CN102225037A - Flushing-free foamed anti-bacteria hand washing product containing high-density alcohol and preparation method thereof - Google Patents
Flushing-free foamed anti-bacteria hand washing product containing high-density alcohol and preparation method thereof Download PDFInfo
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- CN102225037A CN102225037A CN2011101601859A CN201110160185A CN102225037A CN 102225037 A CN102225037 A CN 102225037A CN 2011101601859 A CN2011101601859 A CN 2011101601859A CN 201110160185 A CN201110160185 A CN 201110160185A CN 102225037 A CN102225037 A CN 102225037A
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- polydimethylsiloxane
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- polyethylene glycol
- hands
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Abstract
The invention discloses a flushing-free foamed anti-bacteria hand washing product containing high-density alcohol. The hand washing product comprises, by weight, 50-80% of alcohol, 0.5-10% of polydimethylsiloxane polyether copolymer, 0.05-1.0% of polyethylene glycol, 0.01-5% of skin care agent, 0-5% of auxiliary agent and the balance of water. The invention realizes a perfect combination of a high-density type, a foamed type and a flushing-free type. In addition, the polydimethylsiloxane polyether copolymer and polyethylene glycol used in the invention have no stimulation to adult and children skin, smoothing and moisturizing effects, and is safe and nontoxic to use.
Description
Technical field
The present invention relates to the product scope of washing one's hands, relate in particular to a kind of antibacterial product and preparation method of washing one's hands of flushing free foam type that contains alcohol in high concentration.
Background technology
The current antibacterial type product of washing one's hands mainly contains the conventional surfactants type, and as handwashing liquid, the type product of washing one's hands is main component with the conventional surfactants, if use foam pump, can be made into foam type, product needs the water flushing but the type is washed one's hands, and has certain limitation; Another kind is the flushing free type, as the condensation of washing one's hands, be a kind of with the product of washing one's hands of ethanol as antipathogenic composition, this product can be made the flushing free type, but because big than conventional surfactants of the surface tension of ethanol, be difficult to make the antibacterial product of washing one's hands of flushing free foam type, so be difficult to realize the perfect adaptation of alcohol in high concentration type, foam type and three kinds of forms of flushing free type.
Summary of the invention
The object of the present invention is to provide a kind of antibacterial product and preparation method of washing one's hands of flushing free foam type that contains alcohol in high concentration.
Technical scheme of the present invention is: a kind of antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration, and the percentage by weight of this product of washing one's hands is formed and is comprised:
Ethanol 50～80%;
Polydimethylsiloxane copolyether 0.5～10%;
Polyethylene Glycol 0.05～1.0%;
Skin protectant 0.01～5%:
Auxiliary agent 0～5%;
Water surplus.
In a preferred embodiment of the present invention, the percentage by weight of this product of washing one's hands is formed and is comprised:
Ethanol 70～75%;
Polydimethylsiloxane copolyether 0.5～2%;
Polyethylene Glycol 0.05～0.2%;
Skin protectant 0.5～2%;
Auxiliary agent 1～3%;
Water surplus.
In a preferred embodiment of the present invention, the percentage by weight of this product of washing one's hands is formed and is comprised:
Ethanol 72～75%;
Polydimethylsiloxane copolyether 0.8～1.2%;
Polyethylene Glycol 0.1～0.2%;
Skin protectant 1.0～2%;
Auxiliary agent 2%;
Water surplus.
