CN102283295A - Edible blend oil as well as preparation method and application thereof - Google Patents
Edible blend oil as well as preparation method and application thereof Download PDFInfo
- Publication number
- CN102283295A CN102283295A CN2010102025240A CN201010202524A CN102283295A CN 102283295 A CN102283295 A CN 102283295A CN 2010102025240 A CN2010102025240 A CN 2010102025240A CN 201010202524 A CN201010202524 A CN 201010202524A CN 102283295 A CN102283295 A CN 102283295A
- Authority
- CN
- China
- Prior art keywords
- oil
- edible blend
- lutein
- blend oil
- ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention discloses edible blend oil. The oil provided by the invention contains 0.005-2 wt% of lutein or lutein ester, calculated by the total weight of the edible blend oil. The invention also discloses a preparation method and an application of the edible blend oil.
Description
Technical field
The present invention relates to the edible oil field, relate in particular to a kind of lutein/or ready-mixed oil of lutein ester and its production and use that contains.
Background technology
According to WTO, the whole world has 100,000,000 8 thousand ten thousand crowds to suffer from various types of disease of eye, wherein causes blind crowd that 45,000,000 people are arranged thus.Senile eye illness is to cause the first cause of the middle-aged and old blindings of western countries more than 50 years old, and wherein the number of whole world trouble senile macular degeneration AMD reaches 2500-3000 ten thousand people.In China, cataract crowd accounts for all eye illness morbidity crowds' 20%, becomes primary killer.
Scientific evidence shows, lutein and zeaxanthin are two kinds of carotenoid of unique existence in crystalline lens and the retina, and is significant to the eye health care.Lutein belongs to carotenoid family, with 2 kinds of forms natural being present in vegetables and the fruit, the i.e. lutein of esterification (lutein ester) and free lutein.Owing to can not synthesize lutein in the human body, lutein in the meals that place one's entire reliance upon and lutein ester replenish.The nutritionist advises eating 5 fruits or vegetables every day, and majority do not take in this recommended amounts.
Though the WO2006/117826 patent report in olive oil, add lutein, only be applicable to cold and dressed with saucely, be unfavorable for the cooking or frying, and do not relate to the fatty acid nutritive balance.
Studies show that, the poor stability of lutein/lutein ester, daylight (natural daylight) shines half an hour, and the storage rate of the two only is 0.35%.This also is the cause that the edible blend oil that contains lutein/lutein ester can't be provided in this area always.
At present various countries, also take much count of the proportion of composing of aliphatic acid except that total intake of fat is advised to some extent about the recommended intake of fat.The ratio of aliphatic acid comprises two aspects, the one, and the proportion of composing of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is the ratio between ω-6/ omega-3 polyunsaturated fatty acids on the other hand." the DRIs .Chinese DRIS " that the Chinese Soclety of Nutrition that publishes in October, 2000 writes is to the recommendation such as the table 1 of the suitable intake of China resident fat.
The table 1 Chinese residents dietary fat intake (AI) (fatty energy accounts for the percentage of gross energy) that suits
| Age/year | Fat | SFA | MUFA | PUFA | ω-6/ω-3 | Cholesterol amount/mg |
| 0～ | 45～50 | 4∶1 | ||||
| 0.5～ | 35～40 | 4∶1 | ||||
| 2～ | 30～35 | (4～6)∶1 | ||||
| 7～ | 25～30 | (4～6)∶1 | ||||
| 13～ | 25～30 | ＜10 | 8 | 10 | (4～6)∶1 | |
| 18～ | 20～30 | ＜10 | 10 | 10 | (4～6)∶1 | ＜300 |
| 60～ | 20～30 | 6～8 | 10 | 8～10 | 4∶1 | ＜300 |
Summary of the invention
The present invention aims to provide a kind of edible blend oil that contains lutein or lutein ester and its production and use.
Another object of the present invention provides a kind of method that improves lutein in the edible blend oil or lutein ester stability.
In a first aspect of the present invention, a kind of edible blend oil is provided, in the gross weight of edible blend oil, wherein the content of lutein or lutein ester is 0.005-2wt%.
In another preference, the weight ratio of saturated aliphatic acid, monounsaturated fatty acids and polyunsaturated fatty acid is 0.15-0.4 in the described edible blend oil: 1: 1, the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid was 4-6: 1.
In another preference, described lutein or lutein ester are the marigold flower extracts.
In another preference, described edible blend oil contains and is selected from following grease more than three kinds or three kinds: soybean oil, rapeseed oil, corn oil, sunflower oil, peanut oil, sesame oil, tea-seed oil, olive oil, safflower oil, linseed oil, rice oil and cottonseed oil.
