CN102040336A - 600 DEG C glass glaze powder and preparation method thereof - Google Patents
600 DEG C glass glaze powder and preparation method thereof Download PDFInfo
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- CN102040336A CN102040336A CN 200910070798 CN200910070798A CN102040336A CN 102040336 A CN102040336 A CN 102040336A CN 200910070798 CN200910070798 CN 200910070798 CN 200910070798 A CN200910070798 A CN 200910070798A CN 102040336 A CN102040336 A CN 102040336A
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Abstract
A 600 DEG C glass glaze powder comprises, by weight, the following raw materials: 30-60 parts of pottery clay, 6-10 parts of titanium dioxide, 25-45 parts of lead oxide, and 15-25 parts of boric acid. The preparation method comprises the following steps: (1) putting the raw materials into a ball-mill bottle and ball-mill mixing for 3-4 hours; (2) pressing the mixture; (3) melting the extracted water; (4) drying; (5) ball milling; (6) sieving. The present invention has the advantages of: 1. accessible source of the raw materials and low cost; 2. good chemical stability and humidity-resistance; 3. increased dielectric constant and capacitance by introducing titanium dioxide and leadoxide.
Description
Technical field:
The present invention relates to a kind of preparation method of electrode, particularly a kind of outfit method of 500 ℃ of low-temperature silvers slurry electrode compound.
Background technology:
Glass glaze condenser is the regeneration product of mica capacitor, it has good physics, chemistry and mechanical properties, especially thermotolerance and the stable electrical property that can improve medium by the glass powdered frit of development different ingredients composition are improved the production engineering index, are convenient to produce, are convenient to multilayered structure raising electrical capacity.And as the medium glass powdered frit in the glass glaze condenser to be formulated in China still blank.
Summary of the invention:
Purpose of the present invention just is to provide a kind of 600 ℃ of glass powdered frits and compound method thereof, the dielectric constant height of this glass powdered frit, electrical capacity height, and also its preparing materials price is low.
Technical scheme of the present invention is: a kind of 600 ℃ of glass powdered frits is characterized in that: made according to following weight proportion by following raw materials according: potter's clay 30-60 part, titanium dioxide 6-10 part, plumbous oxide 25-45 part, boric acid 15-25 part.
The optimum weight proportioning of above-mentioned raw materials is 33.6 parts in potter's clay, 8.4 parts of titanium dioxide, 37 parts in plumbous oxide, 21 parts of boric acid.
The compound method of above-mentioned glass powdered frit is finished according to the following step according to following: the ball of 1. above-mentioned raw materials being packed into opens in the bottle, and ball opens and mixed 3-4 hour; 2. press knot: under the pressure of oil press, above-mentioned batch mixing put into to press to form pounce on; 3. found scold water; In High Temperature Furnaces Heating Apparatus, will press the knot powder puff to put into furnace pot and under 1000-1400 ℃ high temperature, be incubated 10-15 minute, treat that powder puff dissolves fully, the blow-on door is poured pyrosol in the enamel basin that is filled with water into, because the bath of glass of the big fusing of the temperature difference forms the disintegrating slag of pulverizing immediately; 4. dry: as to drive away the disintegrating slag water and rinse, put into container, send in the drying baker, oven dry; 5. ball opens: the material slag that will dry is put into ball and is opened bottle, puts into ball again and opens and carry out ball on the machine and open and pulverized 48-60 hour; 6. sieve: above-mentioned material powder is carried out 360 order sub-sieves sieve, promptly obtain the glass powdered frit.
Advantage of the present invention is: 1, material source is easy, cheap.2, chemical stability is good, moisture resistivity is good.3, introducing titanium dioxide and plumbous oxide can improve dielectric constant, improve electrical capacity.
Embodiment:
Embodiment 1: a kind of 600 ℃ of glass powdered frits, take off 33.6 kilograms in row raw material potter's clay, 8.4 kilograms of titanium dioxide, 37 kilograms in plumbous oxide, 21 kilograms of boric acid
The compound method of above-mentioned glass powdered frit is finished according to the following step according to following: the ball of 1. above-mentioned raw materials being packed into opens in the bottle, and ball opens and mixed 3 hours; 2. press knot: under the pressure of oil press, above-mentioned batch mixing put into to press to form pounce on; 3. found scold water; In High Temperature Furnaces Heating Apparatus, will press the knot powder puff to put into furnace pot and under 1000-1400 ℃ high temperature, be incubated 10-15 minute, treat that powder puff dissolves fully, the blow-on door is poured pyrosol in the enamel basin that is filled with water into, because the bath of glass of the big fusing of the temperature difference forms the disintegrating slag of pulverizing immediately; 4. dry: as to drive away the disintegrating slag water and rinse, put into container, send in the drying baker, oven dry; 5. ball opens: the material slag that will dry is put into ball and is opened bottle, puts into ball again and opens and carry out ball on the machine and open and pulverized 48 hours; 6. sieve: above-mentioned material powder is carried out 360 order sub-sieves sieve, promptly obtain the glass powdered frit.
Claims (3)
1. a glass powdered frit is characterized in that: made according to following weight proportion by following raw materials according: potter's clay 30-60 part, titanium dioxide 6-10 part, plumbous oxide 25-45 part, boric acid 15-25 part.
2. 600 ℃ of glass powdered frits according to claim 1 is characterized in that: the optimum weight proportioning of above-mentioned raw materials is 33.6 parts in potter's clay, 8.4 parts of titanium dioxide, 37 parts in plumbous oxide, 21 parts of boric acid.
3. the compound method of 600 ℃ of glass powdered frits according to claim 1, it is characterized in that: finish according to the following step according to following: the ball of 1. above-mentioned raw materials being packed into opens in the bottle, and ball opens and mixed 3-4 hour; 2. press knot: under the pressure of oil press, above-mentioned batch mixing put into to press to form pounce on; 3. found scold water; In High Temperature Furnaces Heating Apparatus, will press the knot powder puff to put into furnace pot and under 1000-1400 ℃ high temperature, be incubated 10-15 minute, treat that powder puff dissolves fully, the blow-on door is poured pyrosol in the enamel basin that is filled with water into, because the bath of glass of the big fusing of the temperature difference forms the disintegrating slag of pulverizing immediately; 4. dry: as to drive away the disintegrating slag water and rinse, put into container, send in the drying baker, oven dry; 5. ball opens: the material slag that will dry is put into ball and is opened bottle, puts into ball again and opens and carry out ball on the machine and open and pulverized 48-60 hour; 6. sieve: above-mentioned material powder is carried out 360 order sub-sieves sieve, promptly obtain the glass powdered frit.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN 200910070798 CN102040336A (en) | 2009-10-14 | 2009-10-14 | 600 DEG C glass glaze powder and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN 200910070798 CN102040336A (en) | 2009-10-14 | 2009-10-14 | 600 DEG C glass glaze powder and preparation method thereof |
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CN102040336A true CN102040336A (en) | 2011-05-04 |
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Family Applications (1)
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CN 200910070798 Pending CN102040336A (en) | 2009-10-14 | 2009-10-14 | 600 DEG C glass glaze powder and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2489410C1 (en) * | 2012-04-06 | 2013-08-10 | Юлия Алексеевна Щепочкина | Brick glaze |
-
2009
- 2009-10-14 CN CN 200910070798 patent/CN102040336A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2489410C1 (en) * | 2012-04-06 | 2013-08-10 | Юлия Алексеевна Щепочкина | Brick glaze |
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C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110504 |