CN102322969A - High-temperature testing probe, device and method for entrained flow gasifier - Google Patents

High-temperature testing probe, device and method for entrained flow gasifier Download PDF

Info

Publication number
CN102322969A
CN102322969A CN201110149570A CN201110149570A CN102322969A CN 102322969 A CN102322969 A CN 102322969A CN 201110149570 A CN201110149570 A CN 201110149570A CN 201110149570 A CN201110149570 A CN 201110149570A CN 102322969 A CN102322969 A CN 102322969A
Authority
CN
China
Prior art keywords
probe
high temperature
temperature
temperature test
gasification furnace
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201110149570A
Other languages
Chinese (zh)
Other versions
CN102322969B (en
Inventor
梁钦锋
刘海峰
龚欣
于广锁
王辅臣
王亦飞
许建良
郭晓镭
代正华
李伟锋
陈雪莉
周志杰
王兴军
郭庆华
刘霞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
East China University of Science and Technology
Original Assignee
East China University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by East China University of Science and Technology filed Critical East China University of Science and Technology
Priority to CN201110149570.3A priority Critical patent/CN102322969B/en
Publication of CN102322969A publication Critical patent/CN102322969A/en
Application granted granted Critical
Publication of CN102322969B publication Critical patent/CN102322969B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E20/00Combustion technologies with mitigation potential
    • Y02E20/16Combined cycle power plant [CCPP], or combined cycle gas turbine [CCGT]
    • Y02E20/18Integrated gasification combined cycle [IGCC], e.g. combined with carbon capture and storage [CCS]

Abstract

The invention discloses a high-temperature testing probe for an entrained flow gasifier. The high-temperature testing probe comprises a hollow barrel-shaped probe main body, a measuring inner core, at least one gas clamping layer and a plurality of thermocouples, wherein the at least one gas clamping layer is arranged at the outer side of the probe main body, the measuring inner core is embedded at an end part of the probe main body as a measuring surface, a cooling chamber is also arranged at the inner part of the probe main body, and is located at the rear part of the measuring inner core, a jetting surface is arranged at an end part of the at least one gas clamping layer close to the measuring inner core, testing ends of the thermocouples are inserted in the measuring inner core, and the other ends of the same penetrate through the probe main body through the cooling chamber. The invention also discloses a high-temperature testing device for the entrained flow gasifier, wherein the high-temperature testing device comprises the high-temperature testing probe, a cooling system and a data acquisition and processing system. The invention further discloses a testing method by adopting the high-temperature testing device. The high-temperature testing probe has the advantages of high temperature resistance and high accuracy, and can be used for realizing long-term, online and accurate temperature test of the entrained flow gasifier under the environment of high temperature.