In another preference, also contain antioxidant and/or emulsifying agent in the described edible blend oil; In the gross weight of edible blend oil, contain antioxidant 0-0.15wt%, contain emulsifying agent 0.3-5wt%.Described antioxidant is selected from following one or more: TBHQ (TBHQ), butylated hydroxy anisole (BHA), dibutyl hydroxy toluene (BHT), support one's family thing E (VE), Rosmarinus officinalis extract and Tea Polyphenols; Described emulsifying agent is selected from following one or more: sucrose fatty ester, polyglyceryl fatty acid ester, butanedioic acid glyceride, D-sorbite fatty acid ester and sorbitan fatty acid ester.
In a second aspect of the present invention, a kind of preparation method of aforesaid edible blend oil provided by the invention is provided, described method comprises step: the edible blend oil that will contain lutein or lutein ester under nitrogen and/or inert gas is warming up to 100-200 ℃, is cooled to 40-50 ℃ again and obtains aforesaid edible blend oil provided by the invention; In the gross weight of edible blend oil, wherein the content of lutein or lutein ester is 0.005-2wt%.
In another preference, described method comprises step:
(1) will be selected from following grease more than three kinds or three kinds mixes: soybean oil, rapeseed oil, corn oil, sunflower oil, peanut oil, sesame oil, tea-seed oil, olive oil, safflower oil, linseed oil, rice oil and cottonseed oil;
(2) under nitrogen and/or inert gas, add lutein or lutein ester, and be warming up to 100-200 ℃ grease and lutein or lutein ester are mixed; With
(3) be cooled to 40-50 ℃, adding antioxidant and/or emulsifying agent make to mix and obtain aforesaid edible blend oil provided by the invention.
In another preference, described preparation method avoids carrying out in the container of iron or copper, or avoids contacting iron or copper.
In another preference, in the step (1) in the mixed grease weight ratio of saturated aliphatic acid, monounsaturated fatty acids and polyunsaturated fatty acid be 0.15-0.4: 1: 1, the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid was 4-6: 1.
In a third aspect of the present invention, a kind of purposes of aforesaid edible blend oil provided by the invention is provided, be used for sight protection.
In a fourth aspect of the present invention, a kind of lutein contained in the edible blend oil/or stable method of lutein ester that makes is provided, described method comprises step: the edible blend oil that will contain lutein or lutein ester under inert gas is warming up to 100-200 ℃, after being cooled to 40-50 ℃ again, packing into has in the packing of uvioresistant effect.
In view of the above, the invention provides a kind of edible blend oil that contains lutein or lutein ester.
The specific embodiment
The inventor is through extensive and deep research, found a kind of method of in edible blend oil, adding lutein/lutein ester, the stability of the lutein/lutein ester in the edible blend oil that obtains by this method is very high, thereby can satisfy by using the effect of such edible blend oil health care eyesight; Find that simultaneously the ready-mixed oil that adds lutein ester can better promote saturated fatty acid myristic acid, laurate, palmitic acid metabolism in vivo in the body, on this basis, has finished the present invention.
Particularly, edible blend oil provided by the invention prepares by following step:
The first step feeds nitrogen in the compound lard that is obtained by following grease mixing more than three kinds or three kinds and/or inert gas is removed the air that may cause the compound lard oxidation: soybean oil, rapeseed oil, corn oil, sunflower oil, peanut oil, sesame oil, tea-seed oil, olive oil, safflower oil, linseed oil, rice oil and cottonseed oil;
Second step added lutein or lutein ester, and is warming up to 100-200 ℃ simultaneously, and lutein or lutein ester and compound lard are mixed;
In the 3rd step, be cooled to 40-50 ℃;
In the 4th step, filter and obtain edible blend oil provided by the invention.
The compound lard of the first step preferably uses the darker grease of color to mix, such as but not limited to, peanut oil, rapeseed oil, corn oil, sesame oil, linseed oil; More preferably; the weight ratio of saturated aliphatic acid, monounsaturated fatty acids and polyunsaturated fatty acid is 0.15-0.4 in the compound lard of the first step: 1: 1; the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid is 4-6: 1; such compound lard can obtain by method well known in the art; for example the patent No. is the rational plant blend oil of a kind of fatty acid proportion claimed in the Chinese patent of ZL 02108374, and the content in this patent is together incorporated in the specification of the present invention.
The inert gas that uses in the first step is helium, neon, argon gas, krypton gas, xenon, radon gas or its mixing.In a method for optimizing of the present invention, said method goes on foot from the first step to the four and all carries out under the protection of nitrogen and/or inert gas, to remove the air and the volatile impurity that can cause oil oxidation.