In a preferred embodiment of the present invention, described polydimethylsiloxane copolyether is the PEG-3 polydimethylsiloxane, the PEG-6 polydimethylsiloxane, the PEG-7 polydimethylsiloxane, the PEG-8 polydimethylsiloxane, the PEG-9 polydimethylsiloxane, the PEG-10 polydimethylsiloxane, the PEG-12 polydimethylsiloxane, the PEG-14 polydimethylsiloxane, the PEG-17 polydimethylsiloxane, the PEG/PPG-3/10 polydimethylsiloxane, the PEG/PPG-4/12 polydimethylsiloxane, the PEG/PPG-6/11 polydimethylsiloxane, the PEG/PPG-8/14 polydimethylsiloxane, the PEG/PPG-8/26 polydimethylsiloxane, the PEG/PPG-10/2 polydimethylsiloxane, the PEG/PPG-12/16 polydimethylsiloxane, the PEG/PPG-12/18 polydimethylsiloxane, the PEG/PPG-14/4 polydimethylsiloxane, the PEG/PPG-15/15 polydimethylsiloxane, the PEG/PPG-16/2 polydimethylsiloxane, the PEG/PPG-16/8 polydimethylsiloxane, the PEG/PPG-17/18 polydimethylsiloxane, the PEG/PPG-18/6 polydimethylsiloxane, the PEG/PPG-18/18 polydimethylsiloxane, the PEG/PPG-19/19 polydimethylsiloxane, the PEG/PPG-20/6 polydimethylsiloxane, the PEG/PPG-20/15 polydimethylsiloxane, the PEG/PPG-20/20 polydimethylsiloxane, the PEG/PPG-20/23 polydimethylsiloxane, the PEG/PPG-20/29 polydimethylsiloxane, the PEG/PPG-22/23 polydimethylsiloxane, the PEG/PPG-22/24 polydimethylsiloxane, the PEG/PPG-23/6 polydimethylsiloxane, the PEG/PPG-25/25 polydimethylsiloxane, the PEG/PPG-27/27 polydimethylsiloxane, the PEG/PPG-30/10 polydimethylsiloxane, two-the PEG/PPG-14/14 polydimethylsiloxane, one or more mixing in two-PEG/PPG-18/6 polydimethylsiloxane or the two-PEG/PPG-20/20 polydimethylsiloxane.
In a preferred embodiment of the present invention, described Polyethylene Glycol is one or more mixing among Polyethylene Glycol-2M, Polyethylene Glycol-5M, Polyethylene Glycol-7M, Polyethylene Glycol-9M, Polyethylene Glycol-14M, Polyethylene Glycol-20M, Polyethylene Glycol-23M, Polyethylene Glycol-25M, Polyethylene Glycol-45M, Polyethylene Glycol-65M, Polyethylene Glycol-90M, Polyethylene Glycol-115M, Polyethylene Glycol-160M or the Polyethylene Glycol-180M.
In a preferred embodiment of the present invention, described skin protectant is one or more mixing in low molecular weight polyols or the fat soluble vitamin.
In a preferred embodiment of the present invention, described low molecular weight polyols is one or more mixing in glycerol, propylene glycol or the 1,3 butylene glycol.
In a preferred embodiment of the present invention, described fat soluble vitamin is one or more mixing in vitamin A, vitamin E or the Vitamin E acetate.
In a preferred embodiment of the present invention, described auxiliary agent is one or more mixing in blood circulation accelerant, whitening agent, wetting agent, antiinflammatory, UV absorbent or the antioxidant.
The invention also discloses a kind of preparation method that contains the antibacterial product of washing one's hands of flushing free foam type of alcohol in high concentration, may further comprise the steps:
Take by weighing ethanol, polydimethylsiloxane copolyether, Polyethylene Glycol, skin protectant, auxiliary agent and water by mass percentage;
With polydimethylsiloxane copolyether mix homogeneously, under the state that stirs, add entry successively earlier, Polyethylene Glycol, ethanol, skin protectant, stir, then mixture is poured in the foam pump, promptly get the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration of the present invention.
Compared with prior art, the invention has the beneficial effects as follows: the product foam fine texture of washing one's hands of the present invention, structure is fluffy, and is in stable condition, is difficult for flowing, and in the process of smearing, do not have sticky sense, can not influence use feeling even do not wash also; Alcohol concentration is higher, has good bacteriostatic effect; Because flushing free, the skin protectant of interpolation is substantially all stayed the surface of hands, prevents that skin from cracking from dryness, and skin effect is obvious; The present invention has realized the perfect adaptation of alcohol in high concentration type, foam type and three kinds of forms of flushing free type.In addition, polydimethylsiloxane copolyether that uses among the present invention and Polyethylene Glycol component itself have the adult, child's skin is non-stimulated and have smooth moisturizing effect, and is safe in utilization nontoxic.
The specific embodiment
Below in conjunction with embodiment the present invention is done further specific descriptions.
