CN102087264A - Method for testing dispersing capability of black oozes in marine medium-speed engine oil - Google Patents
Method for testing dispersing capability of black oozes in marine medium-speed engine oil Download PDFInfo
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- CN102087264A CN102087264A CN2009102420707A CN200910242070A CN102087264A CN 102087264 A CN102087264 A CN 102087264A CN 2009102420707 A CN2009102420707 A CN 2009102420707A CN 200910242070 A CN200910242070 A CN 200910242070A CN 102087264 A CN102087264 A CN 102087264A
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Abstract
The invention relates to a method for testing dispersing capability of black oozes in marine medium-speed engine oil, comprising the following steps of: preparing the marine medium-speed engine oil and marine heavy fuel oil into a mixed oil liquid according to the weight ratio of the marine medium-speed engine oil to the marine heavy fuel oil being (5-15):1, injecting the mixed oil liquid into an oil tank of a crank case simulation test instrument, placing an aluminum test board above the oil tank of the crank case simulation test instrument, controlling the temperature of the mixed oil liquid within the ranges of 95-155 DEG C, independently controlling the temperature of the test board within the ranges of 295-325 DEG C, starting an oil splashing rod motor of the test instrument, controlling the rotational speed of an oil splashing rod within the ranges of 500-1400rpm, splashing the mixed oil liquid in the oil tank on the test board, keeping the operating time to be 2-48 hours, finishing the test, taking out the test board, cleaning by using a solvent, and comparing the test board with a standard board to obtain a test result. The method is simple and easy to operate, the simulation test result coincides with the practical application result, and a basis is provided for the final confirmation of an oil formula.
Description
Technical field
The present invention relates to a kind of method of testing of oil property, especially for the method for test MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property.
Background technology
Along with updating of engine technology, the installation of anti-buffing ring or the peace and quiet ring of piston, oil consumption reduces, and generally is low to moderate 0.2~0.4g/kWh, and the repairing cycle prolongs greatly.Recycling for a long time in the process of oil product; scurrying into crankcase because of fuel has strengthened the influence that oil product causes; the heavy fuel that uses of ship use intermediate speed engine particularly; has higher asphalt content; in use bituminous matter is difficult to dissolved and disperses; partly form black mud thereby caused the ship use intermediate speed machine to appear at crankcase, tappet etc., produce phenomenons such as greasy filth increases, also will influence the normal operation of engine when serious through regular meeting.Therefore, the oil product that requires to be used for the ship use intermediate speed engine must possess good high-temperature detergent-dispersant performance energy, and particularly the black mud dispersibility that fuel oil medium pitch matter is caused will be got well, and could prolong the drain period effectively.The method that in the process for preparation of oil product, does not also have at present mud dispersive property in the lab investigation oil product, black mud dispersive property in the oil formula adjuvant can only aboard ship carry out, the means that shortage is tested in the laboratory can not be evaluated the composition of adjuvant in the process for preparation and the adjustment of content.
By looking into new discovery, do not see both at home and abroad and adopt the evaluation report of crankcase test method detersive black mud dispersive property.
Summary of the invention
The object of the present invention is to provide a kind of method of testing of MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property, be implemented in the black mud dispersive property of measuring oil product in the laboratory, method is simple, and test result and practical application situation are approaching.
Technical solution of the present invention is: a kind of method of testing of MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property, it is characterized in that MARINE MEDIUM SPEED ENGINE OIL and heavy bunker fuel oil according to 5-15: 1 part by weight is mixed with mixed oil liquid, mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, breadboard places the fuel tank top of crankcase simulation test instrument, the temperature of control mixed oil liquid is in 95~155 ℃ of scopes, the temperature of controlling breadboard simultaneously is in 295~325 ℃ of scopes, the starting characteristics test instrument spatters oily excellent motor, control is spattered oily excellent rotating speed in the 500-1400rpm scope, mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 2~48 hours, off-test, take out breadboard, with drawing test result with the on-gauge plate contrast after the solvent cleaning.
Described test is 3 ± 0.5% with the sulfur content of heavy bunker fuel oil, and density is 950~1000kg/m
3, the composition that needs detergent-dispersant additive to play a role in order to the bituminous matter in the assurance adding oil product, colloid etc. remains in certain scope.
Described MARINE MEDIUM SPEED ENGINE OIL is to mix to stir 30~60min under 60 ± 2 ℃ of temperature conditions with the heavy bunker fuel oil.Its role is to make two components fully to mix, and prevent that oil product and additive component from other chemical reactions taking place.
The crankcase simulation test instrument that uses among the present invention is the DKL-153 type machine that the Kunlun, Dalian oil instrument plant produces.
Characteristics of the present invention are: a kind of method of testing of carrying out MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property in the laboratory is provided, this method is utilized the crankcase simulation test instrument, lacquer spot by forming on breadboard under certain test condition is finished the test evaluation.Method is simple, easily operation, and simulation test conforms to the result of practical application, finally determines to provide foundation for oil formula.
Embodiment
Embodiment 1:
Alkylsalicylate decision black mud dispersive property in the MARINE MEDIUM SPEED ENGINE OIL product additive component, the content difference of alkylsalicylate in the oil product, its black mud dispersive property also can be different.The addition of the alkylsalicylate of the MARINE MEDIUM SPEED ENGINE OIL product of present embodiment is 5% of a total amount, and the sulfur content of heavy bunker fuel oil is 3 ± 0.5%, and density is 950kg/m
3To get MARINE MEDIUM SPEED ENGINE OIL product 200mL and mix with the heavy bunker fuel oil of 40mL and be heated to 60 ℃, the temperature difference is no more than ± and 2 ℃, stir 30min, be mixed with mixed oil liquid.Mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, the metallic aluminium breadboard places the fuel tank top of crankcase simulation test instrument, heating mixed oil liquid to 95 ℃, the temperature of breadboard is controlled to be 295 ℃ separately, the starting characteristics test instrument spatters oily excellent motor, and oily excellent rotating speed 800rpm is spattered in control, and the mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 2 hours, breadboard is taken out in off-test, draws test result with the on-gauge plate contrast, burnt heavy 5.2mg grades 5.0 grades.
Embodiment 2:
The addition of the alkylsalicylate of the MARINE MEDIUM SPEED ENGINE OIL product of present embodiment is 4% of a total amount, and the sulfur content of heavy bunker fuel oil is 3 ± 0.5%, and density is 1000kg/m
3To get MARINE MEDIUM SPEED ENGINE OIL product 300mL and mix with the heavy bunker fuel oil of 20mL and be heated to 60 ℃, the temperature difference is no more than ± and 2 ℃, stirred 60 minutes, be mixed with mixed oil liquid.Mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, the metallic aluminium breadboard places the fuel tank top of crankcase simulation test instrument, heating mixed oil liquid to 155 ℃, the temperature of breadboard is controlled to be 325 ℃ separately, the starting characteristics test instrument spatters oily excellent motor, and oily excellent rotating speed 1400rpm is spattered in control, and the mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 48 hours, breadboard is taken out in off-test, draws test result with the on-gauge plate contrast, burnt heavy 4.6mg grades 4.5 grades.
Embodiment 3:
The addition of the alkylsalicylate of the MARINE MEDIUM SPEED ENGINE OIL product of present embodiment is 6% of a total amount, and the sulfur content of heavy bunker fuel oil is 3 ± 0.5%, and density is 1000kg/m
3To get MARINE MEDIUM SPEED ENGINE OIL product 250mL and mix with the heavy bunker fuel oil of 30mL and be heated to 60 ℃, the temperature difference is no more than ± and 2 ℃, stirred 60 minutes, be mixed with mixed oil liquid.Mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, the metallic aluminium breadboard places the fuel tank top of crankcase simulation test instrument, heating mixed oil liquid to 100 ℃, the temperature of breadboard is controlled to be 320 ℃ separately, the starting characteristics test instrument spatters oily excellent motor, and oily excellent rotating speed 1000rpm is spattered in control, and the mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 6 hours, breadboard is taken out in off-test, draws test result with the on-gauge plate contrast, burnt heavy 3.2mg grades 3.0 grades.
Embodiment 4:
The addition of the alkylsalicylate of the MARINE MEDIUM SPEED ENGINE OIL product of present embodiment is 3% of a total amount, and the sulfur content of heavy bunker fuel oil is 3 ± 0.5%, and density is 1000kg/m
3To get MARINE MEDIUM SPEED ENGINE OIL product 300mL and mix with the heavy bunker fuel oil of 20mL and be heated to 60 ℃, the temperature difference is no more than ± and 2 ℃, stir 60min, be mixed with mixed oil liquid.Mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, the metallic aluminium breadboard places the fuel tank top of crankcase simulation test instrument, heating mixed oil liquid to 120 ℃, the temperature of breadboard is controlled to be 310 ℃ separately, the starting characteristics test instrument spatters oily excellent motor, and oily excellent rotating speed 1200rpm is spattered in control, and the mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 10 hours, breadboard is taken out in off-test, draws test result with the on-gauge plate contrast, burnt heavy 3.9mg grades 4.0 grades.
Embodiment 5:
The addition of the alkylsalicylate of the MARINE MEDIUM SPEED ENGINE OIL product of present embodiment is 5% of a total amount, and the sulfur content of heavy bunker fuel oil is 3 ± 0.5%, and density is 1000kg/m
3To get MARINE MEDIUM SPEED ENGINE OIL product 225mL and mix with the heavy bunker fuel oil of 25mL and be heated to 60 ℃, the temperature difference is no more than ± and 2 ℃, stir 60min, be mixed with mixed oil liquid.Mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, the metallic aluminium breadboard places the fuel tank top of crankcase simulation test instrument, heating mixed oil liquid to 130 ℃, the temperature of breadboard is controlled to be 315 ℃ separately, the starting characteristics test instrument spatters oily excellent motor, and oily excellent rotating speed 1300rpm is spattered in control, and the mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 24 hours, breadboard is taken out in off-test, draws test result with the on-gauge plate contrast, burnt heavy 2.9mg grades 3.5 grades.
Claims (3)
1. the method for testing of a MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property, it is characterized in that: with MARINE MEDIUM SPEED ENGINE OIL and heavy bunker fuel oil according to 5-15: 1 weight ratio ratio is mixed with mixed oil liquid, mixed oil liquid is injected in the fuel tank of crankcase simulation test instrument, the metallic aluminium breadboard places the fuel tank top of crankcase simulation test instrument, the temperature of control mixed oil liquid is in 95~155 ℃ of scopes, the temperature of control breadboard is in 295~325 ℃ of scopes separately, the starting characteristics test instrument spatters oily excellent motor, control is spattered in the oily excellent rotating speed 500-1400rpm scope, mixed oil liquid in the fuel tank is splashed on the breadboard, working time is 2~48 hours, off-test, take out breadboard, with drawing test result with the on-gauge plate contrast after the solvent cleaning.
2. the method for testing of MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property according to claim 1 is characterized in that: the sulfur content of described heavy bunker fuel oil is 3 ± 0.5%, and density is 950~1000kg/m
3
3. the method for testing of MARINE MEDIUM SPEED ENGINE OIL black mud dispersive property according to claim 1 is characterized in that: described MARINE MEDIUM SPEED ENGINE OIL is to mix to stir 30~60min under 60 ± 2 ℃ of temperature conditions with the heavy bunker fuel oil.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104034623A (en) * | 2013-03-06 | 2014-09-10 | 中国石油天然气股份有限公司 | Method and equipment for testing detergency of marine medium-speed engine lubricating oil |
CN104865256A (en) * | 2015-04-01 | 2015-08-26 | 长安大学 | Multi-source information-fused quantitative determination method for detergency and dispersancy of automobile engine oil |
CN105717282A (en) * | 2014-12-05 | 2016-06-29 | 中国石油天然气股份有限公司 | Method for testing soot dispersing performance of engine oil |
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GB1329317A (en) * | 1971-01-07 | 1973-09-05 | List H | Internal combustion engine of the reciprocating piston type for oil testing |
JPH10185906A (en) * | 1996-12-20 | 1998-07-14 | Cosmo Sogo Kenkyusho:Kk | Method and apparatus for testing piston cleaning ability of marine lubricating oil |
CN2529249Y (en) * | 2001-07-19 | 2003-01-01 | 中国石油天然气股份有限公司 | Lubricating oil micro-coking investigating instrument |
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2009
- 2009-12-03 CN CN 200910242070 patent/CN102087264B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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GB1329317A (en) * | 1971-01-07 | 1973-09-05 | List H | Internal combustion engine of the reciprocating piston type for oil testing |
JPH10185906A (en) * | 1996-12-20 | 1998-07-14 | Cosmo Sogo Kenkyusho:Kk | Method and apparatus for testing piston cleaning ability of marine lubricating oil |
CN2529249Y (en) * | 2001-07-19 | 2003-01-01 | 中国石油天然气股份有限公司 | Lubricating oil micro-coking investigating instrument |
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Non-Patent Citations (2)
Title |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104034623A (en) * | 2013-03-06 | 2014-09-10 | 中国石油天然气股份有限公司 | Method and equipment for testing detergency of marine medium-speed engine lubricating oil |
CN105717282A (en) * | 2014-12-05 | 2016-06-29 | 中国石油天然气股份有限公司 | Method for testing soot dispersing performance of engine oil |
CN104865256A (en) * | 2015-04-01 | 2015-08-26 | 长安大学 | Multi-source information-fused quantitative determination method for detergency and dispersancy of automobile engine oil |
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