CN101955720A - Glittery metallic powder coating and preparation method thereof - Google Patents
Glittery metallic powder coating and preparation method thereof Download PDFInfo
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Abstract
The invention provides a glittery metallic powder coating and a preparation method thereof, which can solve the problems that the metallic glittery effect is undesirable, and the coat is easy to wear away and distributed unevenly existing in the prior art. The glittery metallic powder coating comprises the following components in percentage by weight: 50 to 70 percent of transparent powder, 25 to 45 percent of dark and light covering power, 2.0 to 5.0 percent of coarse aluminum silver powder, 0.05 to 0.5 percent of fine aluminum silver powder, 0.1 to 1 percent of wax powder, 0.1 to 1 percent of defoaming agent, and 0.05 to 0.5 percent of fluidity improver. The invention also provides a method for preparing the glittery metallic powder coating. The glittery metallic powder coating of the invention has the advantages that: the leveling can be improved; the surface of the coat has a strong metallic glittery effect, and the coat is easy to wear away and uniform in color so as to give people a fashionable and beautiful feeling and show a high-grade decoration effect, therefore, the glittery metallic powder coating is very suitable for high-grade decoration field; and meanwhile, the production cost of the glittery metallic powder coating is not high.
Description
Technical field
The invention belongs to the decorative paint technical field, specifically, relate to metal powder coating of a kind of flash effect and preparation method thereof.
Background technology
Powder coating is a kind of solid powder paint of not solvent-laden 100%, and at normal temperatures, through electrostatic spraying or fluidized bed dipping, reheat baking melting and solidification forms the permanent of smooth and films.The flash of light metal powder coating is a kind of of powder coating, be meant and contain various powder coating with metallic travel pigment, because it can show a kind of bright, luxurious decorative effect, flash effect is strong, fashion is attractive in appearance, is fit to very that household, ornaments and automobile etc. are indoor, the spraying of outer object.
It is inhomogeneous that but the metal of existing flash of light metal powder coating disperses, reduced the gloss of powder coating, and when metal flashing powder adopts the most frequently used aluminium powder, will be because of contacting and the oxidation blackening with air for a long time, thereby lost the effect of flash of light, simultaneously because the conductivity difference of other materials in metallic aluminium powder and the powder coating is very big, when metal powder content is higher, being separated of metal powder and end powder taken place in the spraying especially easily, cause coating that problems such as mill flower take place, also brought a lot of difficult problems to spray coating constructing technique; But metal powder content is low excessively, then is difficult to the flash effect that reaches satisfied.How to solve the problems of the technologies described above, improve the separation problem of metal powder in powder coating, and it is evenly distributed, the flash effect that strengthens powder coating then is the problem that the present invention faced.
Summary of the invention
The invention provides a kind of flash of light metal powder coating and preparation method thereof, can solve that the metallic travel that prior art exists is undesirable, mill flower and problem pockety easily take place coating.
For solving the problems of the technologies described above, the present invention adopts following technical proposals,
A kind of flash of light metal powder coating, comprise following components in weight percentage content: clear bottom powder 50%-70%, dark and light color hides total consumption 25%-45% of end powder, crude aluminum silver powder 2.0-5.0%, thin aluminium silver powder 0.05-0.5%, wax powder 0.1-1%, defoamer 0.1-1%, fluidity improver 0.05-0.5%.The wax powder that adopts is a scratch resistance wax powder.
Clear bottom powder in the composition of the present invention mainly act as filmogen, because transparent, can effectively represent the metal flicker effect of aluminium silver powder.Dark and light color hides end powder and will be used, and is used for adjusting color.And two kinds of color coordination get up to use, can produce the surperficial mottled effect of metalloid powder, can reduce aluminium silver powder consumption significantly, both reduced cost, help spraying application again, since the opacifying power of flash of light aluminium silver powder relatively a little less than, more than two kinds hide end powder and can also increase opacifying power, prevent to expose the ground color.
