CN101891964A - Cementing material for colored pavement and manufacturing method thereof - Google Patents
Cementing material for colored pavement and manufacturing method thereof Download PDFInfo
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- CN101891964A CN101891964A CN2009101074567A CN200910107456A CN101891964A CN 101891964 A CN101891964 A CN 101891964A CN 2009101074567 A CN2009101074567 A CN 2009101074567A CN 200910107456 A CN200910107456 A CN 200910107456A CN 101891964 A CN101891964 A CN 101891964A
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- agglutinate
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Abstract
The invention discloses a cementing material for a colored pavement and a manufacturing method thereof. The cementing material mainly comprises heavy mineral oil, petroleum resin C5 and/or C9, SBR, SBS, PE, PP and/or PS. The manufacturing method comprises the following steps of: firstly, adding materials into a reaction kettle, and stirring and mixing the materials; secondly, shearing the mixture by using a high-speed shearing machine; and finally, discharging air bubbles generated by the stirring to prepare a finish product of the cementing material. The cementing material for the colored pavement has the advantages of high temperature-sensing performance, high temperature deformation resistance and low temperature fission resistance.
Description
[technical field]
The present invention relates to a kind of ground surface material, relate in particular to a kind of cementing material for colored pavement and manufacture method thereof.
[background technology]
Along with further developing of China's economy, the range of application on color asphalt road surface can be increasing, and it promotes the security control of traffic engineering for beautifying the environment, and active effect is arranged.The cardinal principle on color asphalt road surface promptly is to adopt cementing material for colored pavement, makes it have needed color by various adding colors.The mechanical property of cementing material for colored pavement and rheological property are similar with heavy traffic asphaltum to general road, good cementing material for colored pavement should satisfy following many-sided requirement as: temperature-sensitive performance, anti-rut performance, cracking resistance sex change can etc.Provide a kind of use properties good cementing material for colored pavement,, improve result of use to increase the service life, social just required.
[summary of the invention]
The object of the present invention is to provide a kind of cementing material for colored pavement and manufacture method thereof with better temperature-sensitive performance, high temperature deformation resistance performance, anti-low temperature fission performance.
For achieving the above object, the present invention adopts following technical scheme:
A kind of cementing material for colored pavement comprises that following component and weight part thereof are:
30～60 parts of heavy mineral oils;
30～50 parts of petroleum resin C5 and/or C9;
3～7 parts of styrene butadiene rubber sbrs;
3～6 parts of thermoplastic elastomer SBSs;
2～7 parts of polyolefin PE, PP and/or polystyrene PS.
As a kind of improvement of the present invention, described cementing material for colored pavement comprises that also weight part is 1～3 part antiaging agent, thermo-stabilizer and a ultra-violet stabilizer.
As a preferred embodiment of the present invention, described petroleum resin C5 accounts for 60～100% of petroleum resin gross weight.
As another kind of preferred version of the present invention, described petroleum resin C9 accounts for 28～100% of petroleum resin gross weight.
A kind of manufacture method that realizes cementing material for colored pavement of the present invention may further comprise the steps:
1) toward the interior heavy mineral oil that adds setting weight part of reactor, C5 and/or C9, SBR, SBS, PE, PP and/or PS, and intensification mixes;
2) use shears that the material that adds is sheared;
3) discharge the bubble that produces by stirring, make the finished product agglutinate.
As a kind of improvement of manufacture method of the present invention, its step also comprises: the antiaging agent, thermo-stabilizer and the ultra-violet stabilizer that add setting weight part in the reactor in step 1).
As a kind of preferred version of manufacture method of the present invention, its concrete steps are:
1) adds described heavy mineral oil during for normal temperature at reactor, add described petroleum resin C5 and/or C9 when spending being warming up to 150, be warming up to 150 once more and add described styrene butadiene rubber sbr when spending, the thermoplastic elastomer SBS, polyolefin PE, PP and/or polystyrene PS, be warming up to 180 and add described antiaging agent, thermo-stabilizer and ultra-violet stabilizer when spending, low whipping speed is under 100～120r/min condition above-mentioned material to be mixed;
2) using shears is that 3000～4500r/min, temperature are under the condition of 160～220 degree in velocity of shear, and the material that above-mentioned steps adds was sheared 2～3 hours, and insulation reaction is 3～6 hours afterwards.
3) utilize high pressure vacuum to discharge the bubble that produces by stirring, make the finished product agglutinate;
4) be cooled to 130 when spending at reactor, described finished product agglutinate is taken out in reactor.
