CN102260764A - Fish oil fatliquoring agent and preparation method thereof - Google Patents
Fish oil fatliquoring agent and preparation method thereof Download PDFInfo
- Publication number
- CN102260764A CN102260764A CN2011101287240A CN201110128724A CN102260764A CN 102260764 A CN102260764 A CN 102260764A CN 2011101287240 A CN2011101287240 A CN 2011101287240A CN 201110128724 A CN201110128724 A CN 201110128724A CN 102260764 A CN102260764 A CN 102260764A
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- CN
- China
- Prior art keywords
- agent
- oil
- fish
- fish oil
- stuffing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000021323 fish oil Nutrition 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 45
- 239000002480 mineral oil Substances 0.000 claims abstract description 7
- 235000010446 mineral oil Nutrition 0.000 claims abstract description 7
- FPYJFEHAWHCUMM-UHFFFAOYSA-N Maleic anhydride Chemical compound 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O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 5
- 230000003647 oxidation Effects 0.000 claims description 8
- 238000007254 oxidation reaction Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 7
- 150000001298 alcohols Chemical class 0.000 claims description 6
- 239000003112 inhibitor Substances 0.000 claims description 6
- 230000002401 inhibitory effect Effects 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 230000003472 neutralizing Effects 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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[C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- 239000010985 leather Substances 0.000 abstract description 15
- 230000000694 effects Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000035943 smell Effects 0.000 abstract description 3
- 235000019525 fullness Nutrition 0.000 abstract description 2
- 230000003078 antioxidant Effects 0.000 abstract 1
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- 239000000835 fiber Substances 0.000 description 1
- ICIWUVCWSCSTAQ-UHFFFAOYSA-M iodate Chemical compound 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[O-]I(=O)=O ICIWUVCWSCSTAQ-UHFFFAOYSA-M 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000005670 sulfation reaction Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Abstract
The invention provides a fish oil fatliquoring agent and a preparation method thereof. The fish oil fatliquoring agent consists of higher alcohol, maleic anhydride, fish oil, an antioxidant, mineral oil, a sulfonating agent, a composite emulsifier and a preservative. By using the fish oil fatliquoring agent, the optical activity resistance and fullness of leather can be improved so as to achieve obtain a satisfied fatliquoring effect, and the fishlike smell of the fish oil fatliquoring agent is light, thus greatly extending the use range of the fish oil fatliquoring agent. The method for preparing the fish oil fatliquoring agent is relatively simple and has no high requirement on equipment and short production period.
Description
Technical field
The present invention relates to a kind of fatting agent and preparation method thereof, more particularly, the present invention relates to a kind of fish-oil stuffing agent and preparation method thereof.
Background technology
Fatting agent is the chemical materials of consumption maximum in the tanning production, also is one of important chemical materials in the leather processing procedure.It can lubricate leather fiber, prevents that leather from stiff, cracking taking place, and can make leather have corresponding toughness and flexibility again, and keep its intensity, play certain filling effect simultaneously, make leather plentiful flexible, we can say that fatting agent is one of important factor that influences the leather quality performance.In fatting agent research, fatty alcohol phosphate, lipid acid high alcohol ester, neat's foot oil, lanolin, natural phospholipid, fish oil, synthetic macromolecule poly phosphate etc. all have good fillibility.The marine animal oil fatting agent that with fish oil is representative is the bulk product in the leather fat, the characteristics of fish oil are that degree of unsaturation is big, the iodine number height, the distribution range broad of molecular weight, so fish oil simultaneously has tangible advantage as other vegetable and animals oils of raw material ratio of leather fat.At first, reactions such as oxidation, sulfation and iodate take place in iodine number higher unsaturated acid easily, and reactive behavior is higher, easily make the higher leather greasing material of active quantities, and fish-oil stuffing agent perviousness is strong, and pliability is good, the oiliness foot, and the leather unit elongation after the stuffing is big; Secondly also have performances such as filling preferably.Handle leather with the fish-oil stuffing agent and can make leather keep the softness and the performance of moistening of many decades, this is that other fatting agent can not be compared.But, since more and more higher to the sunproof requirement of leather at present, and natural fish oil contains more unsaturated link(age), easy oxidation discoloration, and have a fish like smell, therefore limited the range of application of fish-oil stuffing agent.
