CN102276297B - Initiator used in rapid-dissolving boron fertilizer production, and preparation technology thereof - Google Patents
Initiator used in rapid-dissolving boron fertilizer production, and preparation technology thereof Download PDFInfo
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- CN102276297B CN102276297B CN 201110149922 CN201110149922A CN102276297B CN 102276297 B CN102276297 B CN 102276297B CN 201110149922 CN201110149922 CN 201110149922 CN 201110149922 A CN201110149922 A CN 201110149922A CN 102276297 B CN102276297 B CN 102276297B
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Abstract
The invention relates to an initiator used in rapid-dissolving boron fertilizer production, and a preparation technology thereof. The provided initiator is used in rapid-dissolving boron fertilizer production for improving the boron fertilizer production efficiency and reducing the boron fertilizer production time. A preparation technology of the initiator is also provided by the invention. The initiator used in rapid-dissolving boron fertilizer production is prepared from components of, by weight: 4 to 9 parts of boric acid and 5 to 11 parts of polyhydric alcohol. The preparation method comprises steps that: (1) the raw materials are added into a container according to the weight ratio, and the raw materials are well mixed; (2) the container is placed in a solution tank of an ultrasonic generator; (3) the frequency of the ultrasonic generator is set at 20 to 40KHz, and ultrasonic oscillation is carried out upon the mixture until the substance in the container is in a state of viscousfluid with no visible crystal, such that the initiator used in rapid-dissolving boron fertilizer production is obtained.
Description
Technical field
The present invention relates to the boron fertilizer production in the agricultural cience and farming techniques, particularly a kind of initiator and manufacture craft thereof for instant boric fertilizer production.
Background technology
Boron is as one of necessary nutritive element of growth and development of plants, and is very important in agriculture production.In the trace element that plants needs, the shortage of boron is the most general, and crop is also very urgent to the demand of boron.Investigation shows, plough reach more than 700,000,000 mu of serious boron deficiency of China accounts for nearly 40% of China's cultivated area.If do not use boron fertilizer on these are ploughed, serious boron deficiency symptom can appear in most of crops, such as " the rotten worry " of beet, " colored and unreal " disease of cotton, and " flower bud and do not spend " diseases of rape etc. also have nearly 500,000,000 mu of slight boron deficiencies of arable soil in addition.Though can not produce obvious boron deficiency symptom at these kind plants of ploughing, can affect the yield and quality of crop.As seen China's all boron deficiencies of ploughing more than 70%.The fruit tree of China all is planted on the more barren mountain region still more, and the shortage of boron is even more serious.Therefore using boron fertilizer a lot of areas and crop in China's agriculture production has been a kind of routinely measure.
Be manufacture craft in a kind of boron fertilizer of CN100434400C patent document and preparation method thereof such as grant number: with boric acid, sodium tetraborate, boron trioxide after potassium hydroborons and catalyzer fully mix, carries out preheating to said mixture, dries wherein moisture; Said mixture is contracted under 300～800 ℃ and reacted 2～8 hours; After above-mentioned reaction is finished, product is pulverized.
Present boron fertilizer is produced multiplex borax and boric acid and is mixed for a long time under hot conditions and react, and needs a large amount of heat energy, and production cost is very high, is unfavorable for the energy-saving and emission-reduction work of enterprise; And the production time is generally long, contracting and reaction needed 2～8 hours, and production efficiency is lower, and product competitiveness is low, is unfavorable for market competition.
Summary of the invention
The present invention aims to provide a kind of raising boron fertilizer production efficiency, shortens initiator and manufacture craft thereof that the boron fertilizer production time is used for instant boric fertilizer production.
In order to realize the foregoing invention purpose, the technical scheme of employing is as follows: be used for the initiator that instant boric fertilizer is produced, made by following raw material weight component: 4～9 parts of boric acid, 5～11 parts of polyhydroxy-alcohols; Described polyhydroxy-alcohol is glycerine, glycol ether or ethylene glycol.
The manufacture craft of the initiator of producing for instant boric fertilizer of the present invention is as follows:
(1) with raw material by weight component pack into and mix in the container;
(2) said vesse is placed the solution pool of ultrasonic generator;
(3) frequency that ultrasonic generator is set is carried out ultra-sonic oscillation at 20～40KHz to mixture, namely obtains the initiator produced for instant boric fertilizer until the material in the container is viscous fluid without visible crystals.
The material of described container is stainless steel, glass, plastics.
Solution in the described solution pool is water, scavenging solution.
The present invention has following beneficial effect:
1, in the production of instant boric fertilizer, adds initiator of the present invention, various raw materials just can be reacted under general condition, do not need the condition of high temperature, saved a large amount of heat energy, reduced production cost, be conducive to the energy-saving and emission-reduction work of enterprise, product competitiveness is strong.