Cementing material for colored pavement of the present invention is to utilize styrene butadiene rubber sbr and thermoplastic elastomer SBS's (styrene-butadiene-styrene multipolymer) at high temperature by the high-speed shearing machine effect, dual modified is dispersion medium with the heavy mineral oil, petroleum resin C5 or C9, additives for plastics (polyolefin PE, PP, polystyrene PS) etc. are the colloid of disperse phase, reach the every physicals that improves agglutinate, mix the technical requirements of heat shop cementing material for colored pavement with heat to satisfy bicycle lane or car lane.
Colloidal particle makes modifier molecules chain spacing increase after entering the properties-correcting agent grid, had both played plastification the mechanical property of properties-correcting agent is improved, and makes properties-correcting agent owing to absorbed colloidal particle and swelling again.Surface at macromolecule modifier forms surface absorbed layer easily, and according to the similar compatibility principle, properties-correcting agent that makes and colloidal particle can form good transition combination, thereby reach better compatibility.Properties-correcting agent has absorbed the part colloidal particle, makes that the polar compound content in the agglutinate rises relatively, thereby increases Intermolecular Forces, improves force of cohesion.The properties-correcting agent particulate that swelling is later under the effect of high-speed shearing machine, is dispersed in the agglutinate uniformly, makes complementary formation of character of differing materials inlay blend.When low temperature, the polymer substance of inlaying absorbs and has consumed rupture stress, and high molecular deformability has improved the cracking resistance sex change energy of modified adhesive ramming material.At high temperature, the adsorbed pitch adsorption layer of properties-correcting agent particulate and upper layer thereof plays the effect that hinders the agglutinate molecular motion again, has improved high temperature deformation resistance, anti-rut performance.Properties-correcting agent is the stochastic distribution state in the hot glue ramming material, after the agglutinate cooling, because the cross-linking set effect forms the 3 D stereo reticulated structure.Strong interaction between the grid has limited displacement and the colloidal flowability between the agglutinate particle, improve the force of cohesion and the snappiness of agglutinate, distortion, be full of cracks, rut etc. there are good impedance behavior, thereby improve temperature-sensitive performance, high-temperature stability, the anti-low-temperature embrittleness performance of agglutinate.
The heat of using cementing material for colored pavement of the present invention to produce is mixed heat shop chromatic bitumen mixture and is had good water stability, the anti-rut performance of high temperature, crack resistance at low-temperature and anti-fatigue performance.
[embodiment]
The component of cementing material for colored pavement of the present invention and manufacture method step thereof are as follows:
1) mixing of materials: used material umber is a weight part
A) stirring at low speed in the ready reaction still, still, stirring velocity is 100～120r/min, makes the material thorough mixing of adding;
B) in still, add 30～60 parts heavy mineral oil at normal temperatures;
C) be warming up to 150 ℃, add 30～50 parts C5 and/or C9 petroleum resin;
D) be warming up to 150 ℃ again, add 3～7 parts of thermoplastic elastomer styrene butadiene rubber sbrs respectively, styrene-butadiene-styrene multipolymer SBS3～6 parts, 2～7 parts in plastics, plastics are PE, PP and/or PS;
E) can also be warming up to 180 ℃ again, add totally 1～3 part of antiaging agent, thermo-stabilizer and ultra-violet stabilizer;
2) under 160～220 ℃ of temperature, utilize high-speed shearing machine, velocity of shear 3000～4500r/min sheared insulation reaction 3～6 hours 2～3 hours;
3) utilize high pressure vacuum, discharge the bubble that produces by stirring, when equitemperature drops to 130 ℃, the finished product agglutinate is put in still the high temperature resistant packaging vessel.
Embodiment 1
Stirring at low speed in the ready reaction still, still, stirring velocity is 100r/min, makes the material thorough mixing of adding; The heavy mineral oil that in still, adds 550kg at normal temperatures; Be warming up to 150 ℃, add C5, the C9 of 100kg of 250kg; Be warming up to 150 ℃ again, add SBR 40kg, SBS 30kg, PE 30kg; Be warming up to 180 ℃ again, add antiaging agent 10kg, thermo-stabilizer 10kg and ultra-violet stabilizer 10kg; Under 160～220 ℃ of temperature, utilize high-speed shearing machine, velocity of shear 3800r/min sheared insulation reaction 4 hours 3 hours; Utilize high pressure vacuum again, discharge the bubble in the agglutinate, when equitemperature drops to 130 ℃, obtain OP-50 heat and mix heat shop car lane cementing material for colored pavement, every performance index such as table one.
