CN101787214A - Edible membrane by taking proanthocyanidins crosslinked with collagen as matrix and preparation method thereof - Google Patents
Edible membrane by taking proanthocyanidins crosslinked with collagen as matrix and preparation method thereof Download PDFInfo
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- CN101787214A CN101787214A CN201010119040A CN201010119040A CN101787214A CN 101787214 A CN101787214 A CN 101787214A CN 201010119040 A CN201010119040 A CN 201010119040A CN 201010119040 A CN201010119040 A CN 201010119040A CN 101787214 A CN101787214 A CN 101787214A
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- collagen
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- 102000008186 Collagen Human genes 0.000 title claims abstract description 30
- 108010035532 Collagen Proteins 0.000 title claims abstract description 30
- 229920001436 collagen Polymers 0.000 title claims abstract description 29
- 229920002770 condensed tannin Polymers 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000011159 matrix material Substances 0.000 title claims abstract description 8
- 239000012528 membrane Substances 0.000 title abstract description 10
- 239000000243 solution Substances 0.000 claims abstract description 13
- 235000013305 food Nutrition 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 7
- 238000012856 packing Methods 0.000 claims abstract description 6
- 239000003814 drug Substances 0.000 claims abstract description 5
- 235000018192 pine bark supplement Nutrition 0.000 claims description 18
- 239000007864 aqueous solution Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 14
- 238000007605 air drying Methods 0.000 claims description 5
- 150000002632 lipids Chemical class 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 6
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 239000004519 grease Substances 0.000 abstract 2
- 230000003115 biocidal effect Effects 0.000 abstract 1
- 235000013410 fast food Nutrition 0.000 abstract 1
- 235000013611 frozen food Nutrition 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 230000004888 barrier function Effects 0.000 description 7
- 231100000252 nontoxic Toxicity 0.000 description 6
- 230000003000 nontoxic effect Effects 0.000 description 6
- 230000003064 anti-oxidating effect Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 102000004169 proteins and genes Human genes 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 239000005357 flat glass Substances 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 239000004540 pour-on Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000009447 edible packaging Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229920006280 packaging film Polymers 0.000 description 2
- 239000012785 packaging film Substances 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 2
- 210000001519 tissue Anatomy 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 101710172711 Structural protein Proteins 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000012675 alcoholic extract Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000009881 electrostatic interaction Effects 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 210000000474 heel Anatomy 0.000 description 1
- 210000003041 ligament Anatomy 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Abstract
The invention discloses an edible membrane by taking proanthocyanidins crosslinked with collagen as matrix and a preparation method thereof. In the method, firstly, proanthocyanidins water solution with the mass concentration of (0.1-0.5) per mill and collagen water solution with the mass concentration of (1-5) per mill are prepared respectively; then, the proanthocyanidins water solution and the collagen water solution are mixed according to the dry weight ratio of 1:50-4:50 in the stirring state; next, the mixed solution is stirred evenly to form membrane solution; and finally, membrane making is carried out to obtain the edible membrane. The edible membrane prepared in the method has good grease oxidization resistance, antibiotic property and separation property, simple preparation method and easy operation. In addition, the edible membrane has wide application scope, can be applied for inner packing of the grease food, the frozen food, the medicine electuary and the convenience food and has greater application and promotion value.
Description
Technical field
The present invention relates to a kind of edible membrane material and preparation method thereof, have good anti-Oxidation of Fat and Oils, germ resistance, barrier in particular to a kind of, and safety non-toxic is biodegradable, can