In a preferred version of said method, the 3rd step was to be cooled to 40-50 ℃, added antioxidant and/or emulsifying agent, and stirred to make simultaneously and mix; Mixing speed 10-300 rev/min, mixing time is 20-30 minute.Described antioxidant is selected from following one or more: TBHQ, BHA, BHT, VE, Rosmarinus officinalis extract and Tea Polyphenols; Described emulsifying agent is selected from following one or more: sucrose fatty ester, polyglyceryl fatty acid ester, butanedioic acid glyceride, D-sorbite fatty acid ester and sorbitan fatty acid ester.
Filtration in the 4th step can be the method for this area routine, such as but not limited to, filter bag is to remove insoluble solids impurity.
In a preference of the present invention, the edible blend oil provided by the invention that obtains in the 4th step packed into have in the packing of uvioresistant effect, described packing with uvioresistant effect can be well known in the art, such as but not limited to, PET bottle, vial.
The edible blend oil that obtains by said method is a kind of balanced fatty acid, is rich in the health-care edible oil of lutein or lutein ester and fine vision protection, in the gross weight of edible blend oil, wherein contains the 0.005-2wt% lutein ester; And the weight ratio of the saturated fatty acid of grease, monounsaturated fatty acids and polyunsaturated fatty acid is 0.15-0.4: 1: 1, the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid was 4-6: 1.
Preferably, also contain antioxidant and/or emulsifying agent in the edible blend oil provided by the invention; In the gross weight of edible blend oil, the antioxidant that contains is 0-0.15wt%, and the emulsifying agent that contains is 0.3-5wt%.
As used herein, " lutein (lutein) " is suc as formula the material shown in the I, can extract to obtain from plant, extractible plant comprises spinach, beanpod dish, cabbage, pepper powder, collard, pea, wild cabbage etc.The preferred lutein that extracts purifying from marigold flower (pot marigold).Can use the method for this area routine to extract purification of xanthophylls from marigold flower, include but not limited to, be raw material with the marigold flower, produces through steps such as dehydration pulverizing, solvent extraction, low-molecular-weight alcohol purifying and vacuum concentrate.
As used herein, " lutein ester (Lutein Esters) " is meant after general and aliphatic acid (as laurate, the palmitic acid etc.) esterification of lutein the material that the form with ester exists, for example lutein dipalmitate.The molten purity of preferred oil is the lutein ester of 10%-30% among the present invention.
As used herein, " Rosmarinus officinalis extract " is meant the plant rosemary extract, mainly comprises Rosmarinic acid, rosemary, phenol, carnosic acid, carnosol etc.
Edible blend oil provided by the invention owing to contain lutein or lutein ester, both can reduce, delay aging, degeneration, the pathology of eyes, reduced the incidence of eye illness, can also protect retina to avoid the injury of light.Edible blend oil provided by the invention can also reach the nutrient balance of aliphatic acid, and this product can be used for the cooking or frying.
Though the saturated fatty acid that The World Health Organization (WHO) and FAO (Food and Agriculture Organization of the United Nation) (FAO) are recommended: monounsaturated fatty acids: polyunsaturated fatty acid=1: 1: 1, but when taking in animal food according to present Chinese residents based on saturated fatty acid, the absorption that therefore when taking in vegetable oil, should reduce saturated fatty acid with the absorption that reaches aliphatic acid more near the recommendation of Chinese Soclety of Nutrition, so this ready-mixed oil saturated fatty acid, monounsaturated fatty acids, with the weight ratio of polyunsaturated fatty acid be 0.15-0.4: 1: 1, the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid was 4-6: 1.The weight ratio 0.15-0.2 of wherein saturated, single unsaturated, polyunsaturated fatty acid: be more suitable in the elderly at 1: 1.
Absorption contains the ready-mixed oil of marigold flower extract or fruits and vegetables extract lutein ester, lutein ester at first is hydrolyzed into lutein in the human consumption absorption process, lutein can also promote the saturated fatty acid myristic acid simultaneously, laurate, palmitic acid metabolism in vivo, nutrient research shows, saturated fatty acid intake Gao Shiyi causes cholesterolemia, triglycerides and LDL-C raise, especially with myristic acid in the saturated fatty acid, laurate, palmitic acid increases the total lipoprotein of blood plasma, myristic acid, it is the strongest that laurate improves the effect of serum cholesterol, so it is very necessary to reduce the intake of saturated fatty acid.China resident can guarantee to play the sight protection effect when edible this is filled a prescription edible oil, can gather in the crops the accumulative effect that reduces body inner cholesterol and blood fat on the dual degree again.
The above-mentioned feature that the present invention mentions, or the feature that embodiment mentions can make up arbitrarily.All features that this case specification is disclosed can with any composition forms and usefulness, each feature that is disclosed in the specification can anyly provide the alternative characteristics of identical, impartial or similar purpose to replace.Therefore removing has special instruction, and the feature that is disclosed only is the general example of equalization or similar features.
