CN102036432B - Electric heating membrane and production method thereof - Google Patents
Electric heating membrane and production method thereof Download PDFInfo
- Publication number
- CN102036432B CN102036432B CN 201010505422 CN201010505422A CN102036432B CN 102036432 B CN102036432 B CN 102036432B CN 201010505422 CN201010505422 CN 201010505422 CN 201010505422 A CN201010505422 A CN 201010505422A CN 102036432 B CN102036432 B CN 102036432B
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- CN
- China
- Prior art keywords
- heating film
- radiant heating
- electric radiant
- percent
- electric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 238000005485 electric heating Methods 0.000 title abstract 2
- 239000012528 membrane Substances 0.000 title abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 15
- JHXKRIRFYBPWGE-UHFFFAOYSA-K bismuth chloride Chemical compound Cl[Bi](Cl)Cl JHXKRIRFYBPWGE-UHFFFAOYSA-K 0.000 claims abstract description 8
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims description 37
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 claims description 12
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 7
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 7
- 235000014121 butter Nutrition 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 6
- 229910001923 silver oxide Inorganic materials 0.000 claims description 6
- 239000002002 slurry Substances 0.000 claims description 6
- 239000000470 constituent Substances 0.000 claims description 3
- 230000004927 fusion Effects 0.000 claims description 3
- 239000011521 glass Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 230000032683 aging Effects 0.000 abstract description 3
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 229910021627 Tin(IV) chloride Inorganic materials 0.000 abstract 1
- LLSDKQJKOVVTOJ-UHFFFAOYSA-L calcium chloride dihydrate Chemical compound O.O.[Cl-].[Cl-].[Ca+2] LLSDKQJKOVVTOJ-UHFFFAOYSA-L 0.000 abstract 1
- 229940052299 calcium chloride dihydrate Drugs 0.000 abstract 1
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 230000002950 deficient Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
Landscapes
- Surface Heating Bodies (AREA)
- Resistance Heating (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses an electric heating membrane comprising the following components in percent by weight: 20-40 percent of stannic chloride, 25-35 percent of titanium tetrachloride, 0.2-0.3 percent of calcium chloride dihydrate, 0.1-0.3 percent of bismuth trichloride, 20-40 percent of alcohol and 5-7 percent of water. The invention has the advantages of high heat efficiency, stronger physical and chemical properties, suitability for various environments, no oxidation or ageing phenomena after being heated, convenience for production, high yield, capability of being made into various forms according to the requirement of carrier shapes and convenience for application.
Description
Technical field
The present invention relates to the semiconductor heating technology, specifically a kind of Electric radiant Heating Film and this Electric radiant Heating Film manufacture method.
Background technology
Electric radiant Heating Film is a kind of novel heater element, compares with heat forms such as the resistance wire of commonly using, infrared rays, has the advantages such as heating efficiency is high, electrothermal calefactive rate fast, it is aging to be difficult for, the life-span is long.But still there are the shortcomings such as unstable, that the production yields is not high in existing Electric radiant Heating Film due to the defective on composition and manufacture method, is difficult to extensive use.
Summary of the invention
One of technical problem to be solved by this invention is to provide a kind of steady quality, make qualification rate high, be suitable for all-environment Electric radiant Heating Film.
For solving the problems of the technologies described above, the present invention realizes by the following technical solutions:
By weight, this Electric radiant Heating Film composition is: butter of tin: 20%～40%, and titanium tetrachloride: 25%～35%, U-Ramin MC: 0.2%～0.3%, bismuth trichloride: 0.1%～0.3%, ethanol: 20%～40%, water: 5%～7%.
