CN101831535B - Heat treatment method after forging of ultra-supercritical high and medium pressure rotor steel - Google Patents

Heat treatment method after forging of ultra-supercritical high and medium pressure rotor steel Download PDF

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CN101831535B
CN101831535B CN 200910056943 CN200910056943A CN101831535B CN 101831535 B CN101831535 B CN 101831535B CN 200910056943 CN200910056943 CN 200910056943 CN 200910056943 A CN200910056943 A CN 200910056943A CN 101831535 B CN101831535 B CN 101831535B
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forging
heat treatment
stove
treatment method
rotor steel
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CN101831535A (en
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胡朝备
潘胜
谢培德
宋雷钧
马明方
吕政�
陆寅松
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Shanghai Electric Heavy Forging Co. Ltd.
Shanghai Heavy Machinery Plant Co Ltd
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Abstract

The invention discloses a heat treatment method after forging of ultra-supercritical high and medium pressure rotor steel. The heat treatment after forging of ultra-supercritical high and medium pressure unit rotor steel X12CrMoWVNbN10-1-1 and Cr10.5Mo1W1NiVNbN is carried out by the steps of: step 1. austenite homogenization treatment; step 2. carrying out structural transformation when balanced structure transformation temperature is reached by air cooling; step 3. overall structure softening; and step 4. cooling in a speed limit furnace till discharging. Since the rotor steel is directly put into the furnace for austenization after being forged, the invention has the advantages of short time and good austenite effect, not only eliminates the forging stress, but realizes the homogenization of inner and outer structures of forging. The heat treatment method after forging has the advantages of simple operation, low cost and low energy consumption, and can meet the property requirement of workpieces.