Further, be the charging property between minimizing end powder and the aluminium silver powder and the difference of electroconductibility, growth agent is all added in the separation when effectively reducing their spraying applications in powder at the bottom of three kinds, strengthen the charging property of end powder, reduced resistance, the prescription of wherein said clear bottom powder is by weight: resin and solidifying agent 70-80%, flow agent 0.5-1%, filler 20-30%, growth agent 0.1-0.5%, air release agent 0.3%-1.0%, wetting dispersing agent 0.3%-1.0%;
The prescription that described dark color and light color hide end powder is by weight: resin and solidifying agent 55-75%, flow agent 0.5-1%, filler and pigment 22-40%, growth agent 0.1-0.5%, air release agent 0.3%-1.0%, wetting dispersing agent 0.3%-1.0%, dark and light color hides the end both ratios of powder and adjusts according to the color of final finished; Pigment is selected ordinary powder coating pigment for use.
Further, the size distribution that described clear bottom powder, dark color and light color hide end powder is d10＞d50 * 30%, d90＜d50 * 160%, and the separation of powder when spraying to reduce guarantees to reclaim powder and also can normally add use.D10 refers to 10% grain diameter, and similarly, d90 refers to 90% grain diameter.
Further, described crude aluminum silver powder is non-floating type, and particle diameter d50 is the 40-60 micron; D50 refers to the intermediate value of particle diameter, when this particle diameter, has 50% grain diameter bigger than it, has 50% grain diameter littler than it;
Described thin aluminium silver powder is non-floating type, and particle diameter d50 is the 5-20 micron;
Described wax powder, defoamer and fluidity improver use after 80 eye mesh screens sieve.
Again further, described defoamer is selected BYK961 or PP1362D for use, and described fluidity improver is a gaseous oxidation aluminium.
Crude aluminum silver powder particles particle diameter is bigger, is used for producing the intensive metallic travel, thereby its consumption must be sufficient, is preferably in more than 2%.Thin aluminium silver powder particles is less, is used for increasing metal-like, can also improve the opacifying power of coating, especially when viewing angle hour, the effective greyish white color effects of cover surface.
Scratch resistance wax powder has the surperficial smooth property of raising and increases hard effect, makes coatingsurface smooth evenly.Because after metal powder was scratched by friction, the aluminium silver layer was damaged and blackening, this wax powder can effectively address this problem.Gaseous oxidation aluminium can effectively improve the fluffiness and the flowability of powder, and can adjust the charge distribution of powder, makes powder even, separates between powder and the aluminium silver powder at the bottom of when preventing spraying application.Defoamer gas in the promotion system when paint solidification is discharged, and carries aluminium silver powder come-up, and coating top aluminium silver powder is concentrated, and can be issued to flash effect preferably in the prerequisite of lower aluminium silver powder consumption.
Further, described resin is a vibrin, one or both in the Resins, epoxy; Described solidifying agent comprises isocyanuric acid three-glycidyl ester and hydroxyalkyl amide class solidifying agent; Described filler comprises barium sulfate and lime carbonate; Barium sulfate and lime carbonate particle diameter are the 1000-1800 mesh sieve; Described growth agent is SATA308; Described wax powder is polyethylene wax powder or the cured powder of tetrafluoroethylene; Described air release agent is selected st-yrax or modified polyamide wax for use; Described wetting dispersing agent is 701 polyacrylate(s) materials.
A kind of preparation method of the metal powder coating that glistens comprises the steps:
1) take by weighing material respectively according to following weight percentage, clear bottom powder 50%-70%, dark and light color hides total consumption 25%-45% of end powder;
2) above-mentioned material is placed in the high-speed mixer and to mix 5-10 minute, under 95-115 °, melt extrude compressing tablet with forcing machine then;
3) above-mentioned compressing tablet is worn into the powder particle of median size 30-50 micron respectively with the air classifying barreling, and then the crude aluminum silver powder of the 2.0-5.0% of adding product gross weight, the thin aluminium silver powder of 0.05-0.5%, the wax powder of 0.1-1%, the fluidity improver of 0.05-0.5%, the defoamer mixing of 0.1-1% 10-20 minute, pack at last the finished product powder coating.
Compared with prior art, the present invention has the following advantages and positively effect:
Flash of light metal powder coating provided by the invention can improve the film coated surface planarization, and the surface has strong metallic travel, and production cost is not high.
