CN102038124A - Preparation method of non-antibiotic residual-removal honey - Google Patents
Preparation method of non-antibiotic residual-removal honey Download PDFInfo
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- CN102038124A CN102038124A CN2009100359668A CN200910035966A CN102038124A CN 102038124 A CN102038124 A CN 102038124A CN 2009100359668 A CN2009100359668 A CN 2009100359668A CN 200910035966 A CN200910035966 A CN 200910035966A CN 102038124 A CN102038124 A CN 102038124A
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Abstract
The invention discloses a preparation method of non-antibiotic residual-removal honey, which is characterized in that raw material honey conforming to the specification standard is prepared into non-antibiotic residual-removal honey by the nanofiltration and ion adsorption technology. The method comprises the following steps: (1) sorting; (2) dissolving; (3) adsorbing; (4) carrying out ion ultra; (5) carrying out vacuum concentration; (6) cooling instantaneously; and (7) inspecting and packaging to obtain the non-antibiotic residual-removal honey. In the honey processing process, ultrafilteration and ion adsorption equipment is adopted to remove residues (pesticide residues) and antibiotics from honey, so that the honey reaches the international importing requirements. According to the invention, the technical advantages of being initiatively developed in China and keeping world-leading standard on the aspect of non antibiotic and residual removal are maintained so as to be level with the international standard, so that the technical level of the honey product processing industry in China is improved, thus further enlarging production scale, and building our country into a manufacture powerful nation on the aspect of honey product import.
Description
Technical field
The present invention relates to a kind of method of food, particularly a kind of nonreactive is taken off residual honey preparation method
Background technology
Honey is one of traditional agricultural product of China, annual production reaches 250,000 tons, because the agricultural production of China is in the state that falls behind, the agricultural product excess is used the agricultural chemicals of high residue, make the crops persticide residue strengthen, and the further enrichment of process that makes honey out of flowers by honeybee; Overflow with reasons such as antibiotic in the bee rearing epidemic prevention or the process of curing the disease, residual and antibiotic exceeds standard and is abroad returned goods repeatedly or claim damages thereby the honey quality that causes China is because of farming, more seriously forbids the honey outlet of China.China's bee product processing industry production technology is comparatively backward, and most enterprises can't overcome the antibiotic of product and the residues of pesticides problem that exceeds standard.Though we attempted and obtained some achievements removing on the new technology that homemade honey antibiotic and residues of pesticides exceed standard, scope of the enterprise is little, and output is lower, and is not high to the contribution rate of industry.
Therefore, have only further research new technology, adopt new equipment, honey could be gone anti-take off residual achievement further consolidation and raising, strive for keeping and bring into play anti-residual domestic initiation, the technical advantage leading in the world of taking off, integrate with world level, how to improve technological level and equipment, can be more, more high-quality enters the international market.Analyze residual and antibiotic character of honey middle peasant and content, research improves the technical merit of China's bee product processing industry in the effect of going at present to resist, and could further expand the scale of production, and makes the manufacturing of China's honey product outlet and makes the country prosperous.
Summary of the invention:
The present invention announces that a kind of nonreactive takes off the preparation method of residual honey, has adopted ultrafiltration and ionic adsorption equipment that honey is taken off residual (farming is residual) in honey process in the past and has gone to resist (antibiotic) thereby the requirement that reaches international import.Strive for keeping and bring into play anti-residual domestic initiation, the technical advantage leading in the world of taking off, integrate with, improve the technical merit of China's bee product processing industry, could further expand the scale of production, make the manufacturing power of China's honey product outlet with world level.
Of the present invention be achieved through the following technical solutions:
A kind of nonreactive is taken off residual honey preparation method, and the raw material honey that it is characterized in that standard up to specification is configured to nonreactive through nanofiltration and ionic adsorption technical finesse and takes off residual honey, and method is as follows:
(1) select materials: selecting amylase＞8 ° pH value for use is the honey raw material of 3.5-4.5.
(2) dissolving: the honey after will just considering is separated in water-soluble according to 1: 2 ratio.
(3) absorption: honey adding atlapulgite protein adsorbent 8-10% that will be water-soluble, filter through 55 ℃ sheet frame forcing press again.
(4) ionic adsorption, ultrafiltration: the honey macromolecule negative and positive exchanger 5-10% that filters through excess temperature is to former honey absorption 1 hour, nanofiltration in entering the ultrafiltration pipe with ion exchange column under 45 ℃ of-50 ℃ of column environment in temperature.
(5) vacuum concentrates: adopt quadruple effect continuous evaporation system equipment, negative pressure 〉=-the 0.09Mpa temperature is 40 °-50 ° concentration of raw material being carried out 3-5 minute.
(6) instantaneous cooling: the honey after will concentrating is sent in the pipeline plate type heat exchanger instantaneous cooling 1-3 minute by pipeline.
(7) check, packing: to the honey sampling, moisture is controlled in the 17.5%-18%, has both got nonreactive and has taken off residual honey, is carrying out bottled or barreled according to the product specification size.
(1) select materials in diastatic operative temperature be 45 ℃-50 ℃.
