CN102102297A - Afterfinishing smoothing agent for synthetic fiber - Google Patents
Afterfinishing smoothing agent for synthetic fiber Download PDFInfo
- Publication number
- CN102102297A CN102102297A CN2009102277272A CN200910227727A CN102102297A CN 102102297 A CN102102297 A CN 102102297A CN 2009102277272 A CN2009102277272 A CN 2009102277272A CN 200910227727 A CN200910227727 A CN 200910227727A CN 102102297 A CN102102297 A CN 102102297A
- Authority
- CN
- China
- Prior art keywords
- synthetic fiber
- parts
- afterfinishing
- smoothing agent
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses an afterfinishing smoothing agent for synthetic fiber, which comprises the following components in parts by weight: 20 to 50 parts of emulsified silicon oil, 5 to 10 parts of hydroxy silicone oil and 40 to 75 parts of deionized water. The emulsified silicon oil and a proper amount of water are mixed uniformly in an emulsifying machine at the temperature of 20 to 40 DEG C to obtain a uniform liquid; after the temperature is decreased and the pH value shows weak acid, the hydroxy silicone oil or a derivative thereof is added according to proportions and mixed uniformly, and reacts for 0.5 to 1.5 hours at a constant temperature to be dissolved completely; and then the product is obtained. When the afterfinishing smoothing agent is used, fibers to be treated, with the usage of 4 to 6 percent (owf, namely on weight of solution) of fibers and the bath ratio of 1 to (10-15), are fully impregnated in an impregnation liquid added with the afterfinishing smoothing agent for 15 to 20 minutes at the temperature of 25 to 30 DEG C, then taken out after impregnation, and centrifuged, dehydrated and dried. The afterfinishing smoothing agent disclosed by the invention can be diluted with water of any amount, is simple to use, and enables the synthetic fiber to be characterized by antistatic property, softness, smoothness, decontamination in washing, and the like.
Description
Technical field
The present invention relates to the preparation method and the impregnation technology of the level and smooth auxiliary agent of arrangement behind a kind of artificial synthetic fiber, the level and smooth auxiliary agent of arrangement behind a kind of artificial synthetic fiber that are specifically related to use in a kind of hair products field.
Background technology
Hair product industry before fibre is finished, mostly will be carried out impregnation process through various auxiliary agents.Through the fiber of auxiliary agent impregnation process, can form one deck auxiliary agent film at fiber surface and give product multiple good performance, thus the quality scale and the added value of raising product.It is the organic silicone finishing agent of key component that middle nineteen nineties has grown up with aminoethyl aminopropyl silicone oil, but shortcoming such as the fibre after the arrangement has static electrification, inhales dust, hand feel performance is single.
Summary of the invention
Purpose of the present invention is exactly to provide a kind of making to have the level and smooth auxiliary agent of arrangement behind the multifunctional modification organic silicon emulsion that antistatic behaviour is strong, light is soft, smooth after the artificial synthetic fiber impregnation process, and the emulsification compounded technology and the impregnation technology of the level and smooth auxiliary agent of arrangement behind this organic silicon emulsion is provided simultaneously.
The level and smooth auxiliary agent of arrangement contains 20～50 weight portion silicone emulsions, 5～10 weight portion hydroxy silicon oils, the deionized water of 40～75 weight portions behind the artificial synthetic fiber provided by the invention.
The mentality of designing of arrangement level and smooth auxiliary agent each component molecular structure and proportioning is behind the artificial synthetic fiber provided by the invention, make have that antistatic behaviour is strong after the synthetic fiber impregnation process, light, soft, smooth performance characteristics.Its mechanism is macromolecular silicone emulsion in the organosilicon main chain, makes fiber surface become uniform elastic membrane, makes it reach perfect finishing effect.
Described silicone emulsion can be one or more of dimethicone of different molecular.
Described hydroxy silicon oil can be one or more of different molecular and viscosity.
The preparation method of a kind of artificial synthetic fiber after-treating auxiliary of the present invention is: at 20 ℃--under 40 ℃ of temperature, silicone emulsion and an amount of water stirring and evenly mixing in mulser, obtain uniform liquid, after cooling adjusting pH value is faintly acid, hydroxy silicon oil or derivatives thereof in proportion again, stir, isothermal reaction dissolved it in 0.5～1.5 hour fully, can obtain product.