Major advantage of the present invention is:
When 1, edible blend oil provided by the invention had not only been considered saturated, single unsaturated, how unsaturated and ω-6 unrighted acids/omega-3 unsaturated fatty acid balance but by in edible oil, add original just safely, active material lutein ester without any side effects, can be in time fully replenish the deficiency of taking in because of diet in people's daily life, avoid that shortage because of lutein causes that retina is impaired, eyesight decline, eye illness and cataractous generation even blind.
2, by normally having meal every day, need not extra replenishing, just can from be rich in the lutein ester edible oil, obtain this health-care components of needed by human body, final product is healthy and safe stable.And lutein ester itself is exactly a kind of good antioxidant.
3, edible blend oil provided by the invention can be used for the cooking or frying, and lutein ester is easier is absorbed in the cooking or frying back.
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used to the present invention is described and be not used in and limit the scope of the invention.The experimental technique of unreceipted actual conditions in the following example is usually according to the normal condition or the condition of advising according to manufacturer.Unless otherwise indicated, otherwise all percentage, ratio, ratio or umber by weight.
Unit in the percent weight in volume among the present invention is well-known to those skilled in the art, for example is meant the weight of solute in 100 milliliters solution.
Unless otherwise defined, employed all specialties are identical with the meaning that scientific words and one skilled in the art are familiar with in the literary composition.In addition, any method similar or impartial to described content and material all can be applicable in the inventive method.The usefulness that preferable implementation method described in the literary composition and material only present a demonstration.
Various content of fatty acid are measured and are all adopted gas chromatography in the embodiment of the invention, and chromatographic condition is as follows:
CP-Si188 chromatographic column 50m * 0.25mm;
Temperature programming: 120 ℃ of initial temperatures, keep 3min, be warming up to 180 ℃ with the speed of 10 ℃/min, keep 5.5min, be warming up to 215 ℃ with the speed of 15 ℃/min, keep 3min;
Carrier gas: nitrogen, 250 ℃ of injector temperatures, 280 ℃ of detector temperatures, split ratio 50: 1;
Constant voltage mode: column cap is pressed 20psi, sample size 0.2 μ L.
Lutein content and lutein ester Determination on content all adopt lutein (ester) absorbance under the ultraviolet specrophotometer colorimetric method for determining 445nm wavelength in the embodiment of the invention.
Lutein is available from DSM company in the embodiment of the invention, and purity is 90%.
Lutein ester is available from Cognis company in the embodiment of the invention, and purity is 15% oil-soluble preparation.
Grain and oil Industrial Co., Ltd in other key component in the embodiment of the invention is all praised available from Shanghai.
Embodiment 1
Preparation edible blend oil 1
Accurately weighing 50mg lutein ester joins 500g rice oil; the 300g safflower oil; in the 200g peanut oil, feed helium and protect, be warming up to 150 ℃; keep making it in 30 seconds dissolving; be cooled to 40-50 ℃ again and add 160ppmVE and 3000ppm sucrose fatty ester while stirring, mix, filter bag filters; nitrogen-filled seal obtains edible blend oil 1 in uvioresistant PET bottle.
Embodiment 2
Preparation edible blend oil 2
Accurately weighing 100mg lutein joins 400g corn oil; in 400g seed oil of sunflower, the 200g camellia seed oil; feeding helium protects; be warming up to 150 ℃, keep making it in 30 seconds dissolving, be cooled to 40-50 ℃ again and add 160ppm Tea Polyphenols and 5000ppm sucrose fatty ester while stirring; mix; filter bag filters, and nitrogen-filled seal obtains edible blend oil 2 in uvioresistant PET bottle.
Embodiment 3
Preparation edible blend oil 3
Accurately weighing 800mg lutein ester joins the 300g soybean oil; the 450g rapeseed oil, the 150g seed oil of sunflower is in the 100g olive oil; feeding nitrogen protects; be warming up to 150 ℃, keep making it in 30 seconds dissolving, be cooled to again and add the 160ppm Rosmarinus officinalis extract about 50 ℃ while stirring and add the 5000ppm sucrose fatty ester; mix; filter bag filters, and nitrogen-filled seal obtains edible blend oil 3 in uvioresistant PET bottle.
Embodiment 4
Preparation edible blend oil 4
Accurately weighing 200mg lutein and 300mg lutein ester join among rapeseed oil 400g, corn oil 160g, peanut oil 170g, sunflower oil 195g, linseed oil 55g, the sesame oil 20g; feeding nitrogen protects; be warming up to 150 ℃; keep making it in 30 seconds dissolving; be cooled to and add the 160ppm Rosmarinus officinalis extract about 50 ℃ while stirring and add the 5000ppm sucrose fatty ester, mix, filter bag filters; nitrogen-filled seal obtains edible blend oil 4 in uvioresistant PET bottle.
