CN102103046B - Ball bladder sampling device and sampling method - Google Patents

Ball bladder sampling device and sampling method Download PDF

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CN102103046B
CN102103046B CN2011100262157A CN201110026215A CN102103046B CN 102103046 B CN102103046 B CN 102103046B CN 2011100262157 A CN2011100262157 A CN 2011100262157A CN 201110026215 A CN201110026215 A CN 201110026215A CN 102103046 B CN102103046 B CN 102103046B
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bladders
sampling
stop valve
gas
flexible pipe
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CN102103046A (en
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周劲军
陈广言
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Maanshan Iron and Steel Co Ltd
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Abstract

The invention discloses a ball bladder sampling device and a sampling method. The ball bladder sampling device comprises a flue (2), a sampling gun (1), a sucking pressure pump (3), an air intake and collecting pipe (4), a ball bladder, an air exhaust and collecting pipe (8) and an air sampling hose (9), wherein the sampling gun (1) is arranged at the section of the flue (2), the sucking pressure pump (3) is connected with the sampling gun (1), the air intake and collecting pipe (4) is connected with the sucking pressure pump (3), the ball bladder is connected with the air intake and collecting pipe (4), the air exhaust and collecting pipe (8) is connected with the ball bladder, and the air sampling hose (9) is connected with the air exhaust and collecting pipe (8) and extends outside a wall body (10). The sampling method utilizing the ball bladder sampling device comprises four steps. The sampling method adopts a way of double-ball-bladder sampling, and the ball bladder always keeps the positive pressure status, does not have a phenomenon of inleakage of air and does not need repeated self cleaning. The sampling period (the time needed by completing one-time ball bladder sampling) adopting the double-head ball bladder is saved by 85% compared with the single-head ball bladder sampling method. On the basis of simple operation and low use cost, the sampling method meets the sampling requirements for real time, accuracy and safety.

