wine both at home and abroad, it is open also not have related patent U.S. Patent No..
Summary of the invention
The present invention is directed to the above-mentioned deficiency of prior art, providing a kind of is base-material with the haematococcus pulvialis, and the method that adopts basic steeping in wine to carry, blend is prepared the haematococcus pulvialis Wine with nourishing function.
In order to address the above problem, the technical scheme that the present invention adopts is: a kind of haematococcus pulvialis Wine, this Wine mainly are base-material with the haematococcus pulvialis.
The above-mentioned haematococcus pulvialis of the present invention is grinding particle size 1000～3000 orders, sporoderm-broken rate 75%～95%, content astaxanthin (weight percentage) is 0.05%～4.0% haematococcus pulvialis.
The above-mentioned haematococcus pulvialis of the present invention is without supercritical CO
2The greasy former algae of extraction astaxanthin, or be through supercritical CO
2Algae-residue behind the extraction astaxanthin grease.
A kind of preparation method of above-mentioned haematococcus pulvialis Wine: with the haematococcus pulvialis is base-material, and the method that adopts basic steeping in wine to carry, blend is prepared the natural astaxanthin Wine with nourishing function, and step comprises:
(1) be that < 5%, being ground into granularity then is 60～120 purpose meals through drying treatment to moisture content for 0.05%～4.0% haematococcus pulvialis with astaxanthin-containing;
(2) getting step (1) granularity then is that 60～120 purpose meals pass through the further broken wall treatment of wall-breaking machine, and obtaining granularity is that 1000～3000 orders, sporoderm-broken rate are 75%～95% haematococcus pulvialis powder;
(since after the haematococcus pulvialis results be blocky be that a plurality of frustules concentrate at together, according to the technical requirements of wall-breaking machine, raw material must be earlier through pulverizing and then broken wall treatment.The broken wall process nature is that the cell walls of single common vetch frustule is opened, and in the process of processing, is equivalent to and has carried out micronizing one time, belongs to industry routine techniques technology);
(3) get the haematococcus pulvialis powder of step (2); According to haematococcus pulvialis powder (g/ quality): basic wine (ml/ volume) is that the ratio of 1:50～500 (being that per 1 gram ultra micro haematococcus pulvialis powder adds 50～500 milliliters basic wine) soaks is lixiviate; Soak time is 2～12 hours, and the lixiviate number of times is to obtain vat liquor 2～5 times;
(4) merge (being about to 2～5 vat liquors merges) and filter vat liquor, obtain the wine extraction liquid of astaxanthin-containing;
(5) step (4) wine extraction liquid is mixed with deionized water, blend by the alcoholic strength of desiring to ask, process the haematococcus pulvialis Wine, the content of astaxanthin is 0.1～100 mg/L in this haematococcus pulvialis Wine.
The preparation method of the haematococcus pulvialis Wine that the present invention is above-mentioned can also can add different essence and sweeting agent (the industry those of ordinary skill can add as required voluntarily) as required.
The above-mentioned basic wine of the present invention can be to be selected from a kind of in gin, whisky, brandy, Lang Mu, vodka, the Folium Agaves variegatae, also can be the edible ethanol of Chemical Manufacture.
The above-mentioned basic wine alcoholic strength of the present invention is 10%～95%, and the high more effective constituent of alcoholic strength is leached more easily.
The present invention has the following advantages:
1. the natural astaxanthin in the haematococcus pulvialis powder is very easily leached by alcohol, and extracting efficiency is high; Can adopt CO
2The algae-residue that supercritical extraction astaxanthin grease process produces, resource reutilization has been practiced thrift cost; Product keeps the sweet-smelling of wine, and contained natural astaxanthin material can protect body to avoid the damage of alcohol again, reaches the purpose of health care.
2. the haematococcus pulvialis of the present invention's employing is powdery (being powdery before promptly carrying with basic steeping in wine again); Grinding particle size is at 1000～3000 orders; Sporoderm-broken rate is 75%～95%; Content astaxanthin is 0.05%～4.0% in the haematococcus pulvialis, and above-mentioned Powdered haematococcus pulvialis is prone in spirituous solution, disperse, effective constituent is prone to lixiviate and goes into basic wine; The haematococcus pulvialis cell walls is thicker, the stripping that wherein astaxanthin material can greater efficiency after technology for broken wall is handled.
