CN102175819A - Method for characterizing monomer tobacco style characteristics based on tobacco aromatic components - Google Patents
Method for characterizing monomer tobacco style characteristics based on tobacco aromatic components Download PDFInfo
- Publication number
- CN102175819A CN102175819A CN2011100220239A CN201110022023A CN102175819A CN 102175819 A CN102175819 A CN 102175819A CN 2011100220239 A CN2011100220239 A CN 2011100220239A CN 201110022023 A CN201110022023 A CN 201110022023A CN 102175819 A CN102175819 A CN 102175819A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- note
- aromatic components
- aroma
- varieties
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Abstract
The invention relates to a method for characterizing monomer tobacco style characteristics based on tobacco aromatic components, and belongs to the technical field of tobacco quality evaluation. The method comprises the following steps: a, comparing and analyzing the aroma characteristics of various varieties by utilizing a radar chart, wherein in the radar chart, each data has an independent single numerical shaft, coordinate axes are distributed around the centre point radially, and the points of the value of the same data sequence on different coordinate axes are connected by fold line, so as to form the radar chart which is used for comparing the overall conditions of a plurality of data sequence indexes; and b, detecting aromatic components of different varieties in the same region, and performing multiple comparison on the contents of the aromatic components, so as to detect the differences of each variety with other varieties between various processes; and eliminating indistinctive indexes, and finding out the material basis causing aroma differences between varieties from the contents of the aromatic components. By utilizing the method, the quantitative and objective characterization of various aroma indexes of cured tobaccos is realized, and a material basis for deciding the aroma characteristics of tobaccos is found out.
Description
Technical field:
The present invention relates to objectively characterize the method for the style and features of monomer tobacco leaf, belong to quality of tobacco assessment technique field with the tobacco leaf aroma component.
Background technology:
Aroma component is one of fundamental content of tobacco leaf interior quality, and the kind and the content of the style and features of tobacco leaf and tobacco leaf flavor matter are closely related.At present, to more with qualitative description of the research of note feature
[1,2], to the rarely seen report of the research of its quantification,
List of references:
[1] father-in-law Xiyang, Liu Yi, Xu Jianming, etc.Fragrance profile analysis method is commented application [A] in the perfume (or spice) at cigarette.Industry Professional Committee of Chinese tobacco association 2005 tobacco chemistry scientific seminar papers [C].Industry Professional Committee of Chinese tobacco association tobacco chemistry scientific seminar collection of thesis, 2005:461-464.
[2] the anxious generation of Zhao, Yuan Haiping.Shallow opinion tobacco leaf resource is to the influence [A] of cigarette brand expansion.The 5th council's third session of Chinese tobacco association and academic annual meeting meeting paper [C].China momentous conference paper full-text database, 2006:357-359.
[3] Zhou Jiheng, Yang Hongqi, Lin Guihua, etc.Main volatile Study on Aroma Compounds [J] in the different flue-cured tobacco growing district tobacco leaves.Agricultural University Of Hunan's journal (natural science edition), 2004,30 (1): 20-23.
[4] in for army building, Yang Hanwen, Bi Qingwen, etc.The canonical correlation analysis [J] of neutral aroma component of flue-cured tobacco and aroma quality.Gansu Agriculture University,'s journal, 2009, (02): 72-76.
[5] Wang Yaofu, Gao Huajun, Liu Guoshun, etc.The comparative analysis [J] of different genotype flue-cured tobacco blade flavor matter content.China's agronomy circular, 2005,21 (5): 117-120.
[6] in for army building, appoint Xiao Hong, Xia Lin, etc.The neutral flavor matter analysis [J] of " Jin Panxi " high-quality cigarette development area flue-cured tobacco.The Chinese tobacco science, 2005, (4): 11-13.
[7] Xian Kefa, Shen Chaozhi, Qi Wanmin, etc.Yunnan Flue-cured Tobacco neutral flavor species analysis research [J].The Chinese tobacco journal, 1992, (2): 1-9.
Summary of the invention:
The objective of the invention is to overcome the deficiency of prior art, and a kind of method that characterizes monomer tobacco leaf style and features based on the tobacco leaf aroma component is provided.