Above embodiment gained health blend oil aliphatic acid composition sees Table 2:
Table 2
| Embodiment | Saturated fatty acid (wt%) | Monounsaturated fatty acids (wt%) | Polyunsaturated fatty acid (wt%) | Omega 6 polyunsaturated fatty acid (wt%) | Omega-3 polyunsaturated fatty acids (wt%) |
| Edible blend oil 1 | 9.77 | 45.69 | 44.18 | 38.38 | 5.81 |
| Edible blend oil 2 | 8.38 | 47.02 | 44.47 | 38.31 | 6.15 |
| Edible blend oil 3 | 11.88 | 44.68 | 43.14 | 37.12 | 6.03 |
| Edible blend oil 4 | 12.02 | 44.74 | 43.81 | 36.93 | 6.29 |
Refrigeration test and high temperature heat run
The edible blend oil that above embodiment 1-4 obtains is all done refrigeration test and high temperature heat run.
Refrigeration test: earlier the foregoing description edible blend oil is heated to 130 ℃, immerse 0 ℃ of ice-water bath, placed 5.5 hours, estimate equal clear, no crystallization or floccule illustrate that oil product of the present invention has good stability.
High temperature heat run: 180 ℃ of heating the foregoing description edible blend oils, continue 6 hours, heat found that embodiment 1 lutein ester storage rate is 95.5% in 1 hour, embodiment 2 lutein storage rates are 91.8%, embodiment 3 lutein ester storage rates are 96.6%, embodiment 4 lutein (ester) storage rate is 94.5%, heat the storage rate of finding lutein (ester) after 6 hours and be respectively 94.8%, 88.5%, 95.2%, 93.8%.Illustrate that this product is applicable to culinary art or frying.
Embodiment 5
The light durability test
Select refined rapeseed oil 200g, refined maize oil 210g, peanut oil 500g, refining linseed oil 90g for use; add material-compound tank, feed nitrogen and protect, be warmed up to 130 ℃ and add the 6g lutein ester; be cooled to 40-50 ℃ behind the mixing; add 20ppm natural VE and 80ppmTBHQ, add the 3000ppm sucrose fatty ester again, stir 20-30min at a slow speed; 100 rev/mins of mixing speeds; filter bag filters, and it is canned in the PET bottle of anti-ultraviolet to fill nitrogen, obtains edible blend oil 5.
| Embodiment 5 | Saturated fatty acid (wt%) | Monounsaturated fatty acids (wt%) | Polyunsaturated fatty acid (wt%) | Omega 6 polyunsaturated fatty acid (wt%) | Omega-3 polyunsaturated fatty acids (wt%) |
| Edible blend oil 5 | 16.13 | 42.91 | 41.40 | 34.67 | 6.73 |
Then the edible blend oil 5 that obtains is carried out the natural light irradiation test.Adopt storage rate to investigate the stability of lutein ester, the light absorption value of storage rate=mensuration/initial light absorption value * 100%.The results are shown in Table 3.
Table 3 indoor natural light shines the influence to the stability of edible blend oil 5 lutein esters
The result shows, places 240 hours, and the storage rate of lutein ester is 98.96%, shows that this product is more stable.
Comparative Examples (comparing) with embodiment 3
Accurately weighing 800mg lutein ester joins the 300g soybean oil, the 450g rapeseed oil, the 150g seed oil of sunflower in the 100g olive oil, is stirred and heated to about 50 ℃, make it abundant dissolving, add the 160ppm Rosmarinus officinalis extract again and add the 5000ppm sucrose fatty ester, mix, filter bag filters, nitrogen-filled seal obtains edible blend oil 6 in the common PET bottle.
Found through the heating of 180 ℃ of high temperature that the storage rate of lutein ester in this ready-mixed oil was 85% in 1 hour, indoor natural light is according to the storage rate of finding lutein ester in 240 hours only 0.85%.
The above only is preferred embodiment of the present invention, be not in order to limit essence technology contents scope of the present invention, essence technology contents of the present invention is broadly to be defined in the claim scope of application, any technology entity or method that other people finish, if it is defined identical with the claim scope of application, also or a kind of change of equivalence, all will be regarded as being covered by among this claim scope.
Claims (10)
1. an edible blend oil is characterized in that, in the gross weight of edible blend oil, wherein the content of lutein or lutein ester is 0.005-2wt%.
2. edible blend oil as claimed in claim 1, it is characterized in that, the weight ratio of saturated aliphatic acid, monounsaturated fatty acids and polyunsaturated fatty acid is 0.15-0.4 in the described edible blend oil: 1: 1, the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid was 4-6: 1.
