CN101975725B - Silver paste viscosity detection constant-temperature pretreatment water tank - Google Patents

Silver paste viscosity detection constant-temperature pretreatment water tank Download PDF

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Publication number
CN101975725B
CN101975725B CN 201010283674 CN201010283674A CN101975725B CN 101975725 B CN101975725 B CN 101975725B CN 201010283674 CN201010283674 CN 201010283674 CN 201010283674 A CN201010283674 A CN 201010283674A CN 101975725 B CN101975725 B CN 101975725B
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water tank
temperature water
constant
constant temperature
silver
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CN101975725A (en
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刘志刚
陈鑫
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Changzhou EGing Photovoltaic Technology Co Ltd
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Changzhou EGing Photovoltaic Technology Co Ltd
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Abstract

The invention relates to a silver paste viscosity detection constant-temperature pretreatment water tank which comprises a constant-temperature water tank, a circulating pump, a refrigerator, a water outlet pipe, a water return pipe, a silver paste cup, a rotating shaft, a tray and a partition top plate, wherein the circulating pump is arranged at the bottom of the constant-temperature water tank, the refrigerator is arranged at the lower end of the constant-temperature water tank, the tray is arranged on the inner wall of the constant-temperature water tank, the rotating shaft is sleeved in a rotating shaft hole of the tray, the partition top plate can rotate relative to the constant-temperature water tank, a partition hole is arranged on the partition top plate, and the silver paste cup is arranged in the partition hole. Because a structure for storing a plurality of silver paste cups is additionally arranged on the constant-temperature water tank, the constant-temperature water tank can provide constant-temperature cooled water for a slot type checkout table, and can be used for cooling the plurality of silver paste cups to be detected in advance simultaneously, thereby ensuring the accuracy of measuring the viscosity of the silver paste so that the silver paste to be detected can be directly detected, and being capable of continuously detecting a plurality of silver paste samples so as to improve the detection efficiency.