Method based on tobacco leaf aroma component sign monomer tobacco leaf style and features of the present invention, concrete steps are as follows:
A. identify by the sensory evaluating smoking that contrast characterizes the calibration sample of note power, and the tobacco leaf note that sensory evaluation goes out is quantitatively composed branch; That is: adopt radar map to come the note characteristics of each kind of comparative analysis, in radar map, each data all has an independently single number line, coordinate axis is distributed in around the central point radially, it is exactly radar map that the point of the value of same data sequence on different coordinate axis coupled together formed polygon with broken line, be used for the comparison several number according to the general status of sequence indicator, and the assignment of each index illustrates that the closer to the center of circle these note characteristics are more outstanding; Otherwise, illustrate that then the note characteristics are the most outstanding;
B. same kind aroma component is from different places detected, content to aroma component compares again, to check between each handles---every kind and other kind difference between in twos, reject inapparent index, seek the material base that causes note difference between kind from flavor matter content aspect.
The foundation of the inventive method, for providing a kind of, the evaluation of flue-cured tobacco note feature characterizes with radar map, can carry out quantitative analysis to flue-cured tobacco note feature, solving flue-cured tobacco note feature can only qualitative description and can not quantitative comparison and by qualitative problem to quantitative conversion, has realized the various note indexs of objective sign flue-cured tobacco; By note score value and the correlation analysis of aroma component content, find out the material base of decision tobacco leaf note feature to tobacco leaf.
The sample of the inventive method analysis can expand to other type tobacco leaf, as: burley tobaccos, Turkish tobaccos.
Description of drawings:
Fig. 1 shows the main note feature of NC297.
Fig. 2 shows NC102 note feature.
Fig. 3 shows red big note feature.
Fig. 4 shows K326 note feature.
Embodiment:
The present invention is described further below in conjunction with concrete embodiment, but is not restriction the present invention.
Kind NC102, NC297 note signature analysis draw in 1 U.S.A
Adopt radar map to come the note characteristics of each kind of comparative analysis, see Fig. 1,2,3 and 4.In radar map, each data all has an independently single number line, coordinate axis is distributed in around the central point radially, it is exactly radar map that the point of the value of same data sequence on different coordinate axis coupled together formed polygon with broken line, is used for the general status of comparison several number according to sequence indicator.The assignment of each index illustrates that the closer to the center of circle these note characteristics are not outstanding more; Otherwise, illustrate that then the note characteristics are the most outstanding.
Know that by Fig. 1 the note of NC297 is mainly with delicate fragrance, fragrant and sweet, Jiao Tianwei master, and fresh and sweet and sweet sense is more outstanding, but the fragrance of a flower and Xin Xiang are not outstanding.
Know that by Fig. 2 the note of NC102 is mainly abundanter based on fragrant and sweet, delicate fragrance and burnt odor, fruital, but the banksia rose and the fragrance of a flower are outstanding.
Know that by Fig. 3 red big note is mainly with delicate fragrance, fragrant and sweet, Jiao Tianwei master, and the banksia rose is comparatively outstanding, but hay is fragrant and the fragrance of a flower is not outstanding.
Know by Fig. 4, K326 mainly based on delicate fragrance, burnt odor and fragrant and sweet, fruital than horn of plenty, but hay is fragrant and hot perfume (or spice) is not given prominence to.
2 aroma component analyses
The flavor matter composition is a lot of in the flue-cured tobacco, the contribution of tabacco fragrance is had nothing in common with each other, though some content of material is not high, can be the important source of some characteristic perfume.The flavor matter of flue-cured tobacco is the important chemical composition that is used for the tabacco fragrance evaluation study at present, also is one of important indicator that tobacco incense makings, perfume quantity and odor type style are estimated
[3-7]By same kind aroma component is from different places contained amount comparing analysis, seek the material base that causes note difference between kind from flavor matter content aspect.
Aroma component among red big, NC297, NC102 and the K326 is detected, 70 kinds of identical aroma components (seeing Table 1) are wherein arranged, content to these 70 kinds of aroma components carries out multiple ratio, to check between each handles---every kind and other kind difference between in twos, reject inapparent index gained and the results are shown in Table 2.Have the content of 28 kinds of aroma components to reach the level of signifiance in the table 2, wherein the letones large percentage has 13 kinds, secondly has 4 kinds for alcohols.