Select set of dispense than the oil emulsion that can be mixed with different viscosities or gel-like emulsion or the outward appearance liquid of oily seemingly.
The present invention puts the impregnation technology that level and smooth auxiliary agent is used in order after a kind of above-mentioned artificial synthetic fiber also are provided.This technology mainly comprises immersion---dehydration---dries several steps.Specific as follows:
1, pending fiber is fully immersed in the maceration extract that is added with this finishing auxiliaries, parameter is as follows:
Consumption 4--6% (o.w.f)
Bath raio 1: 10--15
Soaking temperature 25--30 ℃
Soak time 15--20 minute
2, the fiber after will flooding takes out, and centrifugal dehydration, oven dry get final product.
Behind the artificial synthetic fiber provided by the invention the arrangement level and smooth auxiliary agent, can with water arbitrarily than dilution, flood easy to use, particularly artificial fiber is sent out good treatment effect, have after the impregnation process that antistatic behaviour is strong, bright, soft, smooth, characteristics, production equipment is simple, and cost is low.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1
1, the level and smooth adjuvant component prescription of fibre finish (in parts by weight): 45 parts of silicone emulsions, 8 parts of hydroxyl base silicone oil, 47 parts of deionized waters.
2, preparation method:
30 ℃ of temperature, 40 parts deionized waters and 45 parts of silicone emulsions are added in the mulser, open stirring silicone oil is dispersed in the water, add 8 parts of hydroxyls and 7 parts of deionized waters again, constant temperature stirred 1.5 hours, obtained homogeneous transparent liquid, after the adjusting pH value is faintly acid, get product.
3, dipping using method:
Get 1500 milliliters 25 ℃ demineralized water, add the above-mentioned product that makes of 3 grams and stir, make its fully dissolving in water, get maceration extract; Get pending fiber 100 grams, put into maceration extract, soaked 20 minutes; Fiber behind the dipping is pulled out, and oven dry gets final product after the centrifugal dehydration.
Embodiment 2
1, fiber pre-finishing auxiliary agent component prescription (in parts by weight): 30 parts of silicone emulsions, 20 parts of hydroxy silicon oils, 50 parts of deionized waters.
2, preparation method:
When 40 ℃ of temperature, 30 parts deionized waters and 30 parts of silicone emulsions are added in the mulser, opening to stir is dispersed in the water silicone emulsion, add 20 parts of hydroxy silicon oils again, constant temperature stirred 1 hour, obtained uniform transparency liquid, add 20 parts of balance of deionized water again, mix, after the adjusting pH value is faintly acid, get product.
3, dipping using method:
Get 1000 milliliters 30 ℃ demineralized water, add the above-mentioned product that makes of 5 grams and stir, make its fully dissolving in water, get maceration extract; Get pending fiber 100 grams, put into maceration extract, soaked 15 minutes; Fiber behind the dipping is pulled out, and oven dry gets final product after the centrifugal dehydration.
Claims (5)
1. put smooth agent in order behind synthetic fiber, it is characterized in that: (in weight portion) composed of the following components: 20～50 parts silicone emulsion, 5～10 parts big molecule hydroxy silicon oil, 40～75 parts deionized water.
2. put smooth agent in order behind a kind of synthetic fiber according to claim 1, it is characterized in that: described silicone emulsion can be one or more of dimethicone of different molecular.
3. put smooth agent in order behind a kind of synthetic fiber according to claim 1, it is characterized in that: described hydroxy silicon oil can be one or more of different molecular and viscosity.
4. put smooth agent in order behind a kind of synthetic fiber according to claim 1, it is characterized in that the preparation method: at 20 ℃--under 40 ℃ of temperature, silicone emulsion and an amount of water stirring and evenly mixing in mulser, obtain uniform liquid, after cooling was regulated pH value and is faintly acid, hydroxy silicon oil or derivatives thereof in proportion stirred again, isothermal reaction dissolved it in 0.5～1.5 hour fully, can obtain product.