Description

High temperature test probe and the device thereof, the method for testing that are used for airflow bed gasification furnace
Technical field
The present invention relates to a kind of high temperature test probe, particularly relate to a kind of high temperature test probe that is used for airflow bed gasification furnace, and comprise its device and method of testing.
Background technology
The gasification technology of air flow bed is meant carbon compound is passed through nozzle with vaporized chemical and stream, in gasification furnace, carries out the technological process of flame type non-catalytic partial oxidation reaction.The gasification of air flow bed is carried out under high-temperature and high-pressure conditions usually, and on-stream pressure is 3.0~6.5MPa, and operating temperature is 1300~1600 ℃.
Synthetic gas through the gasification furnace preparation has important value; One of be the raw material of liquefaction (directly or indirectly) made fuel oil, synthesizing methanol, ammonia and methyl ether etc., and the gordian technique of technology future developments such as the generating of integrated gasification combined cycle for power generation system, olefin production technology, fuel cell, reduction iron production and oil refining.The gasification hearth temperature is one of most important control parameters in the gasifying process of air flow bed, has only the gasification furnace operating temperature suitable, could improve gasification efficiency, the serviceable life of relevant device such as prolongation nozzle and refractory liner and material and smooth slag tap etc.
At present, the airflow bed gasification furnace of lining of fire brick structure mainly is to measure fire box temperature through the platinum rhodium thermocouple contact method of band protective casing.Yet thermopair at high temperature receives factor affecting such as airflow scouring, slag corrosion and refractory brick expansion, and its mission life is short and measuring accuracy is relatively poor.Even adopt the thermocouple wire or the protective casing of unlike material, fail all effectively to solve that its tolerable temperature is low, serviceable life short and problem such as measuring accuracy difference.In addition, because thermopair is installed or improper also will the causing of method of application measured the inaccurate of temperature, can't realize rational gasifying process process control.
Be the problem of avoiding above-mentioned thermopair contact method temperature element to exist, relevant indirect temperature-measuring method has also obtained certain utilization at the entrained flow bed gasification technology neighborhood.Such as the methane content that utilizes in the synthetic gas, through relevant methane temperature corresponding relation Model Calculation gasification hearth temperature.Because the accuracy of temperature measuring model and gas analysis utilizes methane content to be difficult to accurately obtain the gasification hearth temperature.For another example through measuring sonde turnover cooling range; Adopt indirect temperature-measuring methods such as heat transfer theory indirect temperature-measuring, CCD (Charge-coupled Device, charge coupled cell) image processing techniques thermometric and acoustic thermometry all owing to reasons such as system is complicated, measuring accuracy is lower fail extensively in the actual industrial device, to use.
Along with gasification with the decline of material quality, for example higher ash content and the ash fusion point of Geng Gao etc. in the coal for gasification, the airflow bed gasification furnace of employing water-cooling wall lining just progressively finds application.Because water-cooling wall lining airflow bed gasification furnace operating temperature generally all is higher than 1400 ℃, extreme temperature even surpass 1600 ℃, therefore traditional pyrometer couple can't use in water-cooling wall lining airflow bed gasification furnace.
In addition, because the water-cooling wall lining structure is complicated, can't satisfy the requirement that indirect measurement needs are offered a plurality of measured holes.And be deposited on the temperature measurement accuracy that molten slag layer on the measuring sensor will greatly influence measurement mechanism.The airflow bed gasification furnace of the water-cooling wall lining that has therefore now moved can only pass through gas composition, according to associated temperature Model Calculation gasification hearth temperature.But because the variation of gasified raw material quality and the influence of measurement precision of gas analyzer are calculated the temperature and the gasification hearth actual temperature that obtain and are differed bigger.
By on can know that under airflow bed gasification furnace high temperature and slag environment, existing measuring method also can't realize long period, online and accurate measurement gasification fire box temperature.Therefore need a kind of ability high temperature resistant, prevent slag deposition and measure accurately temperature measuring equipment and method and measure the gasification fire box temperature, realize the long-period stable operation of gas-flow bed gasifying apparatus.
Summary of the invention
The technical matters that the present invention will solve is that the prior art allowable temperature is lower, the measurement defective that the life-span is short and error is big in order to overcome, and provides a kind of and is used for the high temperature test probe of airflow bed gasification furnace and comprises its device, method of testing.
The present invention solves above-mentioned technical matters through following technical proposals: a kind of high temperature test probe that is used for airflow bed gasification furnace; Its characteristics are that said high temperature measurement probe comprises a probe body, measurement inner core, at least one gas interlayer and some thermopairs;
Said probe body is the tubular of hollow, and said measurement inner core is embedded at said probe as measurement face
One end of main body, said probe body inside also be provided with one be positioned at said measurement inner core rear portion cooling chamber;
Said at least one gas interlayer is arranged at the outside of said probe body, and said at least one gas interlayer is a jet face near the end of said measurement inner core;
The test lead of said some thermopairs is inserted in in-core in the said measurement, and the other end passes said probe body through said cooling chamber.
Preferably, said probe body is a multi-layer sleeve structure, and its cross section is circular, oval or square.
Preferably, the external diameter of said probe body is 5mm-50mm.
Preferably, the length of said measurement inner core is 5mm-100mm.