(1) embodiment 1-5 configuration contains the antibacterial product of washing one's hands of flushing free foam type of alcohol in high concentration, and concrete prescription sees Table 1, and wherein each ratio is weight percentage;
The antibacterial product of washing one's hands of comparative example 1-3 configuration comparative example, concrete prescription sees Table 2, and wherein each ratio is weight percentage;
Table 1
Table 2
In above-mentioned recipe ingredient, the polydimethylsiloxane copolyether is the PEG-3 polydimethylsiloxane, the PEG-6 polydimethylsiloxane, the PEG-7 polydimethylsiloxane, the PEG-8 polydimethylsiloxane, the PEG-9 polydimethylsiloxane, the PEG-10 polydimethylsiloxane, the PEG-12 polydimethylsiloxane, the PEG-14 polydimethylsiloxane, the PEG-17 polydimethylsiloxane, the PEG/PPG-3/10 polydimethylsiloxane, the PEG/PPG-4/12 polydimethylsiloxane, the PEG/PPG-6/11 polydimethylsiloxane, the PEG/PPG-8/14 polydimethylsiloxane, the PEG/PPG-8/26 polydimethylsiloxane, the PEG/PPG-10/2 polydimethylsiloxane, the PEG/PPG-12/16 polydimethylsiloxane, the PEG/PPG-12/18 polydimethylsiloxane, the PEG/PPG-14/4 polydimethylsiloxane, the PEG/PPG-15/15 polydimethylsiloxane, the PEG/PPG-16/2 polydimethylsiloxane, the PEG/PPG-16/8 polydimethylsiloxane, the PEG/PPG-17/18 polydimethylsiloxane, the PEG/PPG-18/6 polydimethylsiloxane, the PEG/PPG-18/18 polydimethylsiloxane, the PEG/PPG-19/19 polydimethylsiloxane, the PEG/PPG-20/6 polydimethylsiloxane, the PEG/PPG-20/15 polydimethylsiloxane, the PEG/PPG-20/20 polydimethylsiloxane, the PEG/PPG-20/23 polydimethylsiloxane, the PEG/PPG-20/29 polydimethylsiloxane, the PEG/PPG-22/23 polydimethylsiloxane, the PEG/PPG-22/24 polydimethylsiloxane, the PEG/PPG-23/6 polydimethylsiloxane, the PEG/PPG-25/25 polydimethylsiloxane, the PEG/PPG-27/27 polydimethylsiloxane, the PEG/PPG-30/10 polydimethylsiloxane, two-the PEG/PPG-14/14 polydimethylsiloxane, one or more mixing in two-PEG/PPG-18/6 polydimethylsiloxane or the two-PEG/PPG-20/20 polydimethylsiloxane.
Polyethylene Glycol is one or more mixing among Polyethylene Glycol-2M, Polyethylene Glycol-5M, Polyethylene Glycol-7M, Polyethylene Glycol-9M, Polyethylene Glycol-14M, Polyethylene Glycol-20M, Polyethylene Glycol-23M, Polyethylene Glycol-25M, Polyethylene Glycol-45M, Polyethylene Glycol-65M, Polyethylene Glycol-90M, Polyethylene Glycol-115M, Polyethylene Glycol-160M or the Polyethylene Glycol-180M.
Skin protectant is one or more mixing in low molecular weight polyols or the fat soluble vitamin, and wherein low molecular weight polyols is one or more mixing in glycerol, propylene glycol or the 1,3 butylene glycol; Fat soluble vitamin is one or more mixing in vitamin A, vitamin E or the Vitamin E acetate; Described auxiliary agent is one or more mixing in blood circulation accelerant, whitening agent, wetting agent, antiinflammatory, UV absorbent or the antioxidant.
(2) embodiment 1-5 preparation method: take by weighing earlier ethanol, polydimethylsiloxane copolyether, Polyethylene Glycol, skin protectant and water by mass percentage; With polydimethylsiloxane copolyether mix homogeneously, under the state that stirs, add entry successively then, Polyethylene Glycol, ethanol, skin protectant, stir, then mixture is poured in the foam pump, promptly get the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration of the present invention;
The collocation method of the antibacterial product of washing one's hands of comparative example 1-3 configuration comparative example is with the collocation method of embodiment 1-5.
(3) form content according to the prescription shown in the comparative example 1-3 of the embodiment 1-5 of table 1 and table 2, and the stability of content is estimated according to the present invention's preparation.Subsequently, emulsion is placed foam pump, and to foam stability and foam quality, sticky sensation, wash back skin sense and fungistatic effect and estimate.The result is respectively as showing in table 3 and the table 4.
Wherein, stability is to place 1 ℃, room temperature, 40 ℃ temperature conditions to preserve 3 months down respectively emulsion, and places 50 ℃ temperature conditions to preserve 1 month down, observes emulsion then respectively and whether has lamination, and estimate according to following benchmark:
Zero: no lamination;
*: lamination is arranged.
Foam stability and foam quality are by 10 panelists, use each skin-protection product, foamy retention time and quality are carried out sensory evaluation, and judge by following standard:
Zero: 7-10 people is evaluated as long, exquisite quality of foam retention time;
*: at least one people is evaluated as foam retention time weak point, quality is fineless and smooth.