Summary of the invention
The purpose of this invention is to provide a kind of fish-oil stuffing agent, to solve the above-mentioned problems in the prior art, the comprehensive stuffing performance of this fish-oil stuffing agent of the present invention is good, not only can improve the light fastness and the fullness ratio of leather with fish-oil stuffing agent of the present invention, obtain satisfied stuffing effect, and this fish-oil stuffing agent fishy smell road is light, has widened the use range of this fatting agent.
Another object of the present invention provides a kind of preparation method of above-mentioned fish-oil stuffing agent, and this preparation method is simple relatively, and not high to equipment requirements, the production cycle is shorter.
Fish-oil stuffing agent of the present invention is composed of the following components by weight percentage:
The carbon number of above-mentioned higher alcohols is 16～22
Prepare the method for fish-oil stuffing agent of the present invention, form by following steps:
(1) higher alcohols are joined in the 1# reactor, be warmed up to 50～55 ℃, stir adding MALEIC ANHYDRIDE down, be warming up to 85～95 ℃, reacted 2～3 hours, standby;
(2) fish oil is joined in the 2# reactor, add oxidation inhibitor then successively, mineral oil, 30% the sulphonating agent aqueous solution, its weight percent is: oxidation inhibitor 0.3%～0.5%, mineral oil 15%～20%, sulphonating agent 3%～5%; When temperature was raised to 45～55 ℃, adding 1# material in reactor continued to be warmed up to 85～95 ℃, stirred to mix in 1～1.5 hour;
(3) be cooled to 60～65 ℃, in said mixture, add compound emulsifying agent, sanitas;
(4) keep 60～65 ℃ of temperature, in said mixture, add neutralizing agent, regulate pH value 7～9; Slowly add a certain amount of distilled water and make oil-contg 68～72%, fully stirred 1.5～2.5 hours, promptly obtain the fish-oil stuffing agent.
Embodiment
Below by embodiment the present invention is specifically described.
Embodiment 1
The 23kg higher alcohols are joined in the 50L pre-reactor, be warming up to 50 ℃, stir adding 8.5kg MALEIC ANHYDRIDE down, be warming up to 88～92 ℃, reacted 2 hours, standby; 223.5kg fish oil is joined in the 500L enamel reaction still that agitator, thermometer and condenser are housed, then to wherein adding oxidation inhibitor 1.5kg successively, mineral oil 74kg, 30% sulphonating agent aqueous solution 56.5kg; When being warmed up to 48～52 ℃, the material in the adding pre-reactor continues to be warmed up to 85～95 ℃, stirs to mix in 1 hour; Be cooled to 60～65 ℃ then, add compound emulsifying agent 40kg, sanitas 0.5kg; Keep 60～65 ℃ of temperature, add neutralizing agent 25.7kg, regulate pH value 7～9; Slowly add distilled water 10kg and fully stirred 2 hours, cooling discharge obtains oil-contg and is 70% fish-oil stuffing agent 463.2kg.
Embodiment 2
The 23kg higher alcohols are joined in the 50L pre-reactor, be warming up to 55 ℃, stir adding 8.5kg MALEIC ANHYDRIDE down, be warming up to 88～92 ℃, reacted 3 hours, standby; 241.3kg fish oil is joined in the 500L enamel reaction still that agitator, thermometer and condenser are housed, then to wherein adding oxidation inhibitor 1.6kg successively, mineral oil 79.8kg, 30% sulphonating agent aqueous solution 61kg; When being warmed up to 48～52 ℃, the material in the adding pre-reactor continues to be warmed up to 85～95 ℃, stirs to mix in 1.5 hours; Be cooled to 60～65 ℃ then, add compound emulsifying agent 43kg, sanitas 0.5kg; Keep 60～65 ℃ of temperature, add neutralizing agent 27.7kg, regulate pH value 7～9; Slowly add distilled water 19.4kg and fully stirred 2.5 hours, cooling discharge obtains oil-contg and is 72% fish-oil stuffing agent 505.8kg.