Preferably, said cooling chamber adopts jacket structured.
Preferably, said jacket structured by an interior pipe and mutual nestable formation of an outer tube.
Preferably, said gas interlayer is around the outside that is arranged on said probe body, and the width of said gas interlayer is 0.5mm-10mm.
Preferably, said jet face is the inclined-plane that makes progress, and the angle of said inclined-plane and surface level is an acute angle.
Preferably, said some thermopairs are arranged the 2-10 root along the inner axially spaced-apart of said measurement inner core.
The present invention also provides a kind of high temperature test device that is used for airflow bed gasification furnace, and its characteristics are that it comprises the aforesaid high temperature test probe that is used for airflow bed gasification furnace, and said proving installation also comprises:
One cooling system is used to cool off said high temperature test probe;
One data acquisition processing system is used to gather the probe temperature of said some thermopairs, and the temperature data that arrives of processing collected;
Wherein, said cooling system is communicated with said cooling chamber, and said data acquisition processing system is connected with the other end of said some thermopairs.
Preferably, said cooling system comprises: a cryogen tank is used to store cooling medium;
One coolant pump is used for the cooling medium pump in the said cryogen tank is delivered in the said cooling chamber of said high temperature test probe;
Wherein, said cryogen tank, said coolant pump and said cooling chamber are connected successively.
Preferably, said cooling medium is water or conduction oil.
Preferably, the other end of said some thermopairs connects a temperature tester, is used to measure the probe temperature of said some thermopairs.
Preferably, said data acquisition processing system comprises:
One data acquisition unit is used to gather the probe temperature of said temperature tester;
One computer system is used for the data that the processing said data collector collects;
Wherein, said temperature tester all is connected with said data acquisition unit with said computer system.
The present invention also provides a kind of usefulness the above-mentioned method of testing that is used for the high temperature test device of airflow bed gasification furnace, and its characteristics are that it may further comprise the steps:
S 1, the said high temperature test probe of said high temperature test device is arranged in the gasification hearth inwall, make that the said inner core end face of said high temperature test probe is concordant with said gasification hearth inside surface;
S 2, in said at least one gas interlayer of said high temperature test probe, be blown into gas, and open the said cooling system in the said high temperature test device;
S 3, open said data acquisition processing system, set up the temperature computation model, and to the calibration correction coefficient of said model;
S 4, said data acquisition processing system gathers the probe temperature of said some thermopairs, and said probe temperature is used to obtain the said temperature computation model after the correction coefficient, to confirm the temperature in the said gasification hearth.
Preferably, the gas that is blown in said at least one gas interlayer is inert gas.
Preferably, the formula of said temperature computation model is a formula 1,
Formula 1:T=[(a * t 1+ b * t 2+ 273.15) d+ c * (t 1-t 2)] e-273.15
Wherein, a, b, c, d, e is temperature correction facotor.
Preferably, said step S 3Also comprise: appoint and get an environment temperature, under said environment temperature, according to the temperature that the said some thermopairs in the said high temperature test probe record, through type 1 simulates correction coefficient a in the said temperature computation model, b, c, d, the value of e.
Preferably, said step S 4Also comprise:
S 41, to appoint the temperature get two thermopairs be t 1, t 2, through type 1 obtains an accounting temperature T;
S 42, through the combination of different thermopairs, obtain a set of calculated temperature T;
S 43, according to a said set of calculated temperature T, utilize numerical optimization to confirm the temperature in the said gasification hearth.
Wherein, said numerical optimization can be for getting the method for average or intermediate value.
Positive progressive effect of the present invention is:
One, the present invention's high temperature test probe of being used for airflow bed gasification furnace adopts resistant to elevated temperatures inner core as the test end face, makes that its allowable temperature is higher.Purging in conjunction with adopting gas has prevented that effectively slag deposition from measuring sensor, having improved measuring accuracy greatly.
Two, the present invention's high temperature test device of being used for airflow bed gasification furnace has adopted the present invention's high temperature test probe; In conjunction with cooling system and data acquisition processing system; Effective cooling down high-temperature test probe; Make that whole device can be at long period under the hot environment, online and measure temperature in the gasification hearth exactly, and realized real time execution monitoring airflow bed gasification furnace.
Three, the present invention's high-temperature testing method of being used for airflow bed gasification furnace has adopted the present invention's high temperature test device, and this method is an indirect measurement method.It is simple to operate, precision is high, helps improving the economic interests and the social benefit of enterprise.
Description of drawings
Fig. 1 is used for the structural representation of preferred embodiment of the high temperature test probe of airflow bed gasification furnace for the present invention.
Fig. 2 is used for the structural representation of preferred embodiment of the high temperature test device of airflow bed gasification furnace for the present invention.
Fig. 3 is used for the process flow diagram of preferred embodiment of the high-temperature testing method of airflow bed gasification furnace for the present invention.
Embodiment
Provide preferred embodiment of the present invention below in conjunction with accompanying drawing, to specify technical scheme of the present invention.
As shown in Figure 1, the high temperature test probe 1 that the present invention is used for airflow bed gasification furnace comprises that a probe body 12, measures inner core 11, at least one gas interlayer 13 and some thermopairs 14.