3. edible blend oil as claimed in claim 1, it is characterized in that described edible blend oil contains and is selected from following grease more than three kinds or three kinds: soybean oil, rapeseed oil, corn oil, sunflower oil, peanut oil, sesame oil, tea-seed oil, olive oil, safflower oil, linseed oil, rice oil and cottonseed oil.
4. edible blend oil as claimed in claim 1 is characterized in that, also contains antioxidant and/or emulsifying agent in the described edible blend oil; In the gross weight of edible blend oil, contain antioxidant 0-0.15wt%, contain emulsifying agent 0.3-5wt%.
5. edible blend oil as claimed in claim 4, it is characterized in that, described antioxidant is selected from following one or more: TBHQ (TBHQ), butylated hydroxy anisole (BHA), dibutyl hydroxy toluene (BHT), support one's family thing E (VE), Rosmarinus officinalis extract and Tea Polyphenols; Described emulsifying agent is selected from following one or more: sucrose fatty ester, polyglyceryl fatty acid ester, butanedioic acid glyceride, D-sorbite fatty acid ester and sorbitan fatty acid ester.
6. preparation method as the arbitrary described edible blend oil of claim 1-5, it is characterized in that, described method comprises step: the edible blend oil that will contain lutein or lutein ester under nitrogen and/or inert gas is warming up to 100-200 ℃, is cooled to 40-50 ℃ again and obtains arbitrary described edible blend oil as claim 1-5; In the gross weight of edible blend oil, wherein the content of lutein or lutein ester is 0.005-2wt%.
7. preparation method as claimed in claim 6 is characterized in that, described preparation method avoids carrying out in the container of iron or copper, or avoids contacting iron or copper.
8. preparation method as claimed in claim 7, it is characterized in that, in the step (1) in the mixed grease weight ratio of saturated aliphatic acid, monounsaturated fatty acids and polyunsaturated fatty acid be 0.15-0.4: 1: 1, the weight ratio of ω-6 unrighted acid and omega-3 unsaturated fatty acid was 4-6: 1.
9. the purposes as the arbitrary described edible blend oil of claim 1-5 is characterized in that, is used for sight protection.
10. one kind makes lutein contained in the edible blend oil/or stable method of lutein ester, described method comprises step: the edible blend oil that will contain lutein or lutein ester under inert gas is warming up to 100-200 ℃, after being cooled to 40-50 ℃ again, packing into has in the packing of uvioresistant effect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010202524.0A CN102283295B (en) | 2010-06-17 | 2010-06-17 | Edible blend oil as well as preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010202524.0A CN102283295B (en) | 2010-06-17 | 2010-06-17 | Edible blend oil as well as preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102283295A true CN102283295A (en) | 2011-12-21 |
| CN102283295B CN102283295B (en) | 2014-03-12 |
Family
ID=45330275
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010202524.0A Active CN102283295B (en) | 2010-06-17 | 2010-06-17 | Edible blend oil as well as preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102283295B (en) |
Cited By (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103005012A (en) * | 2012-12-17 | 2013-04-03 | 湖南金点油脂有限公司 | Edible blending oil and preparation method thereof |
| CN103202351A (en) * | 2013-04-23 | 2013-07-17 | 山东省恒兴油脂有限公司 | Functional grease composition and preparation method thereof |
| CN103211040A (en) * | 2013-05-13 | 2013-07-24 | 山东三星玉米产业科技有限公司 | Frying oil and preparation method thereof |
| CN103238678A (en) * | 2013-04-22 | 2013-08-14 | 刘洪举 | Cold pressed flax, sesame and olive edible blend oil |
| CN103392836A (en) * | 2013-07-09 | 2013-11-20 | 菏泽市牡丹区牡丹研究所 | Peony seed oil natural antioxidant composite |
| CN103446197A (en) * | 2013-09-11 | 2013-12-18 | 白心亮 | Novel liver protection product |
| CN103523377A (en) * | 2013-10-20 | 2014-01-22 | 丹阳市正大油脂有限公司 | Method for packing edible oil |
| CN103820209A (en) * | 2014-03-13 | 2014-05-28 | 苏州高新区长巷农场专业合作社 | Refining processing technology for rapeseed blend oil |