Description

Bladders sampler and sampling method
Technical field
The present invention relates to steel industry thermal technology, environmental protection tests field, be specifically related to bladders sampler and sampling method.
Background technology
There is the existing century-old history that in the artificial sample method of utilizing the single head bladders to get gas, because it is easy and simple to handle, easy to carry, use cost is cheap, still is widely used in the coal gas in steel industry, combustion product gases and the special gas sampling analysis at present.But the single head bladders is got the gas method and in use had following defective: 1. sample time, (accomplishing a bladders samples the needed time) was longer, because bladders is single air intake opening (gas outlet) setting; For getting rid of the influence of residual gas, must carry out the bladders self-cleaning before gathering, i.e. bladders sampling is full of, emptying; General self-cleaning number of times is more than 4 times; For the high-purity test, wash number is more, causes sample time more than 3min; 2. real-time is relatively poor, because the uncertainty of sample time causes under the fluctuation of operating conditions condition, sampling is representative poor in real time; 3. have potential safety hazard, for, the harmful gas poisonous for coal gas etc., there is the possibility of detonation, poisoning at the scene in the Rapid Cleaning discharge process in bladders, threatens the person and device security; 4. the deaeration influence of bringing at all, because the single head bladders is connecing gas moment, air intake opening and atmosphere cause air to bring into, influence sampling precision, especially as far as high-pure gas.
Summary of the invention
The object of the present invention is to provide bladders sampler and sampling method, on basis easy and simple to handle, that use cost is cheap, accomplish short, real-time, no potential safety hazard sample time, satisfy on-the-spot convenient, real-time, accurate, safe sampling requirement.
To achieve these goals, the technical scheme of the present invention's employing is:
Said bladders sampler adopts the double end bladders to realize getting gas fast, and assurance air inlet and exhaust are accomplished simultaneously in the process of bladders self-cleaning, stop to bring into air.
Said bladders sampler; Comprise flue, be located at the sampling rifle in flue cross section, the force (forcing) pump of bleeding that is connected with the sampling rifle; The inlet manifold that is connected with the force (forcing) pump of bleeding; The bladders that is connected with inlet manifold, the discharge header that is connected with bladders, and be connected with discharge header and reach body of wall gas production flexible pipe outward.
Said bladders is divided into first bladders and second bladders, and said first bladders and second bladders are connected with said inlet manifold with parallel way one side, and opposite side is connected with said discharge header.
Said inlet manifold is connected through the gas production flexible pipe with the force (forcing) pump of bleeding, and is provided with first stop valve being used to connect on the gas production flexible pipe of the two.
Said first bladders and second bladders are connected through the gas production flexible pipe with said inlet manifold, are provided with second stop valve being used to connect on the gas production flexible pipe of the two.
Said discharge header is connected through the gas production flexible pipe with said first bladders and second bladders, is provided with the 3rd stop valve being used to connect on the gas production flexible pipe of the two.
Be provided with the 4th stop valve being connected with discharge header and reaching on the gas production flexible pipe outside the body of wall.
The connection that said second stop valve and the 3rd stop valve are realized said first bladders and second bladders and inlet manifold and discharge header with separate, be used to control the intake and exhaust of said first bladders and second bladders.
Said first stop valve and the 4th stop valve are used to adjust said first bladders and the second bladders admission pressure.
Utilize the sampling method of said bladders sampler, may further comprise the steps:
(1) connects said each parts of bladders sampler by process chart; Open first stop valve, second stop valve, the 3rd stop valve and the 4th stop valve; Start the force (forcing) pump of bleeding, adjust first stop valve and the 4th stop valve aperture, guarantee that first bladders and second bladders are in swelling state; This up-to-date style gas is dispensed to first bladders and second bladders after inlet manifold is mixed, converge, drain into the safety zone outward through discharge header again; After general 3 minutes, the residual gas in the device is excluded, and the gas that flows in the device is consistent with the interior gas of flue, and first bladders and second bladders begin sampling;
(2) second stop valve and the 3rd stop valve of closing control first bladders turnover gas unload first bladders, and seal first bladders with spring caliper, and sampling is for the first time accomplished;
(3) load onto the first subsequent use bladders and open corresponding second stop valve and the 3rd stop valve again; By the sampling period requirement, second stop valve and the 3rd stop valve of closing control second bladders turnover gas unload second bladders, and seal second bladders with spring caliper, and sampling is for the second time accomplished; Again load onto the second subsequent use bladders and open corresponding second stop valve and the 3rd stop valve;
(4) repeating step (2), (3), so back and forth, until satisfying sampling requirement.
As further improvement; Utilize the sampling method of said bladders sampler; In the sampling period is in 10 minutes the time, and said step (1) adopts two above bladders parallel connection arrangements, i.e. a plurality of balloon courages of getting of parallelly connected layout between inlet manifold and discharge header; According to the sampling period requirement, cut off the turnover gas stop valve of the bladders of respectively taking a sample.
As further improvement; Utilize the sampling method of said bladders sampler, when the sampling period surpassed 10 minutes, said step (1) was controlled the force (forcing) pump start and stop of bleeding through the Long-distance Control means; Promptly before sampling, start the force (forcing) pump of bleeding; Accomplish the cleaning and the sampling work of the quick collector of bladders, after bladders sampling completion, subsequent use bladders install, stop the force (forcing) pump of bleeding.So back and forth, until satisfying sampling requirement.
Because air inflow is bigger under many bladders parallel connection arrangements, should the bigger force (forcing) pump of bleeding of selection pressure flow, maximum flow is greater than 15l/min, and maximum output pressure guarantees that greater than 100kpa sampling pressure can satisfy the requirement of bladders sampling.
The invention has the advantages that: the present invention adopts the mode of two bladders samplings, and bladders keeps barotropic state always, and the phenomenon that does not exist air to bleed does not need the repetition self-cleaning, and the sampling period behind the employing double end bladders practices thrift 85% than single head bladders sampling method.Simultaneously, system adopts many bladders parallel connection arrangements, guarantees the real-time of sampling; , harmful gas poisonous in order to prevent threatens potential safety hazards such as the person, equipment, and gas outlet is extended to the safety zone discharging.The present invention accomplishes short, real-time, no potential safety hazard of sampling period, satisfies on-the-spot convenient, real-time, accurate, safe sampling requirement on basis easy and simple to handle, that use cost is cheap.
Description of drawings
Face the content of Figure of description expression of the present invention and the mark among the figure down and make brief description:
Fig. 1 is the structural representation of said bladders sampler;
Being labeled as among the above-mentioned figure:
1, sampling rifle, 2, flue, 3, the force (forcing) pump of bleeding, 4, inlet manifold, 5, second stop valve; 6, first bladders, the 7, the 3rd stop valve, 8, discharge header, 9, the gas production flexible pipe; 10, body of wall, 11, first stop valve, the 12, the 4th stop valve, 13, second bladders.
Embodiment
Contrast accompanying drawing below; Through description to embodiment; The effect and the principle of work of mutual alignment between specific embodiments of the invention such as the related each several part and annexation, each several part, manipulate method etc.; Do further detailed explanation, design of the present invention, technical scheme are had more complete, accurate and deep understanding to help those skilled in the art.
As shown in Figure 1, said bladders sampler comprises flue 2; Be located at the sampling rifle 1 in flue 2 cross sections; With the force (forcing) pump 3 of bleeding that sampling rifle 1 is connected, the inlet manifold 4 that is connected with the force (forcing) pump 3 of bleeding, the bladders that is connected with inlet manifold 4; The discharge header 8 that is connected with bladders, and be connected with discharge header 8 and reach body of wall 10 gas production flexible pipe 9 outward.
Said bladders is divided into first bladders 6 and second bladders 13, and said first bladders 6 and second bladders 13 are connected with said inlet manifold 4 with parallel way one side, and opposite side is connected with said discharge header 8.
Said inlet manifold 4 is connected through gas production flexible pipe 9 with the force (forcing) pump 3 of bleeding, and is provided with first stop valve 11 being used to connect on the gas production flexible pipe 9 of the two.
Said first bladders 6 and second bladders 13 are connected through gas production flexible pipe 9 with said inlet manifold 4, are provided with second stop valve 5 being used to connect on the gas production flexible pipe 9 of the two.
Said discharge header 8 is connected through gas production flexible pipe 9 with said first bladders 6 and second bladders 13, is provided with the 3rd stop valve 7 being used to connect on the gas production flexible pipe 9 of the two.
Be provided with the 4th stop valve 12 on the gas production flexible pipe 9 outside the body of wall being connected with discharge header 8 and reaching.
The connection that said second stop valve 5 and the 3rd stop valve 7 are realized said first bladders 6 and second bladders 13 and inlet manifold 4 and discharge header 8 with separate, be used to control the intake and exhaust of said first bladders 6 and second bladders 13.
Said first stop valve 11 and the 4th stop valve 12 are used to adjust the admission pressure of said first bladders 6 and second bladders 13.
Utilize the sampling method of said bladders sampler, may further comprise the steps:
(1) connects said each parts of bladders sampler by process chart; Open first stop valve 11, second stop valve 5, the 3rd stop valve 7 and the 4th stop valve 12; Start the force (forcing) pump 3 of bleeding; Adjust first stop valve 11 and the 4th stop valve 12 apertures, guarantee that first bladders 6 and second bladders 13 are in swelling state; This up-to-date style gas is dispensed to first bladders 6 and second bladders 13 after inlet manifold 4 is mixed, converge, drain into the safety zone outward through discharge header 8 again; After a period of time, the residual gas in the device is excluded, and the gas that flows in the device is consistent with flue 2 interior gases, and first bladders 6 and second bladders 13 begin sampling;
(2) second stop valve 5 and the 3rd stop valve 7 of closing control first bladders 6 turnover gas unload first bladders 6, and seal first bladders 6 with spring caliper, and sampling is for the first time accomplished;
(3) load onto the first subsequent use bladders 6 and open corresponding second stop valve 5 and the 3rd stop valve 7 again; By the sampling period requirement, second stop valve 5 and the 3rd of closing control second bladders 13 turnover gas cuts off 7 valves, unloads second bladders 13, and seals second bladders 13 with spring caliper, and sampling is for the second time accomplished; Again load onto the second subsequent use bladders 13 and open corresponding second stop valve 5 and the 3rd stop valve 7;
(4) repeating step (2), (3), so back and forth, until satisfying sampling requirement.
Utilize the sampling method of said bladders sampler; In the sampling period is in 10 minutes the time; Said step (1) adopts two above bladders parallel connection arrangements; At a plurality of balloon courages of getting of 8 parallelly connected layouts of inlet manifold 4 and discharge header,, cut off the turnover gas stop valve of the bladders of respectively taking a sample according to the sampling period requirement.
Utilize the sampling method of said bladders sampler, when the sampling period surpassed 10 minutes, said step (1) was controlled force (forcing) pump 3 start and stop of bleeding through the Long-distance Control means; Before sampling, start the force (forcing) pump 3 of bleeding; Accomplish the cleaning and the sampling work of the quick collector of bladders, after bladders sampling completion, subsequent use bladders installed, force (forcing) pump 3 stopped to bleed; So back and forth, until satisfying sampling requirement.
Utilize the sampling method of said bladders sampler to compare with the sampling method of the single bladders sampler of tradition: collection simultaneously contains O 2Be 0.50% gas, correlation circumstance contrasts like following table:
Figure BDA0000045133120000061
Analyze contrast and go up table,, utilize the sampling method of said bladders sampler to practice thrift 85% than conventional single-ended bladders sampling method owing to there is not the step of repetition self-cleaning; Because the problem that does not exist air to infiltrate, the sampling method that utilizes said bladders sampler is than conventional single-ended bladders sampling method, O 2Test result is lower, more near containing O in the gas 2Standard value.
Combine accompanying drawing that the present invention has been carried out exemplary description above; Obviously the concrete realization of the present invention does not receive the restriction of aforesaid way; As long as adopted the improvement of the various unsubstantialities that method of the present invention design and technical scheme carry out; Or design of the present invention and technical scheme are directly applied to other occasion without improving, all within protection scope of the present invention.

Claims (5)

1. bladders sampler; It is characterized in that: comprise flue (2), be located at the sampling rifle (1) in flue (2) cross section, the force (forcing) pump of bleeding (3) that is connected with sampling rifle (1); The inlet manifold (4) that is connected with the force (forcing) pump of bleeding (3); With the bladders that inlet manifold (4) is connected, the discharge header that is connected with bladders (8), and be connected with discharge header (8) and reach body of wall (10) gas production flexible pipe (9) outward; Said bladders is divided into first bladders (6) and second bladders (13), and said first bladders (6) and second bladders (13) are connected with said inlet manifold (4) with parallel way one side, and opposite side is connected with said discharge header (8); Said inlet manifold (4) is connected through gas production flexible pipe (9) with the force (forcing) pump of bleeding (3), is provided with first stop valve (11) being used to connect on the gas production flexible pipe (9) of the two; Said first bladders (6) and second bladders (13) are connected through gas production flexible pipe (9) with said inlet manifold (4), are provided with second stop valve (5) being used to connect on the gas production flexible pipe (9) of the two; Said discharge header (8) is connected through gas production flexible pipe (9) with said first bladders (6) and second bladders (13), is provided with the 3rd stop valve (7) being used to connect on the gas production flexible pipe (9) of the two; Be provided with the 4th stop valve (12) being connected with discharge header (8) and reaching on the gas production flexible pipe (9) outside the body of wall.
2. according to the described bladders sampler of claim 1; It is characterized in that: the connection that said second stop valve (5) and the 3rd stop valve (7) are realized said first bladders (6) and second bladders (13) and inlet manifold (4) and discharge header (8) with separate, be used to control the intake and exhaust of said first bladders (6) and second bladders (13); Said first stop valve (11) and the 4th stop valve (12) are used to adjust the admission pressure of said first bladders (6) and second bladders (13).
3. utilize the sampling method of each said bladders sampler of claim 1 to 2, it is characterized in that: may further comprise the steps;
(1) connects said each parts of bladders sampler by process chart; Open first stop valve, second stop valve, the 3rd stop valve and the 4th stop valve; Start the force (forcing) pump of bleeding, adjust first stop valve and the 4th stop valve aperture, guarantee that first bladders and second bladders are in swelling state; This up-to-date style gas is dispensed to first bladders and second bladders after inlet manifold is mixed, converge, drain into the safety zone outward through discharge header again; After general 3 minutes, the residual gas in the device is excluded, and the gas that flows in the device is consistent with the interior gas of flue, and first bladders and second bladders begin sampling;
(2) second stop valve and the 3rd stop valve of closing control first bladders turnover gas unload first bladders, and seal first bladders with spring caliper, and sampling is for the first time accomplished;
(3) load onto the first subsequent use bladders and open corresponding second stop valve and the 3rd stop valve again; By the sampling period requirement, second stop valve and the 3rd stop valve of closing control second bladders turnover gas unload second bladders, and seal second bladders with spring caliper, and sampling is for the second time accomplished; Again load onto the second subsequent use bladders and open corresponding second stop valve and the 3rd stop valve;
(4) repeating step (2), (3), so back and forth, until satisfying sampling requirement.
4. according to the sampling method of the said bladders sampler of claim 3; It is characterized in that: in the sampling period is in 10 minutes the time; Said step (1) adopts two above bladders parallel connection arrangements; Promptly a plurality of balloon courages of getting of parallelly connected layout between inlet manifold and discharge header according to the sampling period requirement, cut off the turnover gas stop valve of the bladders of respectively taking a sample.
5. according to the sampling method of the said bladders sampler of claim 4; It is characterized in that: when the sampling period surpasses 10 minutes; Said step (1) is controlled the force (forcing) pump start and stop of bleeding through the Long-distance Control means, promptly before sampling, starts the force (forcing) pump of bleeding, and accomplishes the cleaning and the sampling work of the quick collector of bladders; After bladders sampling completion, subsequent use bladders install, stop the force (forcing) pump of bleeding.
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CN102706702B (en) * 2012-06-29 2014-10-15 山东电力集团公司电力科学研究院 Liquid adding and taking device for U-shaped absorption tube of porous glass plate
CN104535377B (en) * 2014-12-04 2017-02-22 苏州国环环境检测有限公司 Gas sampling apparatus
CN105716913A (en) * 2016-04-01 2016-06-29 枣庄矿业(集团)付村煤业有限公司 Device for quickly sampling gas in disaster area
CN105842401A (en) * 2016-05-11 2016-08-10 西安热工研究院有限公司 No-leakage rapid environment-friendly flue gas pretreater
CN106896194A (en) * 2017-04-17 2017-06-27 武汉华星光电技术有限公司 A kind of device and method for monitoring ozone content in coating developing apparatus lamp box
CN108593358A (en) * 2018-05-18 2018-09-28 江苏泰德环保设备有限公司 micro-positive pressure sampler
CN108801716A (en) * 2018-05-23 2018-11-13 上海北裕分析仪器股份有限公司 A kind of gas producing device and method of acquisition parallel gas

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DE19607574A1 (en) * 1996-02-29 1997-09-04 Siemens Ag Exhaust gas analysis system for engines powered by alcohol fuels
DE10128632A1 (en) * 2001-06-13 2003-01-02 Karlsruhe Forschzent Long-term sampling system
CN201145652Y (en) * 2007-12-11 2008-11-05 中国烟草总公司郑州烟草研究院 Cigarette successive suction trapping device

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