Probe body 12 is the tubular of hollow, measures inner core 11 and is embedded the end in probe body 12 as measurement face, and measure the end face of inner core 11 and the end face of probe body 12.Preferably, probe body 12 is a multi-layer sleeve structure, and its cross section is circular, oval or square.Wherein, measure inner core 11 and adopt the high-temperature alloy material, like nickel alloy, cobalt-base alloy and titanium alloy or the like, other part materials of high temperature test probe 1 are stainless steel in addition.The high temperature test probe can effectively improve whole heat-resisting quantity like this.Further, the external diameter of probe body 12 is 5mm-50mm.The length of measuring inner core 11 is 5mm-100mm.Certainly, probe body 12 confirms according to the actual conditions demand that with the size of measuring inner core 11 provided herein is preferable value.
Probe body 12 inside also are provided with one and are positioned at the cooling chamber 121 of measuring inner core 11 rear portions.Preferably, cooling chamber 121 comprises pipe 125 and one outer tube 124 in, and is jacket structured through mutual nestable formation.Cooling chamber 121 is provided with an import 122 respectively below interior pipe 125, an outlet 123 is set above outer tube 124, makes cooling medium flow into cooling chamber 121 by import 122, flows out cooling chambers 121 by outlet 123 again behind the absorption heat.
The main effect of cooling chamber 121 is to hold cooling medium, circulates in cooling chamber 121 through cooling medium and cools off inner core 11 and whole high temperature test probe 1.The temperature that can effectively guarantee high temperature test probe 1 and measurement inner core 11 so can be not too high, realizes at high temperature continuing to use, and improved whole heat-resisting quantity.
Gas interlayer 13 is arranged at the outside of probe body 12, and gas interlayer 13 is a jet face 132 near the end of measuring inner core 11; Preferably, gas interlayer 13 is a ring-type, and around the outside that is set in probe body 12, and the width of gas interlayer 13 is 0.5mm-10mm, and promptly measuring face outer rim annular space width is 0.5mm-10mm.Certainly gas interlayer 13 also can be designed to strip, in probe body 12 outer periphery several gas interlayers 13 is set.The shape that is gas interlayer 13 can be according to the actual conditions setting, as long as can reach same effect.
Further, a gas is set on gas interlayer 13 is blown into mouth 131, the gas that is blown into is sprayed into certain speed by the face of measurement outer rim annular space, and this speed can be set according to the actual requirements.Jet face 132 is the inclined-plane that makes progress, and the angle of said inclined-plane and surface level is an acute angle, and promptly flow angle θ scope is 0~90 °.Like this, the gas that is blown into can purge measurement face downwards along flow angle when passing through jet face 132, thereby has prevented that effectively slag or flying dust are deposited on the probe measurement face, have reduced measuring error greatly.
Certainly, the gas that is blown into that here uses selects for use inert gas preferable, prevents the deposition of materials such as slag or flying dust at the probe measurement face.
The test lead of some thermopairs 14 is inserted in to be measured in the inner core 11, and the other end passes probe body 12 through cooling chamber 121.Preferably, some thermopairs 14 are arranged the 2-10 root along measuring inner core 11 inner axially spaced-aparts.Some thermopairs 14 distribute and want evenly to help accurate thermometric.Theoretically, the radical that thermopair is selected is many more, and it is measuring the close more of inner core 11 axial arrangings, and the temperature data that finally records is many more, helps improving the thermometric accuracy.But binding operation feasibility and workload in the practical operation select to arrange 2-10 root thermopair here.Certainly, the user also can add or reduce the thermopair number arbitrarily, does not influence the effect that it reaches.
As shown in Figure 2, the high temperature test device that the present invention is used for airflow bed gasification furnace comprises the aforesaid high temperature test probe 1 that is used for airflow bed gasification furnace.In addition, said proving installation also comprises: a cooling system 2 and a data acquisition processing system 3.Cooling system 2 is used to cool off said high temperature test probe, and data acquisition processing system 3 is used to gather the probe temperature of said some thermopairs 14, and the temperature data that arrives of processing collected.
Wherein, cooling system 2 is communicated with cooling chamber 121, and data acquisition processing system 3 is connected with the other end of some thermopairs 14.
Preferably, cooling system 2 comprises: a cryogen tank 21 is used to store cooling medium; One coolant pump 22 is used for 21 cooling medium pump in the cryogen tank is delivered in the cooling chamber 121 of high temperature test probe 1.
Wherein, the import 122 of cryogen tank 21, coolant pump 22, cooling chamber 121, the outlet 123 by cooling chamber 121 takes back cryogen tank 21 again.Can form the loop of a complete cooling system 2 like this.Preferably, the cooling medium of using in the cooling system 2 is water or conduction oil.
Wherein, the other end of the some thermopairs 14 in the high temperature test probe 1 connects a temperature tester 4, is used to measure the probe temperature of said some thermopairs.
Further, data acquisition processing system 3 comprises: a data acquisition unit 31 is used for the probe temperature of collecting temperature tester 4.One computer system 32 is used for the data that deal with data collector 31 collects.
Wherein, temperature tester 4 is connected in data acquisition unit 31, thereby the measurement temperature that some thermopairs 14 are recorded is transferred to data acquisition unit 31.Then, computer system 32 also is connected with data acquisition unit 31, and data acquisition unit 31 is transferred to computer system 32 with the measurement temperature that some thermopairs 14 record, and is used for deal with data with this, finally obtains the temperature of gasification hearth.
As shown in Figure 3, the present invention is used for the method for testing of the high temperature test device of airflow bed gasification furnace, and it may further comprise the steps:
Step 100, the said high temperature test probe of said high temperature test device is arranged in the gasification hearth inwall.Make that the said inner core end face of said high temperature test probe is concordant with said gasification hearth inside surface.Can guarantee that like this temperature that records is the temperature in the gasification hearth.
Step 101, in said at least one gas interlayer of said high temperature test probe, be blown into gas.Wherein, the gas that is blown in said at least one gas interlayer is inert gas.