Flavor matter average content (μ g/g) in table 1 red big, NC297, NC102 and the K326 sample
Table 2 aroma component content multiple ratio is (μ g/g)
Annotate: under 0.05 level of signifiance.
From table 2, NC297 has the content of 17 kinds of flavor matters to reach the level of signifiance with red big the comparing with K326 of reference substance kind; Find that to NC297 flavor matter content analysis the time some can make the more outstanding flavor matter content of delicate fragrance note be higher than even are significantly higher than other kinds, as firpene, linalool, and phenylethyl alcohol.
NC102 has the content of 13 kinds of flavor matters to compare (red big and K326) with 2 reference substance kinds to have reached the level of signifiance.Some flavor matter content such as geraniol are significantly higher than the content of other 3 kinds among the NC102, and these flavor matters are the more outstanding reasons of fragrant and sweet rhythm.The content of some flavor matters such as the citrene among the NC102, benzaldehyde is higher to be to cause the reason of its fruital note than horn of plenty.Class content of material such as red big-and-middle guaiacol are significantly higher than NC102, and this is the reason that causes the red big banksia rose more more outstanding than NC102.
NC102 and NC297 are bigger and the K326 hay is fragrant outstanding than red, and some can make the fragrant flavor matter content of giving prominence to higher relevant (as gamma-valerolactone) of hay with gamma-valerolactone.
Claims (1)
1. the method based on tobacco leaf aroma component sign monomer tobacco leaf style and features is characterized in that this method is: identify that by the sensory evaluating smoking contrast characterizes the calibration sample of note power, and the tobacco leaf note that sensory evaluation goes out is quantitatively composed branch; That is: adopt radar map to come the note characteristics of each kind of comparative analysis, in radar map, each data all has an independently single number line, coordinate axis is distributed in around the central point radially, it is exactly radar map that the point of the value of same data sequence on different coordinate axis coupled together formed polygon with broken line, be used for the comparison several number according to the general status of sequence indicator, and the assignment of each index illustrates that the closer to the center of circle these note characteristics are more outstanding; Otherwise, illustrate that then the note characteristics are the most outstanding; Same kind aroma component is from different places detected, content to aroma component compares again, to check between each handles---every kind and other kind difference between in twos, reject inapparent index, cause the material base of note difference between kind from the searching of flavor matter content aspect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100220239A CN102175819A (en) | 2011-01-19 | 2011-01-19 | Method for characterizing monomer tobacco style characteristics based on tobacco aromatic components |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100220239A CN102175819A (en) | 2011-01-19 | 2011-01-19 | Method for characterizing monomer tobacco style characteristics based on tobacco aromatic components |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102175819A true CN102175819A (en) | 2011-09-07 |
Family
ID=44519024
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011100220239A Pending CN102175819A (en) | 2011-01-19 | 2011-01-19 | Method for characterizing monomer tobacco style characteristics based on tobacco aromatic components |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102175819A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102590460A (en) * | 2012-03-05 | 2012-07-18 | 昆明理工大学 | Method for rating of raw milk quality |
| CN103593561A (en) * | 2013-11-10 | 2014-02-19 | 云南瑞升烟草技术（集团）有限公司 | Method for representing style characteristics of tobacco by adopting characteristic indexes |
| CN105335734A (en) * | 2015-11-24 | 2016-02-17 | 云南中烟工业有限责任公司 | Star-graph identification method of cigarette flavor characteristics |
| CN105512672A (en) * | 2015-11-24 | 2016-04-20 | 云南中烟工业有限责任公司 | Star graph identification method for cigarette quality characteristics |
| CN105572313A (en) * | 2015-10-12 | 2016-05-11 | 中国农业科学院北京畜牧兽医研究所 | Method for grading quality of fresh and raw milk |
| CN109884202A (en) * | 2019-03-05 | 2019-06-14 | 湖北中烟工业有限责任公司 | A kind of evaluation method and application heating the low temperature cigarette essence that do not burn |
-
2011
- 2011-01-19 CN CN2011100220239A patent/CN102175819A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102590460A (en) * | 2012-03-05 | 2012-07-18 | 昆明理工大学 | Method for rating of raw milk quality |
| CN102590460B (en) * | 2012-03-05 | 2015-05-20 | 昆明理工大学 | Method for rating of raw milk quality |
| CN103593561A (en) * | 2013-11-10 | 2014-02-19 | 云南瑞升烟草技术（集团）有限公司 | Method for representing style characteristics of tobacco by adopting characteristic indexes |
| CN103593561B (en) * | 2013-11-10 | 2016-08-17 | 云南瑞升烟草技术（集团）有限公司 | A kind of method using characteristic index to characterize tobacco style feature |
| CN105572313A (en) * | 2015-10-12 | 2016-05-11 | 中国农业科学院北京畜牧兽医研究所 | Method for grading quality of fresh and raw milk |
| CN105335734A (en) * | 2015-11-24 | 2016-02-17 | 云南中烟工业有限责任公司 | Star-graph identification method of cigarette flavor characteristics |
| CN105512672A (en) * | 2015-11-24 | 2016-04-20 | 云南中烟工业有限责任公司 | Star graph identification method for cigarette quality characteristics |
| CN109884202A (en) * | 2019-03-05 | 2019-06-14 | 湖北中烟工业有限责任公司 | A kind of evaluation method and application heating the low temperature cigarette essence that do not burn |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Cheng | Chemical evaluation of electronic cigarettes | |
| CN102175819A (en) | Method for characterizing monomer tobacco style characteristics based on tobacco aromatic components | |
| Stepanov et al. | Carcinogenic tobacco-specific N-nitrosamines in US cigarettes: three decades of remarkable neglect by the tobacco industry | |
| CN103217408B (en) | Method for identifying two flue-cured tobaccos with different odor types in Guizhou | |
| Xiao et al. | Characterization of key aroma compounds from different rose essential oils using gas chromatography-mass spectrometry, gas chromatography–olfactometry and partial least squares regression | |
| Marcilla et al. | Comparative study of the main characteristics and composition of the mainstream smoke of ten cigarette brands sold in Spain | |
| Yang et al. | Characterization and discrimination of premium‐quality, waxy, and black‐pigmented rice based on odor‐active compounds | |
| CN108685150B (en) | Cigarette digital flavoring method based on flavor components | |
| CN108845085A (en) | A method of tobacco leaf odor type is predicted based on tobacco leaf chemical composition | |
| CN107784452A (en) | A kind of objective integrated evaluating method of tobacco style characteristic similarity | |
| CN103892435B (en) | Method for preparing tobacco powder raw materials and stabilizing quality of reconstituted tobacco | |
| Gröger et al. | Application of comprehensive two‐dimensional gas chromatography mass spectrometry and different types of data analysis for the investigation of cigarette particulate matter | |
| Prasetyo et al. | Variations in anatomical characteristics and predicted paper quality of three Eucalyptus species planted in Indonesia | |
| Yin et al. | Identification of aroma types and their characteristic volatile compounds of Chinese faint-scent cigarettes based on descriptive sensory analysis and GC–MS and partial least squares regression | |
| Mowitz et al. | Patch testing with serial dilutions and thin‐layer chromatograms of oak moss absolutes containing high and low levels of atranol and chloroatranol | |
| Buttery et al. | Cooked carrot volatiles. AEDA and odor activity comparisons. Identification of linden ether as an important aroma component | |
| CN114689746B (en) | Method, device, electronic equipment and medium for screening tobacco extract characteristics | |
| Klupinski et al. | Chemical characterization of marijuana blunt smoke by non-targeted chemical analysis | |
| CN102680427A (en) | Method for identifying surface fragrance quality of cigarettes by near infrared spectral analysis technology | |
| Stepanov et al. | Variations of toxic and carcinogenic constituents in nasvai: call for systematic research and regulation | |
| Lee et al. | Analytical method for measurement of tobacco-specific nitrosamines in E-cigarette liquid and aerosol | |
| CN106198861B (en) | A kind of method of quantitatively evaluating cigarette shreds and humectant compatibility | |
| Gan et al. | Chinese “herbal” cigarettes are as carcinogenic and addictive as regular cigarettes | |
| CN109164180B (en) | Method for distinguishing Mark of Masuria cheese identity based on decision tree extraction features | |
| CN106802331A (en) | 19 kinds of methods of sootiness perfume composition in heating non-burning cigarette smoke are determined simultaneously |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110907 |