(4) ionic adsorption, the model of the ion exchange column in the ultrafiltration are Φ 1.2m*5.85m (sun), Φ 1.2m*5.85m (the moon).
Research institution of the present invention cooperated with relevant scientific research institutions in the beginning in 2006, had carried out the research that nonreactive is taken off residual honey production process.This process program is to adopt nanofiltration and Ritz adsorption technology, antibiotic and residues of pesticides in filtration and the absorption honey.Nanofiltration is between the ultrafiltration and counter-infiltration of membrane separation technique, the NF membrane aperture is a nanoscale, molecular cut off is hundred grades, and the relative molecular weight of glucose and fructose has realized that 180～220 the antibiotic in the homemade honey and residues of pesticides are carried out nanoscale to be held back in the pure honey.Honey process chromatographic isolation after the nanofiltration, Ritz adsorbing separation, last simmer down to finished product.
The specific embodiment:
A kind of nonreactive is taken off residual honey preparation method, is 70% with 1 ton former honey purity
(1) select materials: selecting amylase＞8 ° pH value for use is 3.5 honey raw material.Diastatic operative temperature is 45 ℃-50 ℃.
(2) dissolving: the honey after will just considering is separated in water-soluble according to 1: 2 ratio.
(3) absorption: honey adding atlapulgite protein adsorbent 8% that will be water-soluble, filter through 55 ℃ sheet frame forcing press again.
(4) ionic adsorption, ultrafiltration: the honey macromolecule negative and positive exchanger 5% usefulness ion exchange column that filters through excess temperature is to former honey absorption 1 hour, nanofiltration in entering the ultrafiltration pipe under 45 ℃ of-50 ℃ of column environment in temperature.
(5) vacuum concentrates: adopt quadruple effect continuous evaporation system equipment, negative pressure 〉=-the 0.09Mpa temperature is 40 °-50 ° concentration of raw material being carried out 3-5 minute.
(6) instantaneous cooling: the honey after will concentrating is sent in the pipeline plate type heat exchanger instantaneous cooling 1-3 minute by pipeline.
(7) check, packing: to the honey sampling, moisture is controlled in the 17.5%-18%, both gets nonreactive and takes off residual honey, gets 800 kilograms and is carrying out bottled or barreled according to the product specification size.
Claims (3)
1. a nonreactive is taken off residual honey preparation method, and the raw material honey that it is characterized in that standard up to specification is configured to nonreactive through nanofiltration and ionic adsorption technical finesse and takes off residual honey, and method is as follows:
(1) select materials: selecting amylase＞8 ° pH value for use is the honey raw material of 3.5-4.5.
(2) dissolving: the honey after will just considering is separated in water-soluble according to 1: 2 ratio.
(3) absorption: honey adding atlapulgite protein adsorbent 8-10% that will be water-soluble, filter through 55 ℃ sheet frame forcing press again.
(4) ionic adsorption, ultrafiltration: the honey macromolecule negative and positive exchanger 5-10% that filters through excess temperature is to former honey absorption 1 hour, nanofiltration in entering the ultrafiltration pipe with ion exchange column under 45 ℃ of-50 ℃ of column environment in temperature.
(5) vacuum concentrates: adopt quadruple effect continuous evaporation system equipment, negative pressure 〉=-the 0.09Mpa temperature is 40 °-50 ° concentration of raw material being carried out 3-5 minute.
(6) instantaneous cooling: the honey after will concentrating is sent in the pipeline plate type heat exchanger instantaneous cooling 1-3 minute by pipeline.
(7) check, packing: to the honey sampling, moisture is controlled in the 17.5%-18%, has both got nonreactive and has taken off residual honey, is carrying out bottled or barreled according to the product specification size.
2. nonreactive according to claim 1 is taken off residual honey preparation method, it is characterized in that diastatic operative temperature is 45 ℃-50 ℃ in (1).
3. nonreactive according to claim 1 is taken off residual honey preparation method, and the model that it is characterized in that the ion exchange column in (4) is Φ 1.2m*5.85m (sun), Φ 1.2m*5.85m (the moon).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100359668A CN102038124A (en) | 2009-10-15 | 2009-10-15 | Preparation method of non-antibiotic residual-removal honey |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100359668A CN102038124A (en) | 2009-10-15 | 2009-10-15 | Preparation method of non-antibiotic residual-removal honey |
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| Publication Number | Publication Date |
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| CN102038124A true CN102038124A (en) | 2011-05-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2009100359668A Pending CN102038124A (en) | 2009-10-15 | 2009-10-15 | Preparation method of non-antibiotic residual-removal honey |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107125679A (en) * | 2017-03-31 | 2017-09-05 | 西北大学 | Nitro glyoxaline and quinolones medicament relict removal methods in a kind of honey |
-
2009
- 2009-10-15 CN CN2009100359668A patent/CN102038124A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107125679A (en) * | 2017-03-31 | 2017-09-05 | 西北大学 | Nitro glyoxaline and quinolones medicament relict removal methods in a kind of honey |
| CN107125679B (en) * | 2017-03-31 | 2020-03-27 | 西北大学 | Method for removing nitroimidazole and quinolone drug residues in honey |
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Application publication date: 20110504 |