CN101956335B - Formula of foam dyeing system and preparation method thereof - Google Patents
Formula of foam dyeing system and preparation method thereof Download PDFInfo
- Publication number
- CN101956335B CN101956335B CN2010102963091A CN201010296309A CN101956335B CN 101956335 B CN101956335 B CN 101956335B CN 2010102963091 A CN2010102963091 A CN 2010102963091A CN 201010296309 A CN201010296309 A CN 201010296309A CN 101956335 B CN101956335 B CN 101956335B
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- China
- Prior art keywords
- foam
- dyeing system
- reactive
- foam dyeing
- disperse
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000006260 foam Substances 0.000 title claims abstract description 59
- 238000004043 dyeing Methods 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 21
- 239000002562 thickening agent Substances 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 10
- 238000005187 foaming Methods 0.000 claims abstract description 8
- 239000000975 dye Substances 0.000 claims description 33
- 239000004604 Blowing Agent Substances 0.000 claims description 14
- VGKYEIFFSOPYEW-UHFFFAOYSA-N 2-methyl-4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound Cc1cc(ccc1O)N=Nc1ccc(cc1)N=Nc1ccccc1 VGKYEIFFSOPYEW-UHFFFAOYSA-N 0.000 claims description 10
- TUXJTJITXCHUEL-UHFFFAOYSA-N disperse red 11 Chemical compound C1=CC=C2C(=O)C3=C(N)C(OC)=CC(N)=C3C(=O)C2=C1 TUXJTJITXCHUEL-UHFFFAOYSA-N 0.000 claims description 10
- 239000000986 disperse dye Substances 0.000 claims description 6
- 239000000985 reactive dye Substances 0.000 claims description 6
- 239000004744 fabric Substances 0.000 abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000001035 drying Methods 0.000 abstract description 3
- 239000004753 textile Substances 0.000 abstract description 3
- 239000004088 foaming agent Substances 0.000 abstract 2
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 3
- 238000009980 pad dyeing Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000001045 blue dye Substances 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000010016 exhaust dyeing Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052594 sapphire Inorganic materials 0.000 description 1
- 239000010980 sapphire Substances 0.000 description 1
- 238000007592 spray painting technique Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
The invention belongs to the field of textile, and particularly relates to a formula of a foam dyeing system and a preparation method thereof. According to the formula of the foam dyeing system, each liter of foaming dyeing system comprises 2 to 6 milliliters of foaming agent, 1 to 5 milliliters of thickening agent and 10 to 150 grams of dye. The preparation method comprises the following steps of: placing the foaming agent, the thickening agent and the dye prepared according to the proportion into a foaming container, mixing the materials to prepare the foam dyeing system, and stirring the dye at room temperature sequentially at low speed and increased speed; and placing the stirred dye into a material dissolution cylinder of a foam dyeing device, sucking the dye to a foam generator, setting a foam ratio and generating foams. Compared with conventional padding technology, the formula of the foam dyeing system saves water by a half, saves energy sources consumed by the drying of fabrics by a half, shortens the drying time and reduces the cost.
Description
Technical field
The invention belongs to field of textiles, be specifically related to prescription of a kind of foam dyeing system and preparation method thereof.
Background technology
In the dyeing and finishing technology of textiles, the method that adopts usually is that dyestuff is mixed with quantitative water, and they are stirred, and forms the foam dyeing system.This system is medium with water, but owing to lack auxiliary agent in the dyestuff, astable foam does not take place dyestuff, can not use form dyeing machine that cloth is dyeed, and can only pad dyestuff, with padding machine pad dyeing material on the cloth.The shortcoming of this technology is that to pad the liquid carrying rate of dyestuff higher, has consumed a large amount of water, and in the process of oven dry cloth cover, can consume great amount of heat energy.Therefore, need to reduce the band liquid measure of fabric in the process, reduce environmental pollution, reduce the consumption of the energy.
Summary of the invention
Technical problem to be solved by this invention is, the prescription and preparation method thereof of the foam dyeing system of the astable foam of a speciogenesis is provided.
The prescription of this foam dyeing system contains blowing agent 2～6ml/L, thickener 1～5ml/L, dyestuff 10～150 g/L.
Above-mentioned blowing agent is Sulfanole 270, by the Ou Nuofa Chemical Manufacture.
Above-mentioned thickener is at least a kind of among ACE-63, the ACE-70, and star Co., Ltd produces by the pool, Shanghai.