Claims (4)
1. fish-oil stuffing agent is characterized in that said composition is composed of the following components by weight percentage:
2. fish-oil stuffing agent according to claim 1, the carbon number that it is characterized in that described higher alcohols is 16～22.
3. the method for preparing the described fish-oil stuffing agent of claim 1 is characterized in that this method is made up of following steps:
(1) higher alcohols are joined in the 1# reactor, be warmed up to 50～55 ℃, stir adding MALEIC ANHYDRIDE down, be warming up to 85～95 ℃, reacted 2～3 hours, standby;
(2) fish oil is joined in the 2# reactor, add oxidation inhibitor then successively, mineral oil, 30% the sulphonating agent aqueous solution, its weight percent is: oxidation inhibitor 0.3%～0.5%, mineral oil 15%～20%, sulphonating agent 3%～5%; When temperature was raised to 45～55 ℃, adding 1# material in reactor continued to be warmed up to 85～95 ℃, stirred to mix in 1～1.5 hour;
(3) be cooled to 60～65 ℃, in said mixture, add compound emulsifying agent, sanitas;
(4) keep 60～65 ℃ of temperature, in said mixture, add neutralizing agent, regulate pH value 7～9; Slowly add a certain amount of distilled water and make oil-contg 68～72%, fully stirred 1.5～2.5 hours, promptly obtain the fish-oil stuffing agent.
4. the method for preparing the fish-oil stuffing agent according to claim 3 is characterized in that adding neutralizing agent, regulates pH value 7～7.5.
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| CN102703623A (en) * | 2012-06-11 | 2012-10-03 | 科凯精细化工（上海）有限公司 | Novel greasing agent for synthetic leather and preparation method for novel greasing agent |
| CN102839238A (en) * | 2012-09-28 | 2012-12-26 | 郑州科信化工有限公司 | Compound fat liquoring agent |
| CN103088169A (en) * | 2013-02-07 | 2013-05-08 | 浙江传化股份有限公司 | Leather comprehensive fat liquor and preparation method of the same |
| CN103695579A (en) * | 2013-11-29 | 2014-04-02 | 江苏中新资源集团有限公司 | Leather mildew-proof fat-liquoring agent and preparation method thereof |
| CN103695577A (en) * | 2013-12-12 | 2014-04-02 | 江门市江海区一言科技有限公司 | Leather care agent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102703623A (en) * | 2012-06-11 | 2012-10-03 | 科凯精细化工（上海）有限公司 | Novel greasing agent for synthetic leather and preparation method for novel greasing agent |
| CN102839238A (en) * | 2012-09-28 | 2012-12-26 | 郑州科信化工有限公司 | Compound fat liquoring agent |
| CN103088169A (en) * | 2013-02-07 | 2013-05-08 | 浙江传化股份有限公司 | Leather comprehensive fat liquor and preparation method of the same |
| CN103088169B (en) * | 2013-02-07 | 2014-10-22 | 浙江传化股份有限公司 | Leather comprehensive fat liquor and preparation method of the same |
| CN103695579A (en) * | 2013-11-29 | 2014-04-02 | 江苏中新资源集团有限公司 | Leather mildew-proof fat-liquoring agent and preparation method thereof |
| CN103695579B (en) * | 2013-11-29 | 2015-09-16 | 宁波江东仑斯福环保科技有限公司 | A kind of Leather mildew-proof fatting agent and preparation method thereof |
| CN103695577A (en) * | 2013-12-12 | 2014-04-02 | 江门市江海区一言科技有限公司 | Leather care agent and preparation method thereof |
| CN103695577B (en) * | 2013-12-12 | 2016-05-25 | 江门市江海区一言科技有限公司 | A kind of leather care products and preparation method thereof |
| CN106676211A (en) * | 2017-01-09 | 2017-05-17 | 南雄西顿化工有限公司 | Preparation method for light-fastness composite leather greasing agent |
| CN109182621A (en) * | 2018-10-08 | 2019-01-11 | 许昌鑫瑞德化工科技有限公司 | A kind of preparation method of sulfonated leather fat |
| CN113755654A (en) * | 2021-10-14 | 2021-12-07 | 四川大学 | Leather fatting agent and preparation method thereof |
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