3. haematococcus pulvialis according to the invention is without CO
2The greasy former algae of supercritical process extraction astaxanthin also can be for through CO
2Algae-residue behind the supercritical process extraction astaxanthin grease.Both are except that astaxanthin and fatty acid content are different, and all the other are as broad as long, can select to use low algae-residue of content astaxanthin or the higher former algae of content according to product demand; On the other hand, the recycling algae-residue can economize in raw materials.
4. the present invention adopts the alcohol lixiviate, can leach pure soluble substances a large amount of in the common vetch algae, and its composition to the human body beneficial is fully utilized, and has expanded its range of application greatly.The present invention utilizes that natural astaxanthin has better deliquescent characteristics in the haematococcus pulvialis in alcohol, is base-material with the haematococcus pulvialis especially, and the method that adopts basic steeping in wine to carry, blend is prepared the haematococcus pulvialis Wine with nourishing function.
Embodiment
Through embodiment the present invention is described in further detail below, but the present invention not only is confined to following examples.
Embodiment 1
Astaxanthin-containing be 1.0% haematococcus pulvialis after drying treatment, be ground into 60 purpose meals.Handle through technology for broken wall, getting granularity is that 2000 orders, sporoderm-broken rate are 90% haematococcus pulvialis powder again.Get above-mentioned haematococcus pulvialis powder 6g, the edible ethanol that adds 300ml 95% soaks, and carries out intermittence and stirs 2 hours, and the leach liquor of redness is collected in the container, and the edible ethanol that adds 200ml 95% again mixes with residue, lixiviate 1 hour.Once, residue is khaki color to repeat said process (soaking the back lixiviate earlier), and the astaxanthin composition is described, and lixiviate is complete.Merge vat liquor 700ml altogether behind the fine filtering, obtain being wine-colored astaxanthin wine dope.Get 100ml wine extraction liquid and add 430ml de-ionized tap water, can blend into alcoholic strength and be 18% astaxanthin Wine, the content astaxanthin in this astaxanthin Wine is 16 mg/L.
Embodiment 2
Astaxanthin-containing be 2.0% haematococcus pulvialis after drying treatment, be ground into 70 purpose meals.Handle through technology for broken wall, getting granularity is that 3000 orders, sporoderm-broken rate are 95% haematococcus pulvialis powder again.This algae powder is through CO
2Obtain the haematococcus pulvialis algae-residue of astaxanthin-containing 0.3% behind the supercritical extraction separation astaxanthin grease.Get this algae-residue 5g, the Rum that adds 200ml 50% soaks, and carries out intermittence and stirs 1 hour, the leach liquor of redness is received in the container Rum that adds 200ml 50% again mixes with residue, lixiviate 1 hour.Once, residue is khaki color to repeat said process (soaking the back lixiviate earlier), and the astaxanthin composition is described, and lixiviate is complete.Merge vat liquor 600ml altogether behind the fine filtering, the astaxanthin wine dope that obtains taking on a red color directly adds 1900ml de-ionized tap water, and can blend into alcoholic strength is 12% astaxanthin Rum beverage, and content astaxanthin is 6 mg/L in this astaxanthin Rum beverage.
Claims (6)
1. haematococcus pulvialis Wine, it is characterized in that: the base-material of this Wine is a haematococcus pulvialis.
2. haematococcus pulvialis Wine according to claim 1 is characterized in that: described haematococcus pulvialis is granularity 1000～3000 orders, sporoderm-broken rate 75%～95%, content astaxanthin is 0.05%～4.0% haematococcus pulvialis.
3. haematococcus pulvialis Wine according to claim 2 is characterized in that: said haematococcus pulvialis is without supercritical CO
2The extraction greasy former algae of astaxanthin or through supercritical CO
2Algae-residue behind the extraction astaxanthin grease.