Description

The heat treatment method after forging of ultra supercritical high pressure rotor steel
Technical field
The present invention relates to a kind of thermal treatment process, be specifically related to a kind of heat treatment method after forging of ultra supercritical high pressure rotor steel.
Background technology
For large section, large-tonnage ultra supercritical high pressure rotor steel, traditional forging post-heat-treated technology, as shown in Figure 1; When being air cooling to 680 after forging~780 ℃, the 690 ℃ of stoves to be expected of packing into, then 690 ℃ down insulation carried out structural transformation in 200 hours; Be chilled to 240 ℃ with≤8 ℃/h stove again; Insulation fully changes, and being raised to 720 ℃ of insulations again, to carry out organized whole after 22 hours softening, and last stove is cold to be chilled to 180 ℃ with≤8 ℃/h stove and to accomplish and forge post-heat-treated.
Forging by above art breading can be guaranteed the machining cutting ability, but its crystal grain is thick, and the flaw detection reduction coefficient does not reach the flaw detection requirement, and inside appears netted or rolls into a ball cotton-shaped " type troostite " tissue, influences the workpiece performance.Research shows that this is owing to do not carry out processing of austenite homogenizing and directly cooling back isothermal transformation after forging, and organizes grain fineness number uneven thereby cause to cause, and inside and outside composition difference is big, and mixed crystal phenomenon is serious.Therefore, the workpiece that adopts this art breading to come out is difficult to through detecting.
Summary of the invention
Technical problem to be solved by this invention provides a kind of heat treatment method after forging of ultra supercritical high pressure rotor steel, and it can make the inside and outside tissue of forging reach homogenizing.
For solving the problems of the technologies described above, the technical solution of the heat treatment method after forging of ultra supercritical high pressure rotor steel of the present invention is:
Adopt following method that X12CrMoWVNbN10-1-1 and Cr10.5Mo1W1NiVNbN ultra supercritical unit high pressure rotor steel are forged post-heat-treated:
The first step, austenite homogenizing are handled: after the completion of forging finish-forging, it is 950 ± 10 ℃ stove to be expected that forging is directly put into temperature, rises to 1050 ± 10 ℃ of insulations with the heat-up rate of≤50 ℃/h, and soaking time is 0.5~1h/100mm.
In second step, air cooling to balanced weave transition temperature carries out structural transformation: 580~620 ℃ of air cooling to forging surface temperatures, after advance stove immediately, Control for Kiln Temperature is at 690 ± 10 ℃, soaking time is 15h/100mm, carries out balanced weave and changes; Be chilled to 240 ℃ ± 10 ℃ insulations with≤8 ℃/h speed limit stove again, soaking time is 2h/100mm, remains tissue and fully changes.
In the 3rd step, organized whole is softening; Speed with≤15 ℃/h rises to 720 ± 10 ℃, and it is softening that insulation 2h/100mm carries out organized whole.
In the 4th step, the speed limit stove is chilled to comes out of the stove.Be chilled to≤180 ℃ of completion forging post-heat-treated of coming out of the stove with≤8 ℃/h speed limit stove.
The technique effect that the present invention can reach is:
The present invention carries out austenitizing through directly advancing stove after forging, and the time is short, and austenitizing is effective, has not only eliminated forging stress, and makes the inside and outside tissue of forging reach homogenizing.
The present invention is simple to operate, and cost reduces, and energy consumption is few, can satisfy the performance of workpiece requirement.
Description of drawings
Below in conjunction with accompanying drawing and embodiment the present invention is done further detailed explanation:
Fig. 1 is the heat treatment method after forging of prior art ultra supercritical high pressure rotor steel;
Fig. 2 is the heat treatment method after forging of ultra supercritical high pressure rotor steel of the present invention.
Embodiment
As shown in Figure 2, the heat treatment method after forging of ultra supercritical high pressure rotor steel of the present invention, adopt following method that X12CrMoWVNbN10-1-1 and Cr10.5Mo1W1NiVNbN ultra supercritical unit high pressure rotor steel are forged post-heat-treated:
The first step, the austenite homogenizing is handled: forging finish-forging completion back (this moment, the forging temperature was about 900 ℃, about 1000 ℃ of heart portion temperature); Do not carry out air cooling; It is 950 ± 10 ℃ stove to be expected that forging is directly put into temperature, rises to 1050 ± 10 ℃ of insulations with the heat-up rate of≤50 ℃/h, and soaking time is that 0.5~1h/100mm (promptly is the forging insulation 0.5~1 hour of 100mm for diameter; Then be the forging insulation 6~12 hours of 1200mm) for diameter; Carry out the austenite structure homogenizing and handle, eliminate forging stress, adjustment grain fineness number and homogeneous austenite structure are to obtain good matrix;
In second step, air cooling to balanced weave transition temperature carries out structural transformation: 580~620 ℃ of air cooling to forging surface temperatures, after advance stove immediately, Control for Kiln Temperature is at 690 ± 10 ℃, soaking time is 15h/100mm, carries out balanced weave and changes; Be chilled to 240 ℃ ± 10 ℃ insulations with≤8 ℃/h speed limit stove again, soaking time is 2h/100mm, remains tissue and fully changes.
In the 3rd step, organized whole is softening: after insulation finishes, rise to 720 ± 10 ℃ with the speed of≤15 ℃/h, it is softening that insulation 2h/100mm carries out organized whole;
In the 4th step, the speed limit stove is chilled to comes out of the stove: be chilled to≤180 ℃ of completion forging post-heat-treated of coming out of the stove with≤8 ℃/h speed limit stove.
Because being incubated about 12 hours crystal grain down 1040 ℃ of material temperature, this steel grade can not aggravate to grow up; The present invention takes all factors into consideration the furnace temperature and the warm temperature difference of material; And factors such as the cross section of forging, final forging temperature, confirm that finally furnace temperature is 1050 ± 10 ℃, soaking time is 0.5~1h/100mm.
The present invention has abandoned and has forged the cold traditional technology method of laggard line space, but the forging after the finish-forging completion is directly put into 950 ± 10 ℃ high temperature stove to be expected, it is warming up to 1050 ± 10 ℃; Made full use of waste heat after the forging of forging, not only can save energy, and can reach holding temperature in the short period of time; Make internal and external temperature reach consistent, thereby eliminated forging stress, make recrystallize abundant; The insulation short period after the intensification can obtain austenite structure uniformly; Adjusted grain fineness number, had laid a good foundation, made the first thermal treatment UT detect qualification rate and improve for the acquisition of follow-up balanced weave; Can satisfy the flaw detection requirement, prepare for later property heat treatment performs tissue.

Claims (4)

1. the heat treatment method after forging of a ultra supercritical high pressure rotor steel is characterized in that, adopts following method that X12CrMoWVNbN10-1-1 and Cr10.5Mo1W1NiVNbN ultra supercritical unit high pressure rotor steel are forged post-heat-treated:
The first step, the austenite homogenizing is handled; The austenite homogenising treatment method of the said the first step is, after the completion of forging finish-forging, it is 950 ± 10 ℃ stove to be expected that forging is directly put into temperature, rises to 1050 ± 10 ℃ of insulations with the heat-up rate of≤50 ℃/h, and soaking time is 0.5~1h/100mm;
In second step, air cooling to balanced weave transition temperature carries out structural transformation;
In the 3rd step, organized whole is softening;
In the 4th step, the speed limit stove is chilled to comes out of the stove.
2. the heat treatment method after forging of ultra supercritical high pressure rotor steel according to claim 1; It is characterized in that: the method in said second step is; 580~620 ℃ of air cooling to forging surface temperatures, after advance stove immediately, Control for Kiln Temperature is at 690 ± 10 ℃; Soaking time is 15h/100mm, carries out balanced weave and changes; Be chilled to 240 ℃ ± 10 ℃ insulations with≤8 ℃/h speed limit stove again, soaking time is 2h/100mm, remains tissue and fully changes.
3. the heat treatment method after forging of ultra supercritical high pressure rotor steel according to claim 1 is characterized in that: the method in said the 3rd step is, rises to 720 ± 10 ℃ with the speed of≤15 ℃/h, and it is softening that insulation 2h/100mm carries out organized whole.
4. the heat treatment method after forging of ultra supercritical high pressure rotor steel according to claim 1 is characterized in that: the method in said the 4th step is to be chilled to≤180 ℃ of completion forging post-heat-treated of coming out of the stove with≤8 ℃/h speed limit stove.
CN 200910056943 2009-03-12 2009-03-12 Heat treatment method after forging of ultra-supercritical high and medium pressure rotor steel Active CN101831535B (en)

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Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103088199B (en) * 2011-11-04 2014-12-24 上海重型机器厂有限公司 Heat treatment method after forging for forged steel bearing roller used for large heavy plate mill
CN103131964B (en) * 2013-03-26 2014-11-12 上海交通大学 Method for improving as-cast structure homogeneity of X12CrMoWVNbN10-1-1 martensitic stainless steel
CN103667624B (en) * 2013-08-27 2015-09-30 内蒙古北方重工业集团有限公司 High temperature blade steel 1Cr12Ni3Mo2VN step type cooling method for annealing
CN107400761B (en) * 2016-05-20 2019-02-12 上海电气上重铸锻有限公司 The heat treatment method of advanced ultra supercritical rotor forging
CN106119486A (en) * 2016-08-30 2016-11-16 四川六合锻造股份有限公司 A kind of heat treatment method after forging of ultra-supercritical turbine blade steel
CN106929653B (en) * 2017-03-01 2019-05-07 上海电气上重铸锻有限公司 A kind of 25Cr2Ni2MoV rotor made of steel forging heat treatment method after forging
CN107598067B (en) * 2017-09-18 2019-02-12 无锡宏达重工股份有限公司 A kind of processing technology of X12CrMoWVNbN10 stator blade ring forging

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CN101323901A (en) * 2007-06-12 2008-12-17 上海重型机器锻件厂 Austenitic stainless steel as-forged solid solution treatment process after forging

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