5. according to putting smooth agent in order behind claim 1 and the 4 described a kind of synthetic fiber,---dehydration---dries to it is characterized in that impregnation technology: comprise immersion, promptly pending fiber minute is fully immersed by consumption 4--6% (o.w.f), bath raio 1: 10-15, soaking temperature 25--30 ℃, soak time, 15--20 and be added with in the maceration extract of this finishing auxiliaries, fiber is taken out in the dipping back, dries after the centrifugal dehydration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009102277272A CN102102297A (en) | 2009-12-22 | 2009-12-22 | Afterfinishing smoothing agent for synthetic fiber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009102277272A CN102102297A (en) | 2009-12-22 | 2009-12-22 | Afterfinishing smoothing agent for synthetic fiber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102102297A true CN102102297A (en) | 2011-06-22 |
Family
ID=44155339
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009102277272A Pending CN102102297A (en) | 2009-12-22 | 2009-12-22 | Afterfinishing smoothing agent for synthetic fiber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102102297A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103643394A (en) * | 2013-11-30 | 2014-03-19 | 江苏金泰针织有限责任公司 | Preparation method of knitted collar and sleeve materials |
| CN104878606A (en) * | 2015-05-08 | 2015-09-02 | 苏州锴诚缝制设备有限公司 | Smoothing agent for fabrics and preparation method thereof |
| CN105040449A (en) * | 2015-08-21 | 2015-11-11 | 深圳天鼎精细化工制造有限公司 | Organic silicon fabric smoothing agent and preparation method thereof |
-
2009
- 2009-12-22 CN CN2009102277272A patent/CN102102297A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103643394A (en) * | 2013-11-30 | 2014-03-19 | 江苏金泰针织有限责任公司 | Preparation method of knitted collar and sleeve materials |
| CN104878606A (en) * | 2015-05-08 | 2015-09-02 | 苏州锴诚缝制设备有限公司 | Smoothing agent for fabrics and preparation method thereof |
| CN105040449A (en) * | 2015-08-21 | 2015-11-11 | 深圳天鼎精细化工制造有限公司 | Organic silicon fabric smoothing agent and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109667154A (en) | A kind of organic silicon rigidity-increasing depth finishing agent and its preparation process | |
| CN101994256A (en) | Method for preparing artificial synthetic fiber after finishing auxiliary agent and impregnation process | |
| CN106521986A (en) | Aqueous double-faced suede microfiber PU synthetic leather and production method thereof | |
| JPH0284583A (en) | Treatment of fibrous substance | |
| DE4004946A1 (en) | FINE-PART ORGANOPOLYSILOXANE EMULSIONS | |
| EP0044653A2 (en) | Organo-functional polysiloxane compositions for fiber-treating | |
| CN101619542B (en) | Preparation method of organosilicon emulsion straight fiber finishing additive and dipping process | |
| CN104878621B (en) | Acid dye leveling agent | |
| CN102102297A (en) | Afterfinishing smoothing agent for synthetic fiber | |
| CN101503514B (en) | Synthesizing method of amino / sulfhydryl co-modified organosilicon polysiloxane | |
| US20020161116A1 (en) | Water repellent textile finishes and method of making | |
| CN102605627A (en) | Wig treating agent and using method thereof | |
| JP2007162160A (en) | New fiber processing agent and fiber product using the same | |
| DE10259291B4 (en) | Highly concentrated, self-emulsifying preparations containing organopolysiloxanes and alkylammonium compounds and their use in aqueous systems | |
| CN109234477A (en) | A kind of preparation method of Chrome-free leather | |
| CN111320757B (en) | Preparation method of high-fastness ultralow-yellowing silicone oil for polyester fabric and polyester fabric | |
| CN105601844A (en) | Preparation method and application of novel modified organic silicon softening agent | |
| CN101424041A (en) | Method for preparing isolated hair finishing auxiliaries after frizzy hair and use | |
| CN102417582A (en) | Preparation method of cationic polyurethane organosilicon weaving finishing agent | |
| EP3303453A1 (en) | Polyurethane-organopolysiloxanes | |
| CN105586775B (en) | A kind of high wear-resistance carbon fiber emulsion pasting agent and its preparation and application | |
| DE19722680A1 (en) | Silicone softener for jeans | |
| JP3552229B2 (en) | Synthetic fiber darkener | |
| CN107459653B (en) | A kind of dialkyl capped amido silicon oil and preparation method thereof | |
| CN104278517A (en) | After-finishing smoothing addition agent for artificially synthetic fibers and preparation and impregnation methods of after-finishing smoothing addition agent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110622 |