Said cooling system in step 102, the said high temperature test device of unlatching;
Step 103, open said data acquisition processing system.
Step 104, set up the temperature computation model.
The formula of said temperature computation model is a formula 1,
Formula 1:T=[(a * t 1+ b * t 2+ 273.15) d+ c * (t 1-t 2)] e-273.15
Wherein, a, b, c, d, e is temperature correction facotor.
Step 105, appoint and to get an environment temperature, under said environment temperature,, confirm correction coefficient a, b, c, d, e through said temperature computation model according to the temperature that the said some thermopairs in the said high temperature test probe record.
Step 106, said data acquisition processing system are gathered the probe temperature of said some thermopairs.
Step 107, to appoint the temperature get two thermopairs be t 1, t 2, obtain an accounting temperature T through said temperature computation model.
Step 108, through the combination of different thermopairs, obtain a set of calculated temperature T.
Step 109, according to a said set of calculated temperature T, utilize numerical optimization to confirm the temperature in the said gasification hearth.Be about to the said temperature computation model after said probe temperature is used for correction coefficient, to confirm the temperature in the said gasification hearth.
Wherein, said numerical optimization is the method for getting average or intermediate value.
The method of testing specific embodiments of high temperature test device that the present invention is used for airflow bed gasification furnace is following:
Embodiment one:
Adopt the present invention to be used for the interior temperature of the direct measurement of gas fluidized gas producer of high temperature test device burner hearth of airflow bed gasification furnace.
At 2 thermopairs of high temperature measurement probe set inside, select K type thermopair here for use, high-temperature probe inner core material adopts the Inconel625 material.
At first, adopt high temperature process furnances to carry out the demarcation of associated temperature correction coefficient, and check thermometric accuracy of the present invention under no lime-ash situation.The high temperature test probe is put into the tubular furnace flat-temperature zone heat, tubular furnace flat-temperature zone temperature is through Type B thermocouple measurement, 1000~1500 ℃ of temperature measurement range, 50 ℃ of temperature intervals.The relevant tubular type furnace temperature T of record g, and high temperature measurement probe inner core temperature t 1And t 2Wherein, adopt chilled water in the cooling system as cooling medium, through turnover cooling water temperature rise adjustment cooling water flow, thus protection high temperature measurement probe.
Temperature correction facotor is respectively a=-3.97, b=14.72, c=3.06 * 10 in the acquisition computation model through demarcating 10, d=4 and e=0.25, high temperature test unit temp measuring error of the present invention is less than 4% under no lime-ash situation.
Further checking the present invention is used for the high temperature test device of airflow bed gasification furnace and the thermometric accuracy of method of testing in airflow bed gasification furnace.Adopt diesel oil, northern place fine coal and oxygen as gasifying medium, measure the gasification fire box temperature, adopt argon gas to protect the probe measurement face not contaminated as sweep gas with K type armoured thermocouple.When the gasification hearth temperature stabilization, the burner hearth actual temperature T that record K type armoured thermocouple measures g, and probe inner core temperature t 1And t 2, utilize fire box temperature calculated value that computation model obtains and actual value error less than 5%.
The present invention's ability is high temperature resistant, prevent temperature in slag deposition and the accurate measurement of gas fluidized bed gasification burner hearth.
Embodiment two:
Adopt the present invention to be used for the interior temperature of the direct measurement of gas fluidized gas producer of high temperature test device burner hearth of airflow bed gasification furnace.
For further improving the thermometric accuracy of high temperature measurement device; The inner core of high temperature test probe is provided with n root K type thermopair vertically; 2<n≤10 piece, because the improper measuring error that is caused of thermopair placement location, the inner core material of high temperature test probe adopts the Inconel625 material to reduce.
Demarcate the associated temperature correction coefficient that the back obtains the temperature computation model through high temperature process furnances.
Adopt diesel oil, northern place fine coal and oxygen as gasifying medium, measure temperature in the gasification hearth with K type armoured thermocouple.Adopt argon purge gas shiled probe measurement face not contaminated, treat the gasification hearth temperature stabilization after, the burner hearth actual temperature T that record K type armoured thermocouple measures g
Choose 2 K type electric thermo-couple temperature t in the high temperature measurement probe arbitrarily 1iAnd t 2j(i wherein, j<n, i ≠ j) calculate a gasification hearth temperature T according to temperature model as 1 group i, and compare with the gasification hearth temperature computation value of utilizing other several groups of thermopairs combination to obtain.
Adopt optimization methods such as average or intermediate value to obtain the calculated value of true reflection gasification hearth actual temperature, further improve the thermometric accuracy of gasification hearth, make its measuring error less than 2%.
To sum up, can accomplish through above-mentioned concrete use and to adopt the present invention to accomplish the high temperature test in the airflow bed gasification furnace burner hearth, it is simple to operate, precision is high, can realize long period under the airflow bed gasification furnace hot environment, online and temperature test accurately.In addition, the demarcation that the present invention is used for the temperature correction facotor that the high-temperature testing method of airflow bed gasification furnace relates to is a prior art, does not do here and gives unnecessary details.
Though more than described embodiment of the present invention, it will be understood by those of skill in the art that these only illustrate, protection scope of the present invention is limited appended claims.Those skilled in the art can make numerous variations or modification to these embodiments under the prerequisite that does not deviate from principle of the present invention and essence, but these changes and modification all fall into protection scope of the present invention.

Claims (19)

1. a high temperature test probe that is used for airflow bed gasification furnace is characterized in that, said high temperature measurement probe comprises a probe body, measurement inner core, at least one gas interlayer and some thermopairs;
Said probe body is the tubular of hollow, and said measurement inner core is embedded the end in said probe body as measurement face, said probe body inside also be provided with one be positioned at said measurement inner core rear portion cooling chamber;
Said at least one gas interlayer is arranged at the outside of said probe body, and said at least one gas interlayer is a jet face near the end of said measurement inner core;
The test lead of said some thermopairs is inserted in in-core in the said measurement, and the other end passes said probe body through said cooling chamber.
2. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 1 is characterized in that said probe body is a multi-layer sleeve structure, and its cross section is circular, oval or square.
3. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 2 is characterized in that the external diameter of said probe body is 5mm-50mm.
4. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 1 is characterized in that the length of said measurement inner core is 5mm-100mm.
5. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 1 is characterized in that said cooling chamber adopts jacket structured.
6. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 5 is characterized in that, and is said jacket structured by an interior pipe and mutual nestable formation of an outer tube.
7. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 1 is characterized in that said gas interlayer is around the outside that is arranged on said probe body, and the width of said gas interlayer is 0.5mm-10mm.
8. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 6 is characterized in that, said jet face is the inclined-plane that makes progress, and the angle of said inclined-plane and surface level is an acute angle.
9. the high temperature test probe that is used for airflow bed gasification furnace as claimed in claim 1 is characterized in that said some thermopairs are arranged the 2-10 root along the inner axially spaced-apart of said measurement inner core.
10. a high temperature test device that is used for airflow bed gasification furnace is characterized in that, it comprises any described high temperature test probe that is used for airflow bed gasification furnace like claim 1-9, and said proving installation also comprises:
One cooling system is used to cool off said high temperature test probe;
One data acquisition processing system is used to gather the probe temperature of said some thermopairs, and the temperature data that arrives of processing collected;
Wherein, said cooling system is communicated with said cooling chamber, and said data acquisition processing system is connected with the other end of said some thermopairs.
11. the high temperature test device that is used for airflow bed gasification furnace as claimed in claim 10 is characterized in that said cooling system comprises:
One cryogen tank is used to store cooling medium;
One coolant pump is used for the cooling medium pump in the said cryogen tank is delivered in the said cooling chamber of said high temperature test probe;
Wherein, said cryogen tank, said coolant pump and said cooling chamber are connected successively.
12. the high temperature test device that is used for airflow bed gasification furnace as claimed in claim 11 is characterized in that said cooling medium is water or conduction oil.
13. the high temperature test device that is used for airflow bed gasification furnace as claimed in claim 12 is characterized in that the other end of said some thermopairs connects a temperature tester, is used to measure the probe temperature of said some thermopairs.
14. the high temperature test device that is used for airflow bed gasification furnace as claimed in claim 13 is characterized in that said data acquisition processing system comprises:
One data acquisition unit is used to gather the probe temperature of said temperature tester;
One computer system is used for the data that the processing said data collector collects;
Wherein, said temperature tester all is connected with said data acquisition unit with said computer system.
15. one kind with the described method of testing that is used for the high temperature test device of airflow bed gasification furnace of claim 10, it is characterized in that it may further comprise the steps:
S 1, the said high temperature test probe of said high temperature test device is arranged in the gasification hearth inwall, make that the said inner core end face of said high temperature test probe is concordant with said gasification hearth inside surface;
S 2, in said at least one gas interlayer of said high temperature test probe, be blown into gas, and open the said cooling system in the said high temperature test device;
S 3, open said data acquisition processing system, set up the temperature computation model, and to the calibration correction coefficient of said model;
S 4, said data acquisition processing system gathers the probe temperature of said some thermopairs, and said probe temperature is used to obtain the said temperature computation model after the correction coefficient, to confirm the temperature in the said gasification hearth.
16. method of testing as claimed in claim 15 is characterized in that, the gas that is blown in said at least one gas interlayer is inert gas.
17. method of testing as claimed in claim 16 is characterized in that, the formula of said temperature computation model is a formula 1,
Formula 1:T=[(a * t 1+ b * t 2+ 273.15) d+ c * (t 1-t 2)] e-273.15
Wherein, a, b, c, d, e is temperature correction facotor.
18. method of testing as claimed in claim 17 is characterized in that, said step S 3Also comprise: appoint and get an environment temperature, under said environment temperature, according to the temperature that the said some thermopairs in the said high temperature test probe record, through type 1 simulates correction coefficient a in the said temperature computation model, b, c, d, the value of e.
19. method of testing as claimed in claim 18 is characterized in that, said step S 4Also comprise:
S 41, to appoint the temperature get two thermopairs be t 1, t 2, through type 1 obtains an accounting temperature T;
S 42, through the combination of different thermopairs, obtain a set of calculated temperature T;
S 43, according to a said set of calculated temperature T, utilize numerical optimization to confirm the temperature in the said gasification hearth.
CN201110149570.3A 2011-06-03 2011-06-03 High-temperature testing probe, device and method for entrained flow gasifier Active CN102322969B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201110149570.3A CN102322969B (en) 2011-06-03 2011-06-03 High-temperature testing probe, device and method for entrained flow gasifier