1, end powder adds growth agent, and powder promotions in effectively reduces separating between aluminium silver powder and end powder, improves discoloration problem behind spraying decoration in the spraying process and the interpolation recovery powder.
2, add dark, shallow two kinds and hide end powder, guarantee opacifying power, and can produce the effect of metalloid powder, thereby significantly reduce aluminium silver powder consumption, alleviate high metal content and give a series of problems of dusting and bringing.
3, add gaseous oxidation aluminium: improve the flowability of powder, dispersiveness, homogeneity.
4, add defoamer, impel aluminium silver powder come-up, strengthen flash effect.
Spray the article of powder coating of the present invention, have the intensive metallic travel, coating is difficult for taking place the mill flower, and color and luster is even, and fashion is attractive in appearance, demonstrates high-grade decorative effect, and durable in use, is fit to very much high-grade decoration field.
Embodiment
The present invention is described in further detail below in conjunction with examples of implementation.
Embodiment one:
A kind of prescription of the metal powder coating that glistens is as follows:
Clear bottom powder prescription: vibrin 350 grams, Resins, epoxy 350 grams, filler barium sulfate 240 grams, flow agent PV8810 gram, air release agent st-yrax 5 grams, wetting dispersing agent BLC7015 gram, growth agent SATA3083 gram;
Light color hides end powder prescription: vibrin 320 grams, Resins, epoxy 320 grams, filler barium sulfate 90 grams, flow agent PV8810 gram, air release agent st-yrax 5 grams, wetting dispersing agent BLC7015 gram, growth agent SATA3083 gram, titanium dioxide r902 250 grams, pigment ultramarine 1 gram, pigment carbon black 0.2 gram;
The dark end powder prescription that hides: vibrin 320 grams, Resins, epoxy 320 grams, filler barium sulfate 140 grams, flow agent PV8810 gram, air release agent st-yrax 5 grams, wetting dispersing agent BLC7015 gram, growth agent SATA3083 gram, titanium dioxide r902 200 grams, pigment ultramarine 5 grams, pigment carbon black 1 gram;
Thin aluminium silver powder: 2 grams, particle diameter D5012 micron;
Crude aluminum silver powder: 25 grams, particle diameter D5045 micron;
Scratch resistance wax powder TF1725:5 gram uses after 80 eye mesh screens sieve;
Defoamer BYK961:5 gram uses after 80 eye mesh screens sieve;
Gaseous oxidation aluminium, 1 gram uses after 80 eye mesh screens sieve;
Concrete production technique: with the clear bottom powder according to above-mentioned prescription batching after, put into mixer and mixed 5 minutes, the compound that mixes is put into forcing machine descends mixing extruding at 100 degrees centigrade, compressing tablet fragmentation then, tablet after the fragmentation is ground, obtain the clear bottom powder, standby.Light color hides end powder, the dark end powder that hides, and also makes in the same way respectively.
Get clear bottom powder 670 grams, light color hides end powder 100 grams, dark end powder 200 grams that hide, thin aluminium silver powder 2 grams, crude aluminum silver powder 25 grams, scratch resistance wax powder TF17255 gram, defoamer BYK9615 gram, gaseous oxidation aluminium 1 gram, put into and be mixed together 10 minutes, become the powder coating finished product, the packing warehouse-in.