Table one OP-50 heat is mixed heat shop car lane cementing material for colored pavement performance index
Embodiment 2:
Stirring at low speed in the ready reaction still, still, stirring velocity is 100r/min, makes the material thorough mixing of adding; The heavy mineral oil that in still, adds 570kg at normal temperatures; Be warming up to 150 ℃, add C5, the C9 of 130kg of 200kg; Be warming up to 150 ℃ again, add SBR 30kg, SBS 35kg, PE 35kg; Be warming up to 180 ℃ again, add antiaging agent 10kg, thermo-stabilizer 10kg and ultra-violet stabilizer 10kg; Under 160～220 ℃ of temperature, utilize high-speed shearing machine, velocity of shear 4000r/min sheared insulation reaction 4 hours 3 hours; Utilize high pressure vacuum again, discharge the bubble in the agglutinate, when equitemperature drops to 130 ℃, obtain OP-70 heat and mix heat shop bicycle lane cementing material for colored pavement, every performance index such as table two.
Table two OP-70 heat is mixed heat shop bicycle lane cementing material for colored pavement performance index
Embodiment 3:
Stirring at low speed in the ready reaction still, still, stirring velocity is 100r/min, makes the material thorough mixing of adding; The heavy mineral oil that in still, adds 600kg at normal temperatures; Be warming up to 150 ℃, add C5, the C9 of 100kg of 200kg; Be warming up to 150 ℃ again, add SBR 40kg, SBS 40kg, PE 20kg; Be warming up to 180 ℃ again, add antiaging agent 10kg, thermo-stabilizer 10kg and ultra-violet stabilizer 10kg; Under 160～220 ℃ of temperature, utilize high-speed shearing machine, velocity of shear 4200r/min sheared insulation reaction 4 hours 3 hours; Utilize high pressure vacuum again, discharge the bubble in the agglutinate, when equitemperature drops to 130 ℃, obtain OP-90 heat and mix heat shop car lane cementing material for colored pavement, every performance index such as table three.
Table three OP-90 heat is mixed heat shop car lane cementing material for colored pavement performance index
The above is preferred embodiment of the present invention, is not limited to the present invention, all modifications of being made in the present invention spirit and principle, is equal to replacement or improvement etc., all should be included in the scope that the present invention protects.
Claims (7)
1. a cementing material for colored pavement is characterized in that, comprises that following component and weight part thereof are:
30～60 parts of heavy mineral oils;
30～50 parts of petroleum resin C5 and/or C9;
3～7 parts of styrene butadiene rubber sbrs;
3～6 parts of thermoplastic elastomer SBSs;
2～7 parts of polyolefin PE, PP and/or polystyrene PS.
2. agglutinate according to claim 1 is characterized in that: also comprise 1～3 part antiaging agent, thermo-stabilizer and ultra-violet stabilizer.
3. agglutinate according to claim 1 and 2 is characterized in that: described petroleum resin C5 accounts for 60～100% of petroleum resin gross weight.
4. agglutinate according to claim 1 and 2 is characterized in that: described petroleum resin C9 accounts for 28～100% of petroleum resin gross weight.
5. the manufacture method of the arbitrary described cementing material for colored pavement of claim 1 to 4 is characterized in that, may further comprise the steps:
1) toward the interior heavy mineral oil that adds setting weight part of reactor, C5 and/or C9, SBR, SBS, PE, PP and/or PS, and intensification mixes;
2) use shears that the material that adds is sheared;
3) discharge the bubble that produces by stirring, make the finished product agglutinate.
6. manufacture method according to claim 5 is characterized in that: add antiaging agent, thermo-stabilizer and the ultra-violet stabilizer of setting weight part in the reactor in step 1), and heat up and mix.
7. manufacture method according to claim 6 is characterized in that, its concrete steps are:
1) adds described heavy mineral oil during for normal temperature at reactor, add described C5 and/or C9 petroleum resin when spending being warming up to 150, be warming up to 150 once more and add described SBR when spending, SBS, PE, PP and/or PS, be warming up to 180 and add described antiaging agent, thermo-stabilizer and ultra-violet stabilizer when spending, low whipping speed is under 100～120r/min condition above-mentioned material to be mixed;
2) using shears is that 3000～4500r/min, temperature are under the condition of 160～220 degree in velocity of shear, and the material that above-mentioned steps adds was sheared 2～3 hours, and insulation reaction is 3～6 hours afterwards;
3) utilize high pressure vacuum to discharge the bubble that produces by stirring, make the finished product agglutinate;
4) be cooled to 130 when spending at reactor, described finished product agglutinate is taken out in reactor.