| CN103891922A (en) * | 2012-12-26 | 2014-07-02 | 丰益(上海)生物技术研发中心有限公司 | Edible oil composition containing water soluble antioxidant and preparation method thereof |
| CN105076502A (en) * | 2015-08-28 | 2015-11-25 | 安徽丰原马鞍山生物化学有限公司 | Edible oil |
| CN105707295A (en) * | 2015-04-09 | 2016-06-29 | 赵志红 | Selenium-enriched rosemary flaxseed oil |
| CN105733803A (en) * | 2014-12-26 | 2016-07-06 | 丰益(上海)生物技术研发中心有限公司 | Method of treating grease |
| CN106212735A (en) * | 2016-10-08 | 2016-12-14 | 张文 | Herba Rosmarini Officinalis edible oil |
| CN106720460A (en) * | 2015-11-25 | 2017-05-31 | 杭州宏盛粮油贸易有限公司 | Edible oil |
| CN106819152A (en) * | 2017-01-19 | 2017-06-13 | 莒南县金胜粮油实业有限公司 | Fry special ready-mixed oil and preparation method thereof |
| CN106967505A (en) * | 2017-04-26 | 2017-07-21 | 东北农业大学 | It is a kind of to add the method that complex natural antioxidant suppresses corn oil oxidation |
| CN107509822A (en) * | 2017-08-25 | 2017-12-26 | 山东鲁派国际食品有限公司 | A kind of special edible oil of pregnant woman and preparation method thereof |
| CN107736444A (en) * | 2017-10-26 | 2018-02-27 | 桂林市味美园餐饮管理有限公司 | A kind of edible oil and preparation method thereof |
| CN107912544A (en) * | 2017-11-21 | 2018-04-17 | 菏泽海诺知识产权服务有限公司 | A kind of edible blend oil and preparation method thereof |
| CN108611189A (en) * | 2016-12-09 | 2018-10-02 | 丰益(上海)生物技术研发中心有限公司 | The refinery practice of bisphenol-A and alkyl phenol in a kind of control grease |
| WO2021234168A1 (en) * | 2020-05-21 | 2021-11-25 | Mixscience | Pigment composition and uses thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006117826A2 (en) * | 2005-05-02 | 2006-11-09 | Sooft Italia Srl | Composition comprising olive oil enriched and supplemented with lutein |
| CN101228907A (en) * | 2008-02-04 | 2008-07-30 | 张超 | Preparing process of multifunctional edible oil containing lycopene |
| CN101731373A (en) * | 2009-12-31 | 2010-06-16 | 山东三星玉米产业科技有限公司 | DHA-containing corn oil special for pregnant and nursing women and preparation method thereof |
-
2010
- 2010-06-17 CN CN201010202524.0A patent/CN102283295B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006117826A2 (en) * | 2005-05-02 | 2006-11-09 | Sooft Italia Srl | Composition comprising olive oil enriched and supplemented with lutein |
| CN101228907A (en) * | 2008-02-04 | 2008-07-30 | 张超 | Preparing process of multifunctional edible oil containing lycopene |
| CN101731373A (en) * | 2009-12-31 | 2010-06-16 | 山东三星玉米产业科技有限公司 | DHA-containing corn oil special for pregnant and nursing women and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 郭志有等: "叶黄素的功能及应用", 《河北农业科学》, vol. 14, no. 2, 28 February 2010 (2010-02-28) * |
Cited By (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103005012A (en) * | 2012-12-17 | 2013-04-03 | 湖南金点油脂有限公司 | Edible blending oil and preparation method thereof |
| CN103005012B (en) * | 2012-12-17 | 2014-07-02 | 湖南金点油脂有限公司 | Edible blending oil and preparation method thereof |
| CN103891922A (en) * | 2012-12-26 | 2014-07-02 | 丰益(上海)生物技术研发中心有限公司 | Edible oil composition containing water soluble antioxidant and preparation method thereof |
| CN103891922B (en) * | 2012-12-26 | 2020-02-18 | 丰益(上海)生物技术研发中心有限公司 | Edible oil composition comprising water-soluble antioxidant and preparation method thereof |
| CN103238678A (en) * | 2013-04-22 | 2013-08-14 | 刘洪举 | Cold pressed flax, sesame and olive edible blend oil |
| CN103202351A (en) * | 2013-04-23 | 2013-07-17 | 山东省恒兴油脂有限公司 | Functional grease composition and preparation method thereof |
| CN103211040A (en) * | 2013-05-13 | 2013-07-24 | 山东三星玉米产业科技有限公司 | Frying oil and preparation method thereof |
| CN103392836A (en) * | 2013-07-09 | 2013-11-20 | 菏泽市牡丹区牡丹研究所 | Peony seed oil natural antioxidant composite |
| CN103446197A (en) * | 2013-09-11 | 2013-12-18 | 白心亮 | Novel liver protection product |
| CN103446197B (en) * | 2013-09-11 | 2016-04-13 | 白心亮 | A kind of liver protection product |
| CN103523377A (en) * | 2013-10-20 | 2014-01-22 | 丹阳市正大油脂有限公司 | Method for packing edible oil |
| CN103820209A (en) * | 2014-03-13 | 2014-05-28 | 苏州高新区长巷农场专业合作社 | Refining processing technology for rapeseed blend oil |