Above-mentioned dyestuff is made up of DISPERSE DYES, REACTIVE DYES, and DISPERSE DYES are at least a in disperse red, disperse yellow, the disperse blue; REACTIVE DYES are at least a in reactive red, reactive yellow, the reactive blue.
The proportioning of DISPERSE DYES and REACTIVE DYES is 0.8～1.2:1.
The preparation method of above-mentioned a kind of foam dyeing system comprises following step:
A, the blowing agent that will prepare in proportion, thickener and dyestuff drop in the foaming vessel, are hybridly prepared into the foam dyeing system, at room temperature stir 2～5min at a slow speed, quicken to stir 3～7min again;
B, the dyestuff after will stirring are thrown into the change material cylinder of form dyeing machine, again dyestuff are drawn to foam maker, set the bubble ratio of 1:4～1:6, produce foam.
Just having begun speed of agitator among the step a is 300～600r/min, and rotating speed is 1000～1400r/min when quickening to stir, and foam diameter is 6～10um, and the half-life was less than 6 minutes.
The invention has the beneficial effects as follows,, make the foam dyeing system that the instability foam can take place owing to adopt the prescription and the preparation method of above-mentioned foam dyeing system; Can dye to cloth with form dyeing machine, again dyestuff is drawn to foam maker spray-painting material on the cloth and go up dyeing, compare with exhaust dyeing; Practiced thrift half the with water gaging; The energy conservation that consumed of oven dry half the, shortened drying time, reduced cost.
The specific embodiment
Below in conjunction with the specific embodiment the present invention is illustrated further, but do not limit the present invention with this.
Embodiment 1
The prescription of this foam dyeing system contains blowing agent Sulfanole 270,2ml/L, and thickener ACE-63,5ml/L, reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, dispersed blue dye are mixed with the dye solution that concentration is 50g/L.
With blowing agent Sulfanole 270; 2ml/L, thickener ACE-63,5ml/L and reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are formulated as in the dye solution input foaming vessel that concentration is 50g/L, are hybridly prepared into the foam dyeing system; At room temperature stir 4min with 400r/min; Stir 5min with 1200r/min again, this moment, foam diameter was 7um, and the half-life was less than 6 minutes.
Dyestuff after stirring is thrown into the change material cylinder of form dyeing machine, again dyestuff is drawn to foam maker, set the bubble ratio of 1:4, produce foam.
The foam dyeing index is compared with pad dyeing dyeing index, and the various performances of fabric are following:
T/C24X24 100X52 is sapphire blue
Pad dyeing dyeing index foam dyeing index
Ultimate strength 602N/315N 601N/317N
Tearing brute force 31.5N/20.6N 31N/21.2N
3.5 grades 4.0 grades of former changes
Be stained with 3.5 grades 3.5 grades in vain
Do 4.5 grades 4.5 grades
Wet 2.5 grades 2.5 grades
Embodiment 2
The prescription of this foam dyeing system contains blowing agent Sulfanole 270,4ml/L, and thickener ACE-70,4ml/L, reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are mixed with the dye solution that concentration is 10 g/L.
With blowing agent Sulfanole 270; 4ml/L, thickener ACE-70, it is that the dye solution of 10 g/L is put in the foaming vessel that 4ml/L and reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are mixed with concentration, is hybridly prepared into the foam dyeing system; At room temperature stir 4min with 300r/min; Stir 5min with 1000r/min again, this moment, foam diameter was 8um, and the half-life was less than 6 minutes.
Dyestuff after stirring is thrown into the change material cylinder of form dyeing machine, again dyestuff is drawn to foam maker, set the bubble ratio of 1:5, produce foam.
Embodiment 3
The prescription of this foam dyeing system contains blowing agent Sulfanole 270,6ml/L, and thickener ACE-63,4ml/L, reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are mixed with the dye solution that concentration is 150 g/L.
With blowing agent Sulfanole 270; 6ml/L, thickener ACE-63,4ml/L and reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are mixed with in the dye solution input foaming vessel that concentration is 150 g/L, are hybridly prepared into the foam dyeing system; At room temperature stir 4min with 500r/min; Stir 5min with 1400r/min again, this moment, foam diameter was 7um, and the half-life was less than 6 minutes.
Dyestuff after stirring is thrown into the change material cylinder of form dyeing machine, again dyestuff is drawn to foam maker, set the bubble ratio of 1:6, produce foam.