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| CN200910107456.7A CN101891964B (en) | 2009-05-20 | 2009-05-20 | Cementing material for colored pavement and manufacturing method thereof |
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| CN200910107456.7A CN101891964B (en) | 2009-05-20 | 2009-05-20 | Cementing material for colored pavement and manufacturing method thereof |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102295819A (en) * | 2010-06-24 | 2011-12-28 | 上海启鹏工程材料科技有限公司 | Cementing material for colorful pavement and manufacturing method thereof |
| CN102558751A (en) * | 2011-12-16 | 2012-07-11 | 长安大学 | Colored pavement cementing material and preparation method thereof |
| CN103739237A (en) * | 2013-12-10 | 2014-04-23 | 柳州博泽科技有限公司 | Color asphalt mixture and preparation method thereof |
| CN103881402A (en) * | 2014-03-11 | 2014-06-25 | 吉林省嘉瑞沥青科技有限公司 | Colored asphalt and preparation method thereof |
| CN104017379A (en) * | 2014-06-20 | 2014-09-03 | 重庆市智翔铺道技术工程有限公司 | Modified asphalt and preparation method thereof |
| CN104058631A (en) * | 2014-06-04 | 2014-09-24 | 吴江市明港道桥工程有限公司 | Colorless cementing material and preparation method thereof |
| CN106633606A (en) * | 2016-10-13 | 2017-05-10 | 上海浦东路桥建设股份有限公司 | Colored asphalt cementing material suitable for heavy traffic and preparation method thereof |
| CN108059787A (en) * | 2016-11-09 | 2018-05-22 | 中国石油化工股份有限公司 | A kind of caulking material and preparation method thereof |
| CN108070193A (en) * | 2016-11-09 | 2018-05-25 | 中国石油化工股份有限公司 | It is a kind of for caulking material of Colorful Asphalt Pavement and preparation method thereof |
| CN108250777A (en) * | 2018-01-12 | 2018-07-06 | 黄河三角洲京博化工研究院有限公司 | A kind of color asphalt and preparation method thereof |
| CN108395707A (en) * | 2017-02-07 | 2018-08-14 | 中国石油化工股份有限公司 | A kind of patching material of Colorful Asphalt Pavement and preparation method thereof |
| CN108395708A (en) * | 2017-02-07 | 2018-08-14 | 中国石油化工股份有限公司 | Caulking material of Colorful Asphalt Pavement and preparation method thereof |
| CN108424658A (en) * | 2018-03-30 | 2018-08-21 | 佛山市路邦沥青有限公司 | A kind of preparation method of anti-aging color asphalt |
| CN108530911A (en) * | 2018-03-30 | 2018-09-14 | 佛山市路邦沥青有限公司 | A kind of color asphalt |
| CN108641378A (en) * | 2018-03-30 | 2018-10-12 | 佛山市路邦沥青有限公司 | A kind of anti-aging color asphalt |
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| CN101148512A (en) * | 2006-09-18 | 2008-03-26 | 深圳市海川实业股份有限公司 | Granulation method for cementing material used for color pavement |
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2009
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101148512A (en) * | 2006-09-18 | 2008-03-26 | 深圳市海川实业股份有限公司 | Granulation method for cementing material used for color pavement |
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102295819A (en) * | 2010-06-24 | 2011-12-28 | 上海启鹏工程材料科技有限公司 | Cementing material for colorful pavement and manufacturing method thereof |
| CN102558751A (en) * | 2011-12-16 | 2012-07-11 | 长安大学 | Colored pavement cementing material and preparation method thereof |
| CN102558751B (en) * | 2011-12-16 | 2014-10-08 | 长安大学 | Colored pavement cementing material and preparation method thereof |
| CN103739237A (en) * | 2013-12-10 | 2014-04-23 | 柳州博泽科技有限公司 | Color asphalt mixture and preparation method thereof |