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201110149570.3A CN102322969B (en) 2011-06-03 2011-06-03 High-temperature testing probe, device and method for entrained flow gasifier

Publications (2)

Publication Number Publication Date
CN102322969A true CN102322969A (en) 2012-01-18
CN102322969B CN102322969B (en) 2013-04-24

Family

ID=45450760

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201110149570.3A Active CN102322969B (en) 2011-06-03 2011-06-03 High-temperature testing probe, device and method for entrained flow gasifier

Country Status (1)

Country Link
CN (1) CN102322969B (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103343979A (en) * 2013-06-25 2013-10-09 合肥金星机电科技发展有限公司 High-temperature probe cooling device
WO2013174969A1 (en) 2012-05-25 2013-11-28 Shell Internationale Research Maatschappij B.V. Temperature measurement in a gasification reactor
CN105675158A (en) * 2016-01-06 2016-06-15 南京航空航天大学 Device and method for simultaneously measuring gas turbine combustion chamber outlet temperature and combustion product concentration
CN110631731A (en) * 2019-10-31 2019-12-31 安徽南自电气股份有限公司 High-temperature-resistant corrosion-resistant platinum-rhodium wire thermocouple and preparation method thereof
CN110749618A (en) * 2019-12-25 2020-02-04 湖南三德盈泰环保科技有限公司 Ignition point and high-temperature combustion rate integrated analysis method and analyzer
CN111334631A (en) * 2020-04-30 2020-06-26 四川冶金设备开发有限公司 Blast furnace cross temperature measuring device with inner core cooling system
CN112858380A (en) * 2020-12-30 2021-05-28 苏州达储能源科技有限公司 Ammonium bisulfate deposition rate measuring probe with automatic heating and ash removal functions
CN113758592A (en) * 2021-11-08 2021-12-07 天霖(张家港)电子科技有限公司 Temperature measuring device for heat treatment temperature of steel coil in bell-type furnace
CN114777844A (en) * 2022-04-28 2022-07-22 陈松涛 Fixed bed gasification furnace detection device and fixed bed gasification furnace detection method

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1041449A (en) * 1988-09-25 1990-04-18 德克萨科开发公司 Be used in the thermopair in the adverse environment
US6302578B1 (en) * 1998-09-30 2001-10-16 Texaco Inc. Behind the brick thermocouple
WO2003081192A1 (en) * 2002-03-18 2003-10-02 Texaco Development Corporation Protective cap for a thermocouple in a gasifier
CN1746640A (en) * 2004-09-07 2006-03-15 中国科学院力学研究所 Be used to measure the interfere reduced enthalpy probe that jet parameters of fluid at superhigh temperature is used
CN101441119A (en) * 2008-12-03 2009-05-27 重庆大学 High temperature solid surface long term accurate temperature measuring system in complicated environment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1041449A (en) * 1988-09-25 1990-04-18 德克萨科开发公司 Be used in the thermopair in the adverse environment
US6302578B1 (en) * 1998-09-30 2001-10-16 Texaco Inc. Behind the brick thermocouple
WO2003081192A1 (en) * 2002-03-18 2003-10-02 Texaco Development Corporation Protective cap for a thermocouple in a gasifier
CN1746640A (en) * 2004-09-07 2006-03-15 中国科学院力学研究所 Be used to measure the interfere reduced enthalpy probe that jet parameters of fluid at superhigh temperature is used
CN101441119A (en) * 2008-12-03 2009-05-27 重庆大学 High temperature solid surface long term accurate temperature measuring system in complicated environment

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013174969A1 (en) 2012-05-25 2013-11-28 Shell Internationale Research Maatschappij B.V. Temperature measurement in a gasification reactor
CN103343979A (en) * 2013-06-25 2013-10-09 合肥金星机电科技发展有限公司 High-temperature probe cooling device
CN105675158A (en) * 2016-01-06 2016-06-15 南京航空航天大学 Device and method for simultaneously measuring gas turbine combustion chamber outlet temperature and combustion product concentration
CN110631731A (en) * 2019-10-31 2019-12-31 安徽南自电气股份有限公司 High-temperature-resistant corrosion-resistant platinum-rhodium wire thermocouple and preparation method thereof
CN110749618A (en) * 2019-12-25 2020-02-04 湖南三德盈泰环保科技有限公司 Ignition point and high-temperature combustion rate integrated analysis method and analyzer
CN110749618B (en) * 2019-12-25 2020-04-24 湖南三德盈泰环保科技有限公司 Ignition point and high-temperature combustion rate integrated analysis method and analyzer
CN111334631A (en) * 2020-04-30 2020-06-26 四川冶金设备开发有限公司 Blast furnace cross temperature measuring device with inner core cooling system
CN112858380A (en) * 2020-12-30 2021-05-28 苏州达储能源科技有限公司 Ammonium bisulfate deposition rate measuring probe with automatic heating and ash removal functions
CN113758592A (en) * 2021-11-08 2021-12-07 天霖(张家港)电子科技有限公司 Temperature measuring device for heat treatment temperature of steel coil in bell-type furnace
CN113758592B (en) * 2021-11-08 2022-02-08 天霖(张家港)电子科技有限公司 Temperature measuring device for heat treatment temperature of steel coil in bell-type furnace
CN114777844A (en) * 2022-04-28 2022-07-22 陈松涛 Fixed bed gasification furnace detection device and fixed bed gasification furnace detection method

Also Published As

Publication number Publication date
CN102322969B (en) 2013-04-24

Similar Documents

Publication Publication Date Title
CN102322969B (en) High-temperature testing probe, device and method for entrained flow gasifier
Sharma Experimental study on 75 kWth downdraft (biomass) gasifier system
CN101354293B (en) System for measuring temperature of coal gas flow bed gasification reactor and method for measuring temperature of coal gas flow bed gasification reactor using the same
CN110568014B (en) Intelligent accumulated dust sampling device and method for online measurement of effective thermal conductivity of accumulated dust
CN108707479A (en) A kind of radiation waste pot system and its working method
Yu et al. The investigations of temperature distributions in an opposed multi-burner gasifier
CN102305675B (en) Indirect temperature measuring device in entrained flow gasifying furnace
KR101636676B1 (en) Gasification reactor for producing crude gas containing co or h2
CN208667617U (en) A kind of radiation waste pot system
CN200975921Y (en) Molten steel temperature quick response infrared continuous measurement apparatus
CN102585907B (en) Step oxygen supply dry slag removal pressure gasification testing system
CN205957218U (en) Flame image gathers and analytical equipment
CN105371973A (en) Multi-point three-dimensional measurement-based boiler outlet smoke temperature real-time measuring method
CN202107673U (en) Device for testing temperature in entrained flow bed gasification furnace
CN204881881U (en) A wear -resisting protection device that combats earthquake for temperature measurement thermal resistance, thermocouple
CN202152277U (en) Reacting furnace for preparing fullerene in batch
CN116694368B (en) Online monitoring device and online monitoring method for coal gasifier
CN101956900B (en) Equipment and method for monitoring pipeline safety
CN105674237A (en) Real-time measuring method for smoke temperature fields of hearth outlet and horizontal flue of power station boiler
CN107807065B (en) For studying the experimental provision of Al-O-C system kinetics under the conditions of slag deposition
CN105296012B (en) A kind of slag gasification furnace Model test in heat state method
CN207537403U (en) A kind of gasification furnace suitable for pluralities of fuel co-gasification
CN107025316B (en) Method for monitoring temperature of water-cooled wall gasifier
CN219429936U (en) Gasifier combustion chamber structure and entrained flow gasifier
CN204234072U (en) A kind ofly can be used for the reactor producing gas phase hydrogen cyanide

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant