CN101912694A - Compact simultaneous distilling and extracting device - Google Patents
Compact simultaneous distilling and extracting device Download PDFInfo
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- CN101912694A CN101912694A CN 201010251251 CN201010251251A CN101912694A CN 101912694 A CN101912694 A CN 101912694A CN 201010251251 CN201010251251 CN 201010251251 CN 201010251251 A CN201010251251 A CN 201010251251A CN 101912694 A CN101912694 A CN 101912694A
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Abstract
The invention discloses a compact simultaneous distilling and extracting device, which comprises a simultaneous distilling and extracting kit and a condensing system, wherein the simultaneous distilling and extracting kit is formed by interconnecting a water vapor conduit, a condensate return pipe, a water vapor heating sleeve, a solvent vapor conduit and a mixed extracting and condensing cavity; the condensing system comprises a detachable double spiral condensing pipe and a hollow condensing jacket; the double spiral condensing pipe is in ground sleeve joint with the mixed extracting and condensing cavity; and the hollow condensing jacket is matched with the double spiral condensing pipe to form a condensing part of the mixed extracting and condensing cavity. The device combines the technical characteristics of a soxhlet extracting device and a rotary evaporimeter, adopts a double spiral condensing structure, simplifies a heating device, and has the advantages of more compact overall structure, small occupied space, detachability and convenient cleaning; and the difference between mixed extracting and condensing in space position of the cavity body is favorable for separately mixing and condensing the vapor (air), thereby improving the working efficiency of distilling and extracting, and saving energy by 25% by vapor heating.
Description
Technical field
The invention belongs to chemical separating and extract equipment technical field, be specifically related to a kind of compact conformation, easy and simple to handle, little, not fragile, the easy cleaned compact simultaneous distilling and extracting device that takes up space.
Background technology
At present, widely used while distilling and extracting device is the Flath design, is made up of distillation cascade, hybrid extraction condensation chamber, layering return duct three parts.The while distillation extraction instrument of utility model patent ZL 200620134964.6 has increased the device of condensing reflux speed control, and repeatability improves.Because the variation of such distilling and extracting device and Flath design is little, extractant steam and the still inabundant mixing of the sample solution steam of waiting to purify just are condensed into liquid, have therefore reduced the efficient of distillation extraction.Chinese invention patent application (application number: 200710124584.3) the while distilling and extracting device is improved, it has enlarged independent hybrid chamber with the raising distillation efficiency, but still has complex structure, and required working space is big, damage easily, be difficult to defectives such as cleaning.For this reason, the inventor has developed a kind of compact simultaneous distilling and extracting device through lot of experiments, experiment showed, that effect is good.
Summary of the invention
The object of the present invention is to provide a kind of compact conformation, easy and simple to handle, little, not fragile, the easy cleaned compact simultaneous distilling and extracting device that takes up space.
The object of the present invention is achieved like this: comprise distillation extraction external member and condenser system simultaneously, described while distillation extraction external member is interconnected by steam conduit, condensate return pipe, water vapour heating muff, solvent vapour conduit and hybrid extraction condensation chamber and forms; Described condenser system is made up of dismountable double helix condenser pipe, hollow condensation chuck, double helix condenser pipe and hybrid extraction condensation chamber are by the ground socket, and hollow condensation chuck and double helix condenser pipe complement each other to form the condensation portion of hybrid extraction condensation chamber.
The present invention has concentrated the technical characterstic of cable-styled extraction element and Rotary Evaporators, adopts the double helix condensation structure, has simplified heater, and not only overall structure is compact more, and it is little to take up room, and has detachable, convenient advantage of cleaning; Hybrid extraction, be condensate in the locational difference of cavity space and help steam (gas) and mix and to carry out, improved the operating efficiency of distillation extraction with separating of condensation.Steam Heating can save energy 25%.
Description of drawings
Accompanying drawing is an overall structure schematic diagram of the present invention.
Among the figure: 1, steam conduit; 2, condensate return pipe; 3, water vapour heating muff; 4, solvent vapour conduit; 5, hybrid extraction condensation chamber; 6, double helix condenser pipe; 7, hollow condensation chuck; 8, cock; 9, permeability cell; 10, solvent chamber; → indication cooling water flow direction.
The specific embodiment
The invention will be further elaborated below in conjunction with accompanying drawing, but never in any form the present invention is limited, and is equal to replacement based on what the technology of the present invention thinking did, the protection domain that all falls within claims of the present invention and limited.
As shown in drawings, comprise distillation extraction external member and condenser system simultaneously, described while distillation extraction external member is interconnected with hybrid extraction condensation chamber 5 by steam conduit 1, condensate return pipe 2, water vapour heating muff 3, solvent vapour conduit 4 and forms; Described condenser system is made up of dismountable double helix condenser pipe 6, hollow condensation chuck 7, double helix condenser pipe and hybrid extraction condensation chamber are by the ground socket, and hollow condensation chuck and double helix condenser pipe complement each other to form the condensation portion of hybrid extraction condensation chamber.The delivery port of hollow condensation chuck can be connected to form one tunnel condensation water system with the water inlet of double helix condenser pipe; Both also can have independently Inlet and outlet water respectively, form two-way condensation water system.
The equidistant aperture that 3～6 diameters are set is 2～3mm on described hybrid extraction condensation chamber 5 and the wall that water vapour heating muff 3 links to each other, the water vapour in the heating muff can enter the hybrid extraction condensation chamber by these several holes.
Described solvent vapour conduit 4 stretches into 2～4mm in the hybrid extraction condensation chamber 5, and is the involute opening, can prevent that condensation cavity top condensate liquid from flowing in the solvent vapour conduit 4.
Operation principle of the present invention:
The present invention changes the solvent cucurbit and is heated to be steam jacket heating, and the aperture of Steam Heating sleeve pipe on hybrid extraction condensation chamber body wall can keep the continuity that heats.Described solvent vapour conduit stretches into and has formed the involute opening in the hybrid extraction condensation chamber, has prevented that effectively cavity top condensate liquid from flowing into the solvent vapour conduit.Described double helix condenser pipe is fixed on the grinding port plug, is tightly connected by ground and hybrid extraction condensation chamber; Permeability cell is arranged on grinding port plug, can with exterior.Outside atmosphere can be exerted pressure to condensate liquid, and condensate liquid can flow to cavity bottom sooner.Described hybrid extraction condensation chamber top condensation cavity overstriking forms the condensation chuck so that hold the double helix condenser pipe, and dual condensation improves condensation efficiency; Bottom cavity is thinner, holds organic solvent, can raise the solvent height, increases heating surface, improves the efficiency of heating surface of heating muff; Cock is equipped with in the cavity bottom, closes during distillation extraction simultaneously, allows solvent reflux repeatedly, and extraction is opened when finishing, and can collect extract.Extractant steam and the waiting sample solution vapor mixing of purifying places the below of condenser system, and prior art is to place condensing unit top (Flath) or middle (200710124584.3 patent application).
The course of work of the present invention:
Hybrid extraction condensation chamber lower end ground and supporting cucurbit are tightly connected, and the steam one tunnel that cucurbit produces directly enters in the hybrid extraction condensation chamber, and one the tunnel enters extractant heating jacket heated solvent forms steam, mixes in the hybrid extraction condensation chamber, rises.Mist condensation in condenser system of rising flows into cavity lower end and layering, and extractant is got back to the bottom of hybrid extraction condensation chamber, and water is on the upper strata of solvent, and when water level reached the height of condensing reflux pipe, water was back to cucurbit along steam tube wall.
Characteristics of the present invention:
1, changes the solvent cucurbit and be heated to be the steam jacket heating, simplified the heating arrangement of solvent, whole device is simplified; Adopt simultaneously Steam Heating, compared with prior art, can save 25% the energy.
2, hybrid chamber is positioned at the below of condenser system, and the cavity of overstriking has guaranteed have time enough fully to mix when extractant steam and sample solution steam natural to be purified upwards flow.
3, shortened steam (gas) length of tube, reduced the height that steam (gas) climbs, during distillation extraction, steam (gas) conduit is outer can not to install vacuum sleeve additional, more compact structure, easier processing at the same time.
4, the condensation chuck on ground double helix condenser pipe, the cavity wall, dual condensation, condensation efficiency is higher.
5, detachable ground double helix condenser pipe, taking out (can join the protection plastic stent) can be conveniently to hybrid extraction condensation chamber bottom adding extractant, and it is also convenient to clean.
6, owing to reduced by 1 cucurbit, whole device takes up space and only is 1/2 of prior art therefore to have reduced the operating space of distillation extraction simultaneously.
7, the present invention is easier to fix, and only needs fixedly hybrid extraction condensation chamber or double helix condenser pipe, just can be by the fixing whole device that is closely connected.
8, improve operating efficiency, had only 1 cucurbit can single single complete operation, and the double single of the needs of prior art or finish for single 2 times; Compared with prior art, can save adjustment time of 1/2 at least.
Claims (3)
1. compact simultaneous distilling and extracting device, comprise distillation extraction external member and condenser system simultaneously, it is characterized in that: described while distillation extraction external member is by steam conduit (1), condensate return pipe (2), water vapour heating muff (3), solvent vapour conduit (4) interconnects with hybrid extraction condensation chamber (5) and forms, described condenser system is by dismountable double helix condenser pipe (6), hollow condensation chuck (7) is formed, double helix condenser pipe and hybrid extraction condensation chamber are by the ground socket, and hollow condensation chuck and double helix condenser pipe complement each other to form the condensation portion of hybrid extraction condensation chamber.
2. compact simultaneous distilling and extracting device according to claim 1 is characterized in that: the equidistant aperture that 3～6 diameters are set is 2～3mm on described hybrid extraction condensation chamber (5) and the wall that water vapour heating muff (3) links to each other.
3. compact simultaneous distilling and extracting device according to claim 1 is characterized in that: described solvent vapour conduit (4) stretches into 2～4mm in the hybrid extraction condensation chamber (5), and is the involute opening.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010251251 CN101912694B (en) | 2010-08-12 | 2010-08-12 | Compact simultaneous distilling and extracting device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010251251 CN101912694B (en) | 2010-08-12 | 2010-08-12 | Compact simultaneous distilling and extracting device |
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| Publication Number | Publication Date |
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| CN101912694A true CN101912694A (en) | 2010-12-15 |
| CN101912694B CN101912694B (en) | 2013-09-11 |
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| CN 201010251251 Active CN101912694B (en) | 2010-08-12 | 2010-08-12 | Compact simultaneous distilling and extracting device |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102559387A (en) * | 2012-01-19 | 2012-07-11 | 西南大学 | Plant essential oil simultaneous distillation and extraction apparatus |
| CN102581285A (en) * | 2012-03-06 | 2012-07-18 | 宝得粉末注射成形（常熟）有限公司 | Solvent extracting and degreasing machine |
| CN102581284A (en) * | 2012-03-06 | 2012-07-18 | 宝得粉末注射成形（常熟）有限公司 | Degreasing machine with solvent recovery function |
| CN102601371A (en) * | 2012-03-06 | 2012-07-25 | 宝得粉末注射成形（常熟）有限公司 | Defatting mechanism |
| CN102861456A (en) * | 2012-09-25 | 2013-01-09 | 宁波大学 | Inner tube straight-through heat-gathering Soxhlet extractor |
| CN103487458A (en) * | 2013-10-14 | 2014-01-01 | 无锡艾科瑞思产品设计与研究有限公司 | Device and method for detecting Sudan red in chili food |
| CN103550952A (en) * | 2013-11-11 | 2014-02-05 | 江西稀有金属钨业控股集团有限公司 | Wet extraction tank heater and wet extraction tank heating method |
| CN104368168A (en) * | 2013-08-15 | 2015-02-25 | 中国石油天然气股份有限公司 | Method for multimode extraction of soluble substances in solid and distillation recovery and storage of solvent, and apparatus thereof |
| CN105056716A (en) * | 2015-07-31 | 2015-11-18 | 郭应辉 | Drying filtration apparatus |
| CN105126378A (en) * | 2015-09-05 | 2015-12-09 | 腾冲明馨生物技术开发有限公司 | Aromatic-plant distilling extracting pot |
| CN109011672A (en) * | 2018-09-30 | 2018-12-18 | 马鞍山沐及信息科技有限公司 | Condensing unit in a kind of destilling tower |
| CN110314407A (en) * | 2019-08-01 | 2019-10-11 | 山东新希望六和集团有限公司 | A kind of fat rapidly extracting device |
| CN111603795A (en) * | 2020-07-09 | 2020-09-01 | 苏州北开生化设备有限公司 | Efficient rotary evaporation device and working method thereof |