Stickyly feel it is, use each skin-protection product, feel to carry out sensory evaluation to foamy use is sticky, and judge by following standard by 10 panelists:
Zero: 7-10 people is evaluated as foam and feels more sticky or not sticky;
*: at least one people is evaluated as foam and feels very sticky.
Washing back skin sense is by 10 panelists, uses each skin-protection product, skin effect is carried out sensory evaluation, and judge by following standard:
Zero: 7-10 people has been evaluated as skin effect;
*: at least one people is evaluated as no skin effect.
Fungistatic effect
Zero: fungistatic effect is obvious;
*: antibacterial or DeGrain.
Table 3
| Performance | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Stability | ?○ | ?○ | ?○ | ?○ | ?○ |
| Foam stability and foam quality | ?○ | ?○ | ?○ | ?○ | ?○ |
| Sticky sensation | ?○ | ?○ | ?○ | ?○ | ?○ |
| Skin effect | ?○ | ?○ | ?○ | ?○ | ?○ |
| Fungistatic effect | ?○ | ?○ | ?○ | ?○ | ?○ |
Table 4
| Performance | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Stability | ○ | ○ | ○ |
| Foam stability and foam quality | × | ○ | ○ |
| Sticky sensation | × | ○ | × |
| Skin effect | ○ | ○ | × |
| Fungistatic effect | × | × | ○ |
From table 3 embodiment 1-5 and table 4 Comparative Examples 1-3 as can be known, press this product of embodiment 1-5 invention, by foam pump, can form the foam of fine texture, and can play good skin effect and fungistatic effect.
The above; it only is the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (10)
1. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration is characterized in that, the percentage by weight of this product of washing one's hands is formed and comprised:
Ethanol 50～80%;
Polydimethylsiloxane copolyether 0.5～10%;
Polyethylene Glycol 0.05～1.0%;
Skin protectant 0.01～5%;
Auxiliary agent 0～5%;
Water surplus.
2. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 1 is characterized in that, the percentage by weight of this product of washing one's hands is formed and comprised:
Ethanol 70～75%;
Polydimethylsiloxane copolyether 0.5～2%;
Polyethylene Glycol 0.05～0.2%;
Skin protectant 0.5～2%;
Auxiliary agent 1～3%;
Water surplus.
3. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 2 is characterized in that, the percentage by weight of this product of washing one's hands is formed and comprised:
Ethanol 72～75%;
Polydimethylsiloxane copolyether 0.8～1.2%;
Polyethylene Glycol 0.1～0.2%;
Skin protectant 1.0～2%;
Auxiliary agent 2%;
Water surplus.
4. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 1, it is characterized in that described polydimethylsiloxane copolyether is the PEG-3 polydimethylsiloxane, the PEG-6 polydimethylsiloxane, the PEG-7 polydimethylsiloxane, the PEG-8 polydimethylsiloxane, the PEG-9 polydimethylsiloxane, the PEG-10 polydimethylsiloxane, the PEG-12 polydimethylsiloxane, the PEG-14 polydimethylsiloxane, the PEG-17 polydimethylsiloxane, the PEG/PPG-3/10 polydimethylsiloxane, the PEG/PPG-4/12 polydimethylsiloxane, the PEG/PPG-6/11 polydimethylsiloxane, the PEG/PPG-8/14 polydimethylsiloxane, the PEG/PPG-8/26 polydimethylsiloxane, the PEG/PPG-10/2 polydimethylsiloxane, the PEG/PPG-12/16 polydimethylsiloxane, the PEG/PPG-12/18 polydimethylsiloxane, the PEG/PPG-14/4 polydimethylsiloxane, the PEG/PPG-15/15 polydimethylsiloxane, the PEG/PPG-16/2 polydimethylsiloxane, the PEG/PPG-16/8 polydimethylsiloxane, the PEG/PPG-17/18 polydimethylsiloxane, the PEG/PPG-18/6 polydimethylsiloxane, the PEG/PPG-18/18 polydimethylsiloxane, the PEG/PPG-19/19 polydimethylsiloxane, the PEG/PPG-20/6 polydimethylsiloxane, the PEG/PPG-20/15 polydimethylsiloxane, the PEG/PPG-20/20 polydimethylsiloxane, the PEG/PPG-20/23 polydimethylsiloxane, the PEG/PPG-20/29 polydimethylsiloxane, the PEG/PPG-22/23 polydimethylsiloxane, the PEG/PPG-22/24 polydimethylsiloxane, the PEG/PPG-23/6 polydimethylsiloxane, the PEG/PPG-25/25 polydimethylsiloxane, the PEG/PPG-27/27 polydimethylsiloxane, the PEG/PPG-30/10 polydimethylsiloxane, two-the PEG/PPG-14/14 polydimethylsiloxane, one or more mixing in two-PEG/PPG-18/6 polydimethylsiloxane or the two-PEG/PPG-20/20 polydimethylsiloxane.
5. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 1, it is characterized in that described Polyethylene Glycol is one or more mixing among Polyethylene Glycol-2M, Polyethylene Glycol-5M, Polyethylene Glycol-7M, Polyethylene Glycol-9M, Polyethylene Glycol-14M, Polyethylene Glycol-20M, Polyethylene Glycol-23M, Polyethylene Glycol-25M, Polyethylene Glycol-45M, Polyethylene Glycol-65M, Polyethylene Glycol-90M, Polyethylene Glycol-115M, Polyethylene Glycol-160M or the Polyethylene Glycol-180M.
6. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 1 is characterized in that, described is one or more mixing in low molecular weight polyols or the fat soluble vitamin.
7. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 6 is characterized in that described low molecular weight polyols is one or more mixing in glycerol, propylene glycol or the 1,3 butylene glycol.
8. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 6 is characterized in that described fat soluble vitamin is one or more mixing in vitamin A, vitamin E or the Vitamin E acetate.
9. the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration according to claim 1, it is characterized in that described auxiliary agent is one or more mixing in blood circulation accelerant, whitening agent, wetting agent, antiinflammatory, UV absorbent or the antioxidant.
10. a preparation method that contains the antibacterial product of washing one's hands of flushing free foam type of alcohol in high concentration according to claim 1 is characterized in that, may further comprise the steps:
(1) takes by weighing ethanol, polydimethylsiloxane copolyether, Polyethylene Glycol, skin protectant, auxiliary agent and water by mass percentage;
(2), under the state that stirs, add entry successively with polydimethylsiloxane copolyether mix homogeneously, Polyethylene Glycol, ethanol, skin protectant, stir, then mixture is poured in the foam pump, promptly get the antibacterial product of washing one's hands of flushing free foam type that contains alcohol in high concentration of the present invention.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110160185A CN102225037B (en) | 2011-06-15 | 2011-06-15 | Flushing-free foamed anti-bacteria hand washing product containing high-density alcohol and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110160185A CN102225037B (en) | 2011-06-15 | 2011-06-15 | Flushing-free foamed anti-bacteria hand washing product containing high-density alcohol and preparation method thereof |
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| Publication Number | Publication Date |
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| CN102225037A true CN102225037A (en) | 2011-10-26 |
| CN102225037B CN102225037B (en) | 2012-10-03 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104244921A (en) * | 2012-04-30 | 2014-12-24 | 金伯利-克拉克环球有限公司 | Foaming formulations including silicone polyesters |
| CN109288728A (en) * | 2018-11-27 | 2019-02-01 | 南通优护优家卫生用品有限公司 | The alcohol disinfecting agent that can be foamed |
-
2011
- 2011-06-15 CN CN201110160185A patent/CN102225037B/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104244921A (en) * | 2012-04-30 | 2014-12-24 | 金伯利-克拉克环球有限公司 | Foaming formulations including silicone polyesters |
| CN104244921B (en) * | 2012-04-30 | 2017-03-01 | 金伯利-克拉克环球有限公司 | Comprise the effervescent preparations of silicone polyester |
| CN109288728A (en) * | 2018-11-27 | 2019-02-01 | 南通优护优家卫生用品有限公司 | The alcohol disinfecting agent that can be foamed |
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| Publication number | Publication date |
|---|---|
| CN102225037B (en) | 2012-10-03 |
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Effective date of registration: 20200421 Address after: 215500 Xinzhuang section, provincial road 227, Changshu City, Suzhou City, Jiangsu Province Patentee after: Suzhou Crowley Cosmetics Co., Ltd. Address before: 215555, Suzhou, Jiangsu province Changshu Xinzhuang Town Lung nilfisk bio Industrial Park Patentee before: JIANGSU LONGRICH BIOTECH Co.,Ltd. |
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Address after: 215500 Xinzhuang section of 227 provincial road, Changshu City, Suzhou City, Jiangsu Province Patentee after: Crowley Cosmetics Co.,Ltd. Address before: 215500 Xinzhuang section of 227 provincial road, Changshu City, Suzhou City, Jiangsu Province Patentee before: Suzhou Crowley Cosmetics Co.,Ltd. |
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