4. the preparation method of the described haematococcus pulvialis Wine of claim 3, it is characterized in that: this concrete haematococcus pulvialis Wine preparation process comprises:
(1) be that < 5%, being ground into granularity then is 60～120 purpose meals through drying treatment to moisture content for 0.05%～4.0% haematococcus pulvialis with astaxanthin-containing;
(2) getting step (1) granularity then is that 60～120 purpose meals pass through the further broken wall treatment of wall-breaking machine, and obtaining granularity is that 1000～3000 orders, sporoderm-broken rate are 75%～95% haematococcus pulvialis powder;
(3) get the haematococcus pulvialis powder of step (2), according to haematococcus pulvialis powder (g/ quality): it is lixiviate that basic wine (ml/ volume) soaks for the ratio of 1:50～500, and soak time is 2～12 hours, and the lixiviate number of times is to obtain vat liquor 2～5 times;
(4) merge and filter vat liquor, obtain the wine extraction liquid of astaxanthin-containing;
(5) step (4) wine extraction liquid is mixed with deionized water, blend by the alcoholic strength of desiring to ask, process the haematococcus pulvialis Wine, the content of astaxanthin is 0.1～100 mg/L in this haematococcus pulvialis Wine.
5. the preparation method of haematococcus pulvialis Wine according to claim 4 is characterized in that: said basic wine is a kind of in gin, whisky, brandy, Lang Mu, vodka, Folium Agaves variegatae or the edible ethanol.
6. the preparation method of haematococcus pulvialis Wine according to claim 5 is characterized in that: said basic wine alcoholic strength is 10%～95%.
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| CN 201110265009 CN102337196B (en) | 2011-09-08 | 2011-09-08 | Haematococcus alcoholic drink and preparation method thereof |
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| CN 201110265009 CN102337196B (en) | 2011-09-08 | 2011-09-08 | Haematococcus alcoholic drink and preparation method thereof |
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| CN102337196A true CN102337196A (en) | 2012-02-01 |
| CN102337196B CN102337196B (en) | 2013-06-26 |
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| CN 201110265009 Expired - Fee Related CN102337196B (en) | 2011-09-08 | 2011-09-08 | Haematococcus alcoholic drink and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103191089A (en) * | 2013-03-29 | 2013-07-10 | 李树森 | Novel astaxanthin heath-care wine and preparation method thereof |
| CN107312695A (en) * | 2017-08-24 | 2017-11-03 | 中国科学院海洋研究所 | A kind of astaxanthin wine and its preparation and Special-purpose wine bottle |
| CN109735419A (en) * | 2019-02-26 | 2019-05-10 | 中铭生物科技(深圳)有限公司 | A kind of manufacturing method of astaxanthin advocaat |
| CN112592795A (en) * | 2020-12-18 | 2021-04-02 | 唐建华 | Astaxanthin red wine and brewing method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1405294A (en) * | 2002-11-03 | 2003-03-26 | 陈克拉 | Wine for modulating immune from gene of ancient organism at deep sea and its production method |
| CN101381337A (en) * | 2007-09-03 | 2009-03-11 | 陈锦猜 | Astaxanthin extraction method |
-
2011
- 2011-09-08 CN CN 201110265009 patent/CN102337196B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1405294A (en) * | 2002-11-03 | 2003-03-26 | 陈克拉 | Wine for modulating immune from gene of ancient organism at deep sea and its production method |
| CN101381337A (en) * | 2007-09-03 | 2009-03-11 | 陈锦猜 | Astaxanthin extraction method |
Non-Patent Citations (1)
| Title |
|---|
| 王艳: "小球藻合成虾青素的应用前景", 《食品工业科技》, vol. 28, no. 12, 31 December 2007 (2007-12-31), pages 230 - 232 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103191089A (en) * | 2013-03-29 | 2013-07-10 | 李树森 | Novel astaxanthin heath-care wine and preparation method thereof |
| CN107312695A (en) * | 2017-08-24 | 2017-11-03 | 中国科学院海洋研究所 | A kind of astaxanthin wine and its preparation and Special-purpose wine bottle |
| CN107312695B (en) * | 2017-08-24 | 2020-11-03 | 中国科学院海洋研究所 | Shrimp protein wine and preparation and special wine bottle thereof |
| CN109735419A (en) * | 2019-02-26 | 2019-05-10 | 中铭生物科技(深圳)有限公司 | A kind of manufacturing method of astaxanthin advocaat |
| CN112592795A (en) * | 2020-12-18 | 2021-04-02 | 唐建华 | Astaxanthin red wine and brewing method thereof |
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| CN102337196B (en) | 2013-06-26 |
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