The performance test of the powder coating that present embodiment makes is as follows:
| Sequence number | Interventions Requested | Inspecting standard | Performance index |
| 1 | Paint film appearance | GB/T?9761-1988 | Smooth |
| 2 | Shock test | GB/T?1732-1993 | Recoil 50KGcm flawless |
| 3 | Draw the lattice experiment | GB/T?9286-1998 | Be not more than 1 grade |
| 4 | Pliability test | GB/T?6742-2007 | By 3mm plug flawless |
| 5 | Pencil hardness | GB/T?6739-2006 | H |
| 6 | The cupping experiment | GB/T?9753-2007 | 〉=7mm bisque crack-free |
| 7 | Granularity | ISO?8130-13-2001 | Mean particle size 30-50um |
Embodiment two:
The prescription of flash of light metal powder coating is as follows:
Clear bottom powder prescription: vibrin 720 grams, TGIC 55 grams, filler barium sulfate 200 grams, flow agent L58810 gram, air release agent st-yrax 5 grams, brightening agent BLC7015 gram, growth agent SATA3083 gram;
Light color hides end powder prescription: vibrin 720 grams, TGIC 55 grams, flow agent L58810 gram, air release agent st-yrax 5 grams, brightening agent BLC7015 gram, growth agent SATA3083 gram, titanium dioxide R706200 gram, pigment iron oxide yellow 5 grams;
The dark end powder prescription that hides: vibrin 720 grams, TGIC 55 grams, flow agent L588 10 grams, air release agent st-yrax 5 grams, brightening agent BLC7015 gram, growth agent SATA3083 gram, titanium dioxide R706200 gram, pigment iron oxide yellow 15 grams, pigment carbon black 1 gram;
Thin aluminium silver powder: 3 grams, particle diameter D5015 micron;
Crude aluminum silver powder: 25 grams, particle diameter D5050 micron;
Scratch resistance wax powder TF1778:5 gram uses after 80 eye mesh screens sieve;
Defoamer PP1362D:5 gram uses after 80 eye mesh screens sieve;
Gaseous oxidation aluminium, 1 gram uses after 80 eye mesh screens sieve;
Concrete production technique: with the clear bottom powder according to above-mentioned prescription batching after, put into mixer and mixed 5 minutes, the compound that mixes is put into forcing machine descends mixing extruding at 100 degrees centigrade, compressing tablet fragmentation then, tablet after the fragmentation is ground, obtain the clear bottom powder, standby.Light color hides end powder, the dark end powder that hides, and also makes in the same way respectively.
Get clear bottom powder 670 grams, light color hides end powder 150 grams, dark end powder 150 grams that hide, thin aluminium silver powder 3 grams, crude aluminum silver powder 25 grams, scratch resistance wax powder TF17785 gram, defoamer PP1362D 5 grams, gaseous oxidation aluminium 1 gram, put into and be mixed together 10 minutes, become the powder coating finished product, the packing warehouse-in.
The performance test of the powder coating that present embodiment makes is as follows:
| Sequence number | Interventions Requested | Inspecting standard | Performance index |
| 1 | Paint film appearance | GB/T?9761-1988 | Smooth |
| 2 | Shock test | GB/T?1732-1993 | Recoil 50KGcm flawless |
| 3 | Draw the lattice experiment | GB/T?9286-1998 | Be not more than 1 grade |
| 4 | Pliability test | GB/T?6742-2007 | By 3mm plug flawless |
| 5 | Pencil hardness | GB/T?6739-2006 | H |
| 6 | The cupping experiment | GB/T?9753-2007 | 〉=7mm bisque crack-free |
| 7 | Granularity | ISO?8130-13-2001 | Mean particle size 30-50um |
Check: adopt new powder spraying back and recovery powder spraying back color and effect comparison method to test.Get the new powder of 500 grams, 3 iron plates that about 15 * 20cm is square, a clean plastic cloth.Earlier plastic cloth is completed below iron plate, to first iron plate spraying, the about 60-100 micron of coating thickness then with its taking-up, is put into second iron plate spraying, up to powder has been sprayed.Second iron plate taken out, and the recovery powder that drops on the plastic cloth is collected.Put into the 3rd block of plate, spray with the recovery powder, coating thickness also is at the 60-100 micron.Then with first and the 3rd iron plate baking-curing that has sprayed powder, measure the aberration between the two boards, Δ E＜3.0, and visual flash effect difference gets final product when little.If with the finished product powder that existing ordinary skill is made, aberration Δ E is generally more than 4.0, and visual effect difference is obvious.
The above only is preferred embodiment of the present invention, is not to be the restriction of the present invention being made other form, and any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the equivalent embodiment of equivalent variations.But every technical solution of the present invention content that do not break away to any simple modification, equivalent variations and remodeling that above embodiment did, still belongs to the protection domain of technical solution of the present invention according to technical spirit of the present invention.