| CN115487536A (en) * | 2022-10-25 | 2022-12-20 | 湖南农业大学 | Large Soxhlet extraction equipment and method for extracting materials |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4006062A (en) * | 1975-01-09 | 1977-02-01 | Council Of Scientific And Industrial Research | Still extractor with novel stopcock means |
| CN2116519U (en) * | 1992-02-25 | 1992-09-23 | 南开大学 | Extractive-distillation apparatus |
| ES2043551A1 (en) * | 1992-05-18 | 1993-12-16 | Consejo Superior Investigacion | Device for the separation and concentration of volatile components of heat-sensitive samples by distillation and simultaneous extraction using organic solvents |
| CN200995139Y (en) * | 2006-12-11 | 2007-12-26 | 中国烟草总公司郑州烟草研究院 | Simultaneous distilling extractor |
| CN101439234A (en) * | 2007-11-21 | 2009-05-27 | 深圳波顿香料有限公司 | Improved device for simultaneous distillation and extraction |
-
2010
- 2010-08-12 CN CN 201010251251 patent/CN101912694B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4006062A (en) * | 1975-01-09 | 1977-02-01 | Council Of Scientific And Industrial Research | Still extractor with novel stopcock means |
| CN2116519U (en) * | 1992-02-25 | 1992-09-23 | 南开大学 | Extractive-distillation apparatus |
| ES2043551A1 (en) * | 1992-05-18 | 1993-12-16 | Consejo Superior Investigacion | Device for the separation and concentration of volatile components of heat-sensitive samples by distillation and simultaneous extraction using organic solvents |
| CN200995139Y (en) * | 2006-12-11 | 2007-12-26 | 中国烟草总公司郑州烟草研究院 | Simultaneous distilling extractor |
| CN101439234A (en) * | 2007-11-21 | 2009-05-27 | 深圳波顿香料有限公司 | Improved device for simultaneous distillation and extraction |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102559387A (en) * | 2012-01-19 | 2012-07-11 | 西南大学 | Plant essential oil simultaneous distillation and extraction apparatus |
| CN102581285A (en) * | 2012-03-06 | 2012-07-18 | 宝得粉末注射成形（常熟）有限公司 | Solvent extracting and degreasing machine |
| CN102581284A (en) * | 2012-03-06 | 2012-07-18 | 宝得粉末注射成形（常熟）有限公司 | Degreasing machine with solvent recovery function |
| CN102601371A (en) * | 2012-03-06 | 2012-07-25 | 宝得粉末注射成形（常熟）有限公司 | Defatting mechanism |
| CN102861456A (en) * | 2012-09-25 | 2013-01-09 | 宁波大学 | Inner tube straight-through heat-gathering Soxhlet extractor |
| CN104368168B (en) * | 2013-08-15 | 2016-08-10 | 中国石油天然气股份有限公司 | In solid, soluble substance multimode is extracted and solvent Distillation recovery deposit method and device |
| CN104368168A (en) * | 2013-08-15 | 2015-02-25 | 中国石油天然气股份有限公司 | Method for multimode extraction of soluble substances in solid and distillation recovery and storage of solvent, and apparatus thereof |
| CN103487458B (en) * | 2013-10-14 | 2015-10-21 | 无锡艾科瑞思产品设计与研究有限公司 | Tonyred pick-up unit in a kind of chilli food and method |
| CN103487458A (en) * | 2013-10-14 | 2014-01-01 | 无锡艾科瑞思产品设计与研究有限公司 | Device and method for detecting Sudan red in chili food |
| CN103550952A (en) * | 2013-11-11 | 2014-02-05 | 江西稀有金属钨业控股集团有限公司 | Wet extraction tank heater and wet extraction tank heating method |
| CN103550952B (en) * | 2013-11-11 | 2015-09-09 | 江西稀有金属钨业控股集团有限公司 | Heater of wet-process extraction groove and heating method |
| CN105056716A (en) * | 2015-07-31 | 2015-11-18 | 郭应辉 | Drying filtration apparatus |
| CN105126378A (en) * | 2015-09-05 | 2015-12-09 | 腾冲明馨生物技术开发有限公司 | Aromatic-plant distilling extracting pot |
| CN109011672A (en) * | 2018-09-30 | 2018-12-18 | 马鞍山沐及信息科技有限公司 | Condensing unit in a kind of destilling tower |
| CN110314407A (en) * | 2019-08-01 | 2019-10-11 | 山东新希望六和集团有限公司 | A kind of fat rapidly extracting device |
| CN111603795A (en) * | 2020-07-09 | 2020-09-01 | 苏州北开生化设备有限公司 | Efficient rotary evaporation device and working method thereof |
| CN115487536A (en) * | 2022-10-25 | 2022-12-20 | 湖南农业大学 | Large Soxhlet extraction equipment and method for extracting materials |
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| CN101912694B (en) | 2013-09-11 |
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