2, in the production of instant boric fertilizer, add initiator of the present invention, effectively shortened the time that condensation reaction needs, enhance productivity.
3, initiator of the present invention, reaction conditions only needs ultra-sonic oscillation, and the reaction times is short; Under Ultrasonic Conditions, initiator is more even.
Specific embodiment
Embodiment 1
Be used for the initiator that instant boric fertilizer is produced, made by following raw material weight component: 4 parts of boric acid, 5 parts of glycerine.Manufacture craft is as follows:
(1) gets 4 parts of boric acid, mix in 5 parts of stainless steel casks of packing into of glycerine;
(2) above-mentioned stainless steel cask is placed the pond of ultrasonic generator;
(3) frequency that ultrasonic generator is set is carried out ultra-sonic oscillation at 20KHz to mixture, namely obtains the initiator produced for instant boric fertilizer until the material in the stainless steel cask is viscous fluid without visible crystals.
Embodiment 2
Be used for the initiator that instant boric fertilizer is produced, made by following raw material weight component: 5 parts of boric acid, 8 parts of glycol ethers.Manufacture craft is as follows:
(1) gets 5 parts of boric acid, mix in 8 parts of glasswares of packing into of glycol ether;
(2) above-mentioned glassware is placed the pond of ultrasonic generator;
(3) frequency that ultrasonic generator is set is carried out ultra-sonic oscillation at 28KHz to mixture, namely obtains the initiator produced for instant boric fertilizer until the material in the glassware is viscous fluid without visible crystals.
Embodiment 3
Be used for the initiator that instant boric fertilizer is produced, made by following raw material weight component: 9 parts of boric acid, 11 parts of ethylene glycol.Manufacture craft is as follows:
(1) gets 9 parts of boric acid, mix in 11 parts of plastic tub of packing into of ethylene glycol;
(2) above-mentioned plastic tub is placed the cleaning liquid pool of ultrasonic generator;
(3) frequency that ultrasonic generator is set is carried out ultra-sonic oscillation at 40KHz to mixture, namely obtains the initiator produced for instant boric fertilizer until the material in the plastic tub is viscous fluid without visible crystals.
Claims (1)
1. be used for the initiator that instant boric fertilizer is produced, it is characterized in that: made by following raw material weight component: 4～9 parts of boric acid, 5～11 parts of polyhydroxy-alcohols; Described polyhydroxy-alcohol is glycerine, glycol ether or ethylene glycol; Its manufacture craft may further comprise the steps:
(1) with raw material by weight component pack into and mix in the container;
(2) said vesse is placed the solution pool of ultrasonic generator;
(3) frequency that ultrasonic generator is set is carried out ultra-sonic oscillation at 20～40KHz to mixture, namely obtains the initiator produced for instant boric fertilizer until the material in the container is viscous fluid without visible crystals.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110149922 CN102276297B (en) | 2011-06-07 | 2011-06-07 | Initiator used in rapid-dissolving boron fertilizer production, and preparation technology thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110149922 CN102276297B (en) | 2011-06-07 | 2011-06-07 | Initiator used in rapid-dissolving boron fertilizer production, and preparation technology thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102276297A CN102276297A (en) | 2011-12-14 |
| CN102276297B true CN102276297B (en) | 2013-04-10 |
Family
ID=45102091
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110149922 Expired - Fee Related CN102276297B (en) | 2011-06-07 | 2011-06-07 | Initiator used in rapid-dissolving boron fertilizer production, and preparation technology thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102276297B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102584410A (en) * | 2011-01-07 | 2012-07-18 | 徐巍 | Novel preparation method of liquid boron fertilizer and liquid boron fertilizer |
| CN113968754A (en) * | 2021-09-29 | 2022-01-25 | 河北昊德生物科技有限公司 | Initiator for producing instant boron fertilizer and preparation process thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5928672A (en) * | 1996-03-28 | 1999-07-27 | Hammons; Barry D. | Polyborate composition |
| CN100491295C (en) * | 2005-06-07 | 2009-05-27 | 董吉山 | Chelated aqueous formulation boron fertilizer |
| CN1328226C (en) * | 2005-12-15 | 2007-07-25 | 安徽省农望农业科技开发有限公司 | Instant soluble leaf-surface sprayed boric fertilizer and its production method |
| CN1903801B (en) * | 2006-07-31 | 2011-05-04 | 朱建烨 | Method of preparing liquid boron fertilizer |
-
2011
- 2011-06-07 CN CN 201110149922 patent/CN102276297B/en not_active Expired - Fee Related
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| Publication number | Publication date |
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| CN102276297A (en) | 2011-12-14 |
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| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130410 |