In addition, the present invention also provides a kind of Electric radiant Heating Film manufacture method, with overcome in prior art Electric radiant Heating Film make in the not high defective of yields.The method comprises the steps:
1). get appropriate butter of tin, titanium tetrachloride, U-Ramin MC, bismuth trichloride, ethanol, water and put into Hybrid Heating machine Hybrid Heating, heating-up temperature is 65～75 degrees centigrade, stirs, and solid constituent is dissolved fully, is cooled to normal temperature;
2). the mixed liquor after dissolving filters to get treatment fluid;
3). treatment fluid is sprayed into the Electric radiant Heating Film carrier surface by the negative pressure spray gun forms electric membranous layer in heating furnace, furnace temp is 650～750 degrees centigrade;
4). coat the silver oxide slurry at electric membranous layer two end surfaces, put into the baking of electrode finishing stove, silver oxide slurry and electric membranous layer fusion are integrated, baking temperature is 400～500 degrees centigrade, forms the Electric radiant Heating Film finished product.
Wherein, described Electric radiant Heating Film carrier is glass or pottery or mica or carborundum.
Compared with prior art, the present invention has following advantage:
Heating efficiency is high, has stronger physical and chemical performance, be suitable for using in various environment, and non-oxidation and aging phenomenon after heating, easy to make, yields is high, and can be made into various forms according to the support shapes needs, uses very convenient.
Embodiment
For the ease of those skilled in the art's understanding, the present invention is further described in detail below in conjunction with specific embodiment:
The Electric radiant Heating Film that the present embodiment provides by weight, its composition is:
Butter of tin: 33%, titanium tetrachloride: 30%, U-Ramin MC: 0.3%, bismuth trichloride: 0.2%, ethanol: 30%, water: 6.5%.
According to said ratio, during making: at first butter of tin, titanium tetrachloride, U-Ramin MC, bismuth trichloride, ethanol, water are put into Hybrid Heating machine Hybrid Heating, heating and temperature control stirs between 65～75 degrees centigrade, solid constituent is dissolved fully, be cooled to normal temperature; Then the mixed liquor after dissolving filters to get treatment fluid; Again treatment fluid is sprayed into the Electric radiant Heating Film carrier surface by the negative pressure spray gun in heating furnace and forms electric membranous layer, furnace temp is controlled between 650～750 degrees centigrade; Coat the silver oxide slurry at electric membranous layer two end surfaces at last, put into the baking of electrode finishing stove, silver oxide slurry and electric membranous layer fusion are integrated, baking temperature is controlled between 400～500 degrees centigrade, forms thus the Electric radiant Heating Film finished product.
Wherein, described Electric radiant Heating Film carrier is glass or pottery or mica or carborundum.
In addition, the concrete component of described Electric radiant Heating Film also can be other numerals, can be 20%～40% as butter of tin between arbitrary value, as 20% or 30% or 40% etc.; Arbitrary value between titanium tetrachloride can be 25%～35% is as 25% or 35% etc.; Arbitrary value between U-Ramin MC can be 0.2%～0.3% is as 0.2% or 0.15% etc.; Arbitrary value between bismuth trichloride can be 0.1%～0.3% is as 0.1% or 0.3% etc.; Arbitrary value between ethanol can be 20%～40% is as 20% or 40% etc.; Arbitrary value between water can be 5%～7%, as 5% or 6% or 7% etc., its effect is all suitable with above-mentioned concrete scheme, does not give unnecessary details one by one at this.
More than be the better implementation of the present invention; in addition; the present invention that coexists conceives other implementation of lower existence; need to prove; the preferred version that above-described embodiment is only realized for the present invention; and indefiniteness is exhaustive, and without departing from the inventive concept of the premise, any apparent replacement is all within protection range of the present invention.
Claims (3)
1. an Electric radiant Heating Film, is characterized in that, by weight its component is:
Butter of tin: 20%～33%, titanium tetrachloride: 25%～35%, U-Ramin MC: 0.2%～0.3%, bismuth trichloride: 0.1% or 0.3%, ethanol: 20%～40%, water: 5%～7%.