Description

The silver paste viscosity detection constant-temperature pretreatment water tank
Technical field
The present invention relates to silver-colored slurry viscosity pick-up unit for a kind of cell piece, relate in particular to silver-colored slurry viscosity Thermostatic detection device, more specifically say the constant temperature water tank in silver-colored slurry viscosity Thermostatic detection device.
Background technology
A kind of thick mixture slurry that silver slurry is comprised of particulate, bonding agent, solvent, the auxiliary agent of highly purified (99.9%) argent.It is very strict that conductive silver paste requires its component.The particulate of argent is the Main Ingredients and Appearance of conductive silver paste, and the conductive characteristic of solar cell is mainly to embody by it.The content of argent in slurry is directly relevant with electric conductivity, and the content of silver is high, to the electric conductivity that improves it, is useful, but, when its content surpasses critical volume concentration, its electric conductivity can not improve.General silver content is in 80~90%(weight ratio) time, oneself reaches mxm. electric conduction quantity, when content continues to increase, electrically no longer improves, and resistance value is in rising trend; When content, lower than 60% the time, the variation of resistance is unstable.In concrete application, in the silver slurry, silver-colored fraction of particle should be considered stable resistance, restricted by the factors such as curing characteristics, bonding strength, economy, as too high as silver-colored fraction of particle, be bonded the probability that resin wraps low, after film-forming, the bonding force of silver conductor descends, the danger that has silver granuel to come off.So the content of the silver in the silver slurry is generally suitable at 60-70%.
The viscosity of silver paste of solar cells has directly affected light-receiving area and the cell photoelectric conversion efficiency of solar cell surface, and it is a very crucial technology of making in solar cell.If silver-colored slurry viscosity is on the low side, although the good fluidity of slurry, after printing, grid line caves in greatly at silicon chip surface, has increased the shading-area of solar cell surface, reduce the light-receiving area of solar cell surface, reduced the photoelectric transformation efficiency of solar cell in unit area; On the contrary, if viscosity is higher, although the silver slurry prints rear grid line, be not easy to cave in, highly viscous slurry is difficult for printing, easily lumps, and electrical property is unstable.Therefore, in the preparation process of silver slurry, must be tested the viscosity of slurry, at present, test silver-colored slurry viscosity and usually use rotational viscosimeter.Experimental results show that: temperature deviation is very large to the viscosity influence of battery silver paste, and temperature raises, and viscosity descends.When 0.5 ℃ of temperature deviation, its viscosity number deviation surpasses 5%, therefore, when measuring battery silver paste viscosity, must in constant temperature enclosure, carry out, also silver slurry to be checked must be placed in constant temperature enclosure and deposit enough time before detection, the temperature that silver is starched reaches the indoor temperature of constant temperature enclosure, so just can guarantee the accuracy of viscosity measurement.This method of testing test condition requires harsh, and efficiency is low, and the frequency of sampling observation is subject to the restriction of detection method, and this detection method directly has influence on the production of silver slurry.
In order to overcome silver-colored slurry viscosity testing process above shortcomings, the applicant develops a kind of silver-colored slurry viscosity Thermostatic detection device, its structure as shown in Figure 1, it comprises constant temperature water tank 1, ebullator 2, refrigeration machine 3, rising pipe 4, return pipe 5 and silver slurry cup 6, ebullator 2 is arranged in constant temperature water tank 1, rising pipe 4 one ends are connected with the water delivering orifice of ebullator 2, the other end and slot type check-out console 11 interlink, return pipe 5 one ends and slot type check-out console ll interlink, the other end leads to constant temperature water tank l, silver slurry cup 6 is placed on slot type check-out console 11, slot type check-out console 11 is positioned at the below of viscosimeter 12.
Because the silver slurry cup that the silver slurry will be housed is placed on slot type check-out console 11, and slot type check-out console l is constantly injected from constant temperature water tank l extraction thermostatted water by ebullator 2, the silver slurry is first carried out the equality of temperature processing by the thermostatted water in slot type check-out console 11, and then carry out viscosity measurement, can guarantee like this accuracy that silver-colored slurry viscosity is measured, can shorten again the constant temperature processing time of silver slurry to be checked, improved detection efficiency, but sample of every detection still needs silver slurry to be checked is carried out to the constant temperature processing, and each sample stationary temperature is processed needs 8~10 minutes.Although more much better than original technology, can't realize the serialization of a plurality of samples to be checked is detected.
Summary of the invention
In order further to optimize the silver-colored slurry viscosity Thermostatic detection device of applicant's development, utilize constant temperature water tank wherein first the silver slurry to be carried out to the constant temperature processing, in silver-colored slurry viscosity testing process, silver through constant temperature processing slurry directly can be carried out to viscosity measurements, the purpose of this invention is to provide a kind of silver-colored paste viscosity detection constant-temperature pretreatment water tank.
The technical scheme that the present invention takes is as follows:
Described silver-colored paste viscosity detection constant-temperature pretreatment water tank, comprise constant temperature water tank, ebullator, refrigeration machine, rising pipe, return pipe and silver slurry cup, the liquid sucting port of ebullator communicates with the constant temperature water tank intracavity bottom, the liquid outlet of ebullator interlinks by rising pipe and slot type check-out console, the inner chamber of return pipe and constant temperature water tank interlinks, refrigeration machine is arranged on the lower end of constant temperature water tank, it is characterized in that: further comprising rotating shaft, pallet and separation top board, pallet is arranged on the inwall of constant temperature water tank, be provided with permeable hole on pallet, heart position is provided with shaft hole therein, pallet is corresponding with the height of silver slurry cup to the distance of constant temperature water tank end face, shaft set is in the shaft hole of pallet, the lower end of rotating shaft is placed in the seat hole of constant temperature water tank bottom, the upper end of rotating shaft is fixedly connected with the separation top board, separating top board can rotate with respect to constant temperature water tank, be provided with septated hole on the separation top board, silver slurry cup is placed in septated hole.
Further, be provided with equably three above back-up blocks on the sustained height of constant temperature water tank inwall, described pallet is placed on back-up block.
Owing to having set up the structure of depositing a plurality of silver slurry cups on constant temperature water tank, constant temperature water tank not only provides the chilled water of constant temperature for the slot type check-out console, and can carry out cooling processing in advance to a plurality of silver to be checked slurry cups simultaneously, so just can carry out continuous detecting to a plurality of silver-colored slurry samples to be checked, when detecting, silver slurry in silver slurry cup to be checked does not need to carry out the constant temperature processing on the slot type check-out console again to be waited for, can directly carry out viscosity measurements.If the silver-colored slurry viscosity Thermostatic detection device of applicant's design is equipped with such constant temperature water tank, can guarantee the accuracy that silver-colored slurry viscosity is measured, silver-colored slurry to be checked can directly be detected, can carry out continuous detecting to a plurality of silver-colored slurry samples, improved detection efficiency simultaneously.
The accompanying drawing explanation
Below in conjunction with drawings and Examples, the utility model is further illustrated.
The structural representation that Fig. 1 is silver-colored slurry viscosity Thermostatic detection device;
Fig. 2 is structural representation of the present invention;
Fig. 3 is for separating the schematic diagram of top board;
The schematic diagram that Fig. 4 is supporting plate;
In figure: the l-constant temperature water tank; The 2-ebullator; The 3-refrigeration machine; The 4-rising pipe; The 5-return pipe; 6-silver slurry cup; The 7-rotating shaft; The 8-pallet; 9-separates top board; The 10-back-up block; 11-slot type check-out console; The 12-viscosimeter; The 81-permeable hole; The 82-shaft hole; The 91-septated hole.
Embodiment
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described:
Described silver-colored paste viscosity detection constant-temperature pretreatment water tank, as shown in Figure 2 to 4, it comprises constant temperature water tank 1, ebullator 2, refrigeration machine 3, rising pipe 4, return pipe 5, silver slurry cup 6, rotating shaft 7, pallet 8 and separation top board 9, ebullator 2 liquid sucting ports with at constant temperature water tank l intracavity bottom, communicate, the liquid outlet of ebullator 2 interlinks by rising pipe 4 and slot type check-out console 11, return pipe 5 interlinks with the inner chamber of constant temperature water tank l, refrigeration machine 3 is arranged on the lower end of constant temperature water tank 1, be provided with equably three above back-up blocks 10 on the sustained height of constant temperature water tank l inwall, described pallet 8 is placed on back-up block 10, be provided with permeable hole 81 on pallet 8, heart position is provided with shaft hole 82 therein, pallet 8 is corresponding with the height of silver slurry cup 6 to the distance of constant temperature water tank l end face, rotating shaft 7 is sleeved in the shaft hole 82 of pallet 8, the lower end of rotating shaft 7 is placed in the seat hole of constant temperature water tank l bottom, the upper end of rotating shaft 7 is fixedly connected with separation top board 9, separating top board 9 can rotate with respect to constant temperature water tank l, be provided with septated hole 91 on separation top board 9, silver slurry cup 6 is placed in septated hole 91.

Claims (2)

1. a silver-colored paste viscosity detection constant-temperature pretreatment water tank, comprise constant temperature water tank (1), ebullator (2), refrigeration machine (3), rising pipe (4), return pipe (5) and silver slurry cup (6), ebullator (2) liquid sucting port communicates with constant temperature water tank (1) intracavity bottom, the liquid outlet of ebullator (2) interlinks by rising pipe (4) and slot type check-out console (11), return pipe (5) interlinks with the inner chamber of constant temperature water tank (l), refrigeration machine (3) is arranged on the lower end of constant temperature water tank (l), it is characterized in that: further comprising rotating shaft (7), pallet (8) and separation top board (9), pallet (8) is arranged on the inwall of constant temperature water tank (1), be provided with permeable hole (81) on pallet (8), heart position is provided with shaft hole (82) therein, pallet (8) is corresponding with the height of silver slurry cup (6) to the distance of constant temperature water tank (1) end face, rotating shaft (7) is sleeved in the shaft hole (82) of pallet (8), the lower end of rotating shaft (7) is placed in the seat hole of constant temperature water tank (l) bottom, the upper end of rotating shaft (7) is fixedly connected with separation top board (9), separating top board (9) can rotate with respect to constant temperature water tank (1), be provided with septated hole (91) on separation top board (9), silver slurry cup (6) is placed in septated hole (91).
2. according to the described silver-colored paste viscosity detection constant-temperature pretreatment water tank of claim l, it is characterized in that: be provided with equably three above back-up blocks (10) on the sustained height of constant temperature water tank (1) inwall, described pallet (8) is placed on back-up block (10).
CN 201010283674 2010-09-13 2010-09-13 Silver paste viscosity detection constant-temperature pretreatment water tank Active CN101975725B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104330335B (en) * 2014-10-24 2017-06-13 无锡帝科电子材料科技有限公司 A kind of device for the detection of electric slurry plasticity
CN110879189A (en) * 2019-12-10 2020-03-13 上海航天化工应用研究所 Solid propellant slurry viscosity multi-sample continuous test device
CN114199332B (en) * 2021-11-30 2024-07-16 保定雷弗流体科技有限公司 Automatic detection device and method for flow of transmission pump

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3777551A (en) * 1971-12-20 1973-12-11 Texaco Inc Continuous recording viscometer
CN2814396Y (en) * 2005-08-22 2006-09-06 北京普利生仪器有限公司 Fluid viscosity measuring device based on adding sample capillary tube
CN200972464Y (en) * 2006-05-26 2007-11-07 中国水产科学研究院东海水产研究所 Device for investigating activity of micro carbonic anhydrase
CN201765142U (en) * 2010-09-13 2011-03-16 常州亿晶光电科技有限公司 Constant temperature pretreatment water tank for silver paste viscosity detection

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3777551A (en) * 1971-12-20 1973-12-11 Texaco Inc Continuous recording viscometer
CN2814396Y (en) * 2005-08-22 2006-09-06 北京普利生仪器有限公司 Fluid viscosity measuring device based on adding sample capillary tube
CN200972464Y (en) * 2006-05-26 2007-11-07 中国水产科学研究院东海水产研究所 Device for investigating activity of micro carbonic anhydrase
CN201765142U (en) * 2010-09-13 2011-03-16 常州亿晶光电科技有限公司 Constant temperature pretreatment water tank for silver paste viscosity detection

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