Claims (10)
- One kind the flash of light metal powder coating, it is characterized in that comprising following components in weight percentage content: clear bottom powder 50%-70%, dark and light color hides total consumption 25%-45% of end powder, crude aluminum silver powder 2.0-5.0%, thin aluminium silver powder 0.05-0.5%, wax powder 0.1-1%, defoamer 0.1-1%, mobile properties-correcting agent 0.05-0.5%.
- 2. flash of light metal powder coating according to claim 1 is characterized in that: the prescription of described clear bottom powder is by weight: resin and solidifying agent 70-80%, flow agent 0.5-1%, filler 20-30%, growth agent 0.1-0.5%, air release agent 0.3-1.0%, wetting dispersing agent 0.3-1.0%;The prescription that described dark color and light color hide end powder is by weight: resin and solidifying agent 55-75%, flow agent 0.5-1%, filler and pigment 22-40%, growth agent 0.1-0.5%, air release agent 0.3-1.0%, wetting dispersing agent 0.3-1.0%, dark and light color hides the end both ratios of powder and adjusts according to the color of final finished.
- 3. flash of light metal powder coating according to claim 2 is characterized in that: the size distribution that described clear bottom powder, dark color and light color hide end powder is d10＞d50 * 30%, d90＜d50 * 160%.
- 4. flash of light metal powder coating according to claim 1 and 2 is characterized in that: described crude aluminum silver powder is non-floating type, and particle diameter d50 is the 40-60 micron; Described thin aluminium silver powder is non-floating type, and particle diameter d50 is the 5-20 micron; Described wax powder, defoamer and fluidity improver use after 80 eye mesh screens sieve.
- 5. flash of light metal powder coating according to claim 1 and 2 is characterized in that: described defoamer is BYK961, PP1362D, and described fluidity improver is a gaseous oxidation aluminium.
- 6. flash of light metal powder coating according to claim 2 is characterized in that: described resin is a vibrin, one or both in the Resins, epoxy; Described solidifying agent is one or both in isocyanuric acid three-glycidyl ester, the hydroxyalkyl amide class solidifying agent.
- 7. flash of light metal powder coating according to claim 2 is characterized in that: described flow agent is the esters of acrylic acid material; Described filler is one or both in barium sulfate, the lime carbonate, and barium sulfate and lime carbonate particle diameter are the 1000-1800 mesh sieve.
- 8. flash of light metal powder coating according to claim 2 is characterized in that: described growth agent is SATA308; Described wax powder is one or both in polyethylene wax powder, the cured powder of tetrafluoroethylene.
- 9. flash of light metal powder coating according to claim 2 is characterized in that: described air release agent is one or both in st-yrax, the modified polyamide wax; Described wetting dispersing agent is 701 polyacrylate(s) materials.
- 10. the preparation method of the metal powder coating that glistens is characterized in that comprising the steps:1) take by weighing material respectively according to following weight percentage, clear bottom powder 50%-70%, dark and light color hides total consumption 25%-45% of end powder;2) above-mentioned material is placed in the high-speed mixer and to mix 5-10 minute, under 95-115 °, melt extrude compressing tablet with forcing machine then;3) above-mentioned compressing tablet is worn into the powder particle of median size 30-50 micron respectively with air cyclonic separation barreling, and then the crude aluminum silver powder of the 2.0-5.0% of adding product gross weight, the thin aluminium silver powder of 0.05-0.5%, the wax powder of 0.1-1%, the fluidity improver of 0.05-0.5%, the defoamer mixing of 0.1-1% 10-20 minute, pack at last the finished product powder coating.
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| CN109627931A (en) * | 2018-12-12 | 2019-04-16 | 东莞市爱粤金属粉末有限公司 | Outdoor silver color powdery paints and preparation method thereof |
| CN111303736A (en) * | 2020-04-17 | 2020-06-19 | 浙江固丽新材料科技有限公司 | Powder coating |
| CN112538246A (en) * | 2020-12-04 | 2021-03-23 | 惠州莹光塑胶颜料有限公司 | Plastic master batch with metallic luster and preparation method thereof |
| CN115232533A (en) * | 2022-08-19 | 2022-10-25 | 江西锐克斯科技有限公司 | Super-weather-resistant metal powder coating and preparation method thereof |
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