2. Electric radiant Heating Film manufacture method according to claim 1, is characterized in that, the method is:
1). get appropriate butter of tin, titanium tetrachloride, U-Ramin MC, bismuth trichloride, ethanol, water and put into Hybrid Heating machine Hybrid Heating, heating-up temperature is 65～75 degrees centigrade, stirs, and solid constituent is dissolved fully, is cooled to normal temperature;
2). the mixed liquor after dissolving filters to get treatment fluid;
3). treatment fluid is sprayed into the Electric radiant Heating Film carrier surface by the negative pressure spray gun forms electric membranous layer in heating furnace, furnace temp is 650～750 degrees centigrade;
4). coat the silver oxide slurry at electric membranous layer two end surfaces, put into the baking of electrode finishing stove, silver oxide slurry and electric membranous layer fusion are integrated, baking temperature is 400～500 degrees centigrade, forms the Electric radiant Heating Film finished product.
3. Electric radiant Heating Film manufacture method according to claim 2, is characterized in that, described Electric radiant Heating Film carrier is glass or pottery or mica or carborundum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010505422 CN102036432B (en) | 2010-10-11 | 2010-10-11 | Electric heating membrane and production method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010505422 CN102036432B (en) | 2010-10-11 | 2010-10-11 | Electric heating membrane and production method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102036432A CN102036432A (en) | 2011-04-27 |
| CN102036432B true CN102036432B (en) | 2013-06-19 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 201010505422 Expired - Fee Related CN102036432B (en) | 2010-10-11 | 2010-10-11 | Electric heating membrane and production method thereof |
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| Country | Link |
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| CN (1) | CN102036432B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102843793B (en) * | 2011-06-24 | 2015-05-20 | 北京万众光通科技发展有限公司 | Electrothermal conversion body coating formula and application method |
| CN103391650A (en) * | 2013-07-31 | 2013-11-13 | 浙江哈尔斯真空器皿股份有限公司 | Electrothermal film and manufacturing method thereof |
| CN105732030A (en) * | 2016-02-02 | 2016-07-06 | 季红军 | Preparation method of electrothermal film composite material |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1074579A (en) * | 1992-12-11 | 1993-07-21 | 戴金利 | A kind of semiconductor electric-heating thin film and processing method thereof |
| CN1529534A (en) * | 2003-10-17 | 2004-09-15 | 杨金林 | Electric-heating film and manufacturing method thereof |
| EP1681905A1 (en) * | 2005-01-17 | 2006-07-19 | Cheng-Ping Lin | Method of fabricating semiconductor electric heating film |
| CN101668359A (en) * | 2009-08-11 | 2010-03-10 | 罗日良 | Electrothermal film and manufacturing method thereof |
-
2010
- 2010-10-11 CN CN 201010505422 patent/CN102036432B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1074579A (en) * | 1992-12-11 | 1993-07-21 | 戴金利 | A kind of semiconductor electric-heating thin film and processing method thereof |
| CN1529534A (en) * | 2003-10-17 | 2004-09-15 | 杨金林 | Electric-heating film and manufacturing method thereof |
| EP1681905A1 (en) * | 2005-01-17 | 2006-07-19 | Cheng-Ping Lin | Method of fabricating semiconductor electric heating film |
| CN101668359A (en) * | 2009-08-11 | 2010-03-10 | 罗日良 | Electrothermal film and manufacturing method thereof |
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| Publication number | Publication date |
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| CN102036432A (en) | 2011-04-27 |
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| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20110427 Assignee: HUIZHOU CITY GEPUS TECHNOLOGY Co.,Ltd. Assignor: Li Ruiyong Contract record no.: 2014440000097 Denomination of invention: Electric heating membrane and production method thereof Granted publication date: 20130619 License type: Exclusive License Record date: 20140311 |
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| LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230713 Address after: 516000, 2nd Floor, Building B, Front Row, Huahui Industrial Park, Empress Village, Zhenlong Town, Huiyang District, Huizhou City, Guangdong Province Patentee after: Guangdong Gepusi Technology Co.,Ltd. Address before: No. 1, Huahui Industrial Park, Huitai Road, Huitai Industrial Zone, Huizhou City, Guangdong Province 516001 Patentee before: Li Ruiyong |
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Granted publication date: 20130619 |