| CN103881402A (en) * | 2014-03-11 | 2014-06-25 | 吉林省嘉瑞沥青科技有限公司 | Colored asphalt and preparation method thereof |
| CN104058631A (en) * | 2014-06-04 | 2014-09-24 | 吴江市明港道桥工程有限公司 | Colorless cementing material and preparation method thereof |
| CN104058631B (en) * | 2014-06-04 | 2016-07-06 | 吴江市明港道桥工程有限公司 | A kind of colourless cementitious matter and preparation method thereof |
| CN104017379A (en) * | 2014-06-20 | 2014-09-03 | 重庆市智翔铺道技术工程有限公司 | Modified asphalt and preparation method thereof |
| CN106633606A (en) * | 2016-10-13 | 2017-05-10 | 上海浦东路桥建设股份有限公司 | Colored asphalt cementing material suitable for heavy traffic and preparation method thereof |
| CN108070193A (en) * | 2016-11-09 | 2018-05-25 | 中国石油化工股份有限公司 | It is a kind of for caulking material of Colorful Asphalt Pavement and preparation method thereof |
| CN108059787A (en) * | 2016-11-09 | 2018-05-22 | 中国石油化工股份有限公司 | A kind of caulking material and preparation method thereof |
| CN108070193B (en) * | 2016-11-09 | 2020-02-14 | 中国石油化工股份有限公司 | Caulking material for colored asphalt pavement and preparation method thereof |
| CN108059787B (en) * | 2016-11-09 | 2020-05-19 | 中国石油化工股份有限公司 | Caulking material and preparation method thereof |
| CN108395707A (en) * | 2017-02-07 | 2018-08-14 | 中国石油化工股份有限公司 | A kind of patching material of Colorful Asphalt Pavement and preparation method thereof |
| CN108395708A (en) * | 2017-02-07 | 2018-08-14 | 中国石油化工股份有限公司 | Caulking material of Colorful Asphalt Pavement and preparation method thereof |
| CN108395707B (en) * | 2017-02-07 | 2019-10-11 | 中国石油化工股份有限公司 | A kind of patching material of Colorful Asphalt Pavement and preparation method thereof |
| CN108250777A (en) * | 2018-01-12 | 2018-07-06 | 黄河三角洲京博化工研究院有限公司 | A kind of color asphalt and preparation method thereof |
| CN108424658A (en) * | 2018-03-30 | 2018-08-21 | 佛山市路邦沥青有限公司 | A kind of preparation method of anti-aging color asphalt |
| CN108530911A (en) * | 2018-03-30 | 2018-09-14 | 佛山市路邦沥青有限公司 | A kind of color asphalt |
| CN108641378A (en) * | 2018-03-30 | 2018-10-12 | 佛山市路邦沥青有限公司 | A kind of anti-aging color asphalt |
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Address after: 201209 No. 158 Chuansha Road, Caolu Town Industrial Zone, Pudong New Area, Shanghai Patentee after: SHANGHAI KNP MATERIAL TECHNOLOGY Co.,Ltd. Patentee after: SHENZHEN OCEANPOWER INDUSTRY Co.,Ltd. Patentee after: SHENZHEN OCEAN POWER ENGINEERING TECHNOLOGY Co.,Ltd. Patentee after: GUANGDONG OCEANPOWER TECHNOLOGY Co.,Ltd. Address before: 201209 No. 158, Chuansha Road, Shanghai, Pudong New Area Patentee before: Shanghai Qipeng Chemical Co.,Ltd. Patentee before: SHENZHEN OCEANPOWER INDUSTRY Co.,Ltd. Patentee before: SHENZHEN OCEAN POWER ENGINEERING TECHNOLOGY Co.,Ltd. Patentee before: HEYUAN OCEAN POWER TECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20220729 Address after: 518054 Room 201, building a, No. 1, Qianhai 1st Road, Qianhai Shenzhen Hong Kong cooperation zone, Shenzhen, Guangdong Province Patentee after: Shenzhen Qianhai Haichuan New Material Technology Co.,Ltd. Address before: 201209 No. 158 Chuansha Road, Caolu Town Industrial Zone, Pudong New Area, Shanghai Patentee before: SHANGHAI KNP MATERIAL TECHNOLOGY Co.,Ltd. Patentee before: SHENZHEN OCEANPOWER INDUSTRY Co.,Ltd. Patentee before: SHENZHEN OCEAN POWER ENGINEERING TECHNOLOGY Co.,Ltd. Patentee before: GUANGDONG OCEANPOWER TECHNOLOGY Co.,Ltd. |