Embodiment 4
The prescription of this foam dyeing system contains blowing agent Sulfanole 270,3ml/L, and thickener ACE-70,1ml/L, reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are mixed with the dye solution that concentration is 80 g/L.
With blowing agent Sulfanole 270; 3ml/L, thickener ACE-70,1ml/L and reactive red, reactive yellow, reactive blue, disperse red, disperse yellow, disperse blue are mixed with in the dye solution input foaming vessel that concentration is 80 g/L, are hybridly prepared into the foam dyeing system; At room temperature stir 4min with 400r/min; Stir 5min with 1300r/min again, this moment, foam diameter was 7um, and the half-life was less than 6 minutes.
Dyestuff after stirring is thrown into the change material cylinder of form dyeing machine, again dyestuff is drawn to foam maker, set the bubble ratio of 1:5, produce foam.
Claims (8)
1. the prescription of a foam dyeing system; It is characterized in that: contain blowing agent 2～6ml/L in the described prescription; Thickener 1～5ml/L; Dye strength is 10～150 g/L, and described dyestuff is made up of DISPERSE DYES and REACTIVE DYES, and the proportioning of DISPERSE DYES and REACTIVE DYES is 0.8～1.2:1.
2. the prescription of a kind of foam dyeing system as claimed in claim 1 is characterized in that: described blowing agent is Sulfanole 270.
3. the prescription of a kind of foam dyeing system as claimed in claim 1 is characterized in that: described thickener is at least a among ACE-63, the ACE-70.
4. the prescription of a kind of foam dyeing system as claimed in claim 1 is characterized in that: described DISPERSE DYES are at least a in disperse red, disperse yellow, the disperse blue.
5. the prescription of a kind of foam dyeing system as claimed in claim 1 is characterized in that: described REACTIVE DYES are at least a in reactive red, reactive yellow, the reactive blue.
6. the preparation method of a kind of foam dyeing system as claimed in claim 1 comprises following step:
A, the blowing agent that will prepare in proportion, thickener and dyestuff drop in the foaming vessel, are hybridly prepared into the foam dyeing system, at room temperature stir 2～5min at a slow speed, quicken to stir 3～7min again;
B, the dyestuff after will stirring are thrown into the change material cylinder of form dyeing machine, again dyestuff are drawn to foam maker, set the bubble ratio of 1:4～1:6, produce foam.
7. the preparation method of a kind of foam dyeing system as claimed in claim 6 is characterized in that: just having begun speed of agitator among the said step a is 300～600r/min, and rotating speed is 1000～1400r/min when quickening to stir.
8. the preparation method of a kind of foam dyeing system as claimed in claim 6 is characterized in that: described foam diameter is 6～10um, and the half-life was less than 6 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102963091A CN101956335B (en) | 2010-09-29 | 2010-09-29 | Formula of foam dyeing system and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102963091A CN101956335B (en) | 2010-09-29 | 2010-09-29 | Formula of foam dyeing system and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101956335A CN101956335A (en) | 2011-01-26 |
| CN101956335B true CN101956335B (en) | 2012-08-22 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010102963091A Expired - Fee Related CN101956335B (en) | 2010-09-29 | 2010-09-29 | Formula of foam dyeing system and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN101956335B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102650096B (en) * | 2011-02-28 | 2014-05-28 | 上海辉誉化工有限公司 | Reactive dyeing method applying color fixing liquid in foamed manner |
| CN102650097B (en) * | 2011-02-28 | 2014-05-28 | 上海辉誉化工有限公司 | Foam spraying dyeing method adopting reactive dyes |
| CN109056368A (en) * | 2018-07-02 | 2018-12-21 | 苏州大学 | Nanometer bubble dyeing and finishing functional liquid and dyeing and finishing technology |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101435162A (en) * | 2008-12-29 | 2009-05-20 | 郑州枫林无纺科技有限公司 | Formula of foam dyeing system and foam dyeing method of base cloth for multifunctional water stabbed superfine fiber leather |
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- 2010-09-29 CN CN2010102963091A patent/CN101956335B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101435162A (en) * | 2008-12-29 | 2009-05-20 | 郑州枫林无纺科技有限公司 | Formula of foam dyeing system and foam dyeing method of base cloth for multifunctional water stabbed superfine fiber leather |
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| Publication number | Publication date |
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| CN101956335A (en) | 2011-01-26 |
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Granted publication date: 20120822 Termination date: 20180929 |