| CN105733803B (en) * | 2014-12-26 | 2020-02-18 | 丰益(上海)生物技术研发中心有限公司 | Method for treating grease |
| CN105733803A (en) * | 2014-12-26 | 2016-07-06 | 丰益(上海)生物技术研发中心有限公司 | Method of treating grease |
| CN105707295A (en) * | 2015-04-09 | 2016-06-29 | 赵志红 | Selenium-enriched rosemary flaxseed oil |
| CN105076502A (en) * | 2015-08-28 | 2015-11-25 | 安徽丰原马鞍山生物化学有限公司 | Edible oil |
| CN106720460A (en) * | 2015-11-25 | 2017-05-31 | 杭州宏盛粮油贸易有限公司 | Edible oil |
| CN106212735A (en) * | 2016-10-08 | 2016-12-14 | 张文 | Herba Rosmarini Officinalis edible oil |
| CN108611189A (en) * | 2016-12-09 | 2018-10-02 | 丰益(上海)生物技术研发中心有限公司 | The refinery practice of bisphenol-A and alkyl phenol in a kind of control grease |
| CN108611189B (en) * | 2016-12-09 | 2023-02-21 | 丰益(上海)生物技术研发中心有限公司 | Refining process for controlling bisphenol A and alkylphenol in grease |
| CN106819152A (en) * | 2017-01-19 | 2017-06-13 | 莒南县金胜粮油实业有限公司 | Fry special ready-mixed oil and preparation method thereof |
| CN106967505A (en) * | 2017-04-26 | 2017-07-21 | 东北农业大学 | It is a kind of to add the method that complex natural antioxidant suppresses corn oil oxidation |
| CN107509822A (en) * | 2017-08-25 | 2017-12-26 | 山东鲁派国际食品有限公司 | A kind of special edible oil of pregnant woman and preparation method thereof |
| CN107736444A (en) * | 2017-10-26 | 2018-02-27 | 桂林市味美园餐饮管理有限公司 | A kind of edible oil and preparation method thereof |
| CN107912544A (en) * | 2017-11-21 | 2018-04-17 | 菏泽海诺知识产权服务有限公司 | A kind of edible blend oil and preparation method thereof |
| WO2021234168A1 (en) * | 2020-05-21 | 2021-11-25 | Mixscience | Pigment composition and uses thereof |
| FR3110587A1 (en) * | 2020-05-21 | 2021-11-26 | Mixscience | Pigment composition and its uses |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102283295B (en) | 2014-03-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102283295B (en) | Edible blend oil as well as preparation method and application thereof | |
| Jeon et al. | Physicochemical properties and oxidative stabilities of mealworm (Tenebrio molitor) oils under different roasting conditions | |
| Imoisi et al. | Palm oil, its nutritional and health implications | |
| CN105104578A (en) | Edible oil for improving oil and fat balance and oil and fat health and preparation method of edible oil | |
| JP2009100736A (en) | Edible oil-and-fat composition | |
| CN106509158A (en) | Healthy blend oil | |
| JP2021119794A (en) | Fading inhibitor for green food product | |
| EP2053922B1 (en) | Baked fruit filled bar fortified with omega-3 fatty acids and process for making same | |
| Ghazali et al. | Oxidative stability of virgin coconut oil compared with RBD palm olein in deep-fat frying of fish crackers | |
| CN111248291A (en) | Compound nut beverage with balanced essential fatty acid proportion and preparation method thereof | |
| US3489573A (en) | Preparation of colored fatty compositions | |
| CN101530137A (en) | Novel edible oil for rice and method for preparing same | |
| CN113875827A (en) | Formula edible oil | |
| CN106889211A (en) | A kind of method for improving edible oil and fat frost resistance | |
| CN103181423B (en) | Plant-lard for food baking and preparation method thereof | |
| CN111513145A (en) | Edible blend oil containing lutein ester and preparation method thereof | |
| Ghazzawi et al. | Impact of roasting and frying on fatty acids, and other valuable compounds present in peanuts. | |
| EP3413726B1 (en) | Vitamin composition | |
| JP6572046B2 (en) | Edible oil and fat composition, method for producing the same, and method for producing cooked food | |
| CN110584059A (en) | Sesame paste and preparation method thereof | |
| JP6971550B2 (en) | Mayonnaise-like food oil composition and mayonnaise-like food | |
| JP6512811B2 (en) | Isolated liquid seasoning | |
| Li et al. | Impact of additives on the formation of thermally induced trans linoleic acid in peanut oil | |
| CN104905366A (en) | Sunflower seed butter containing plant protein drink and preparation method thereof | |
| KR20160041827A (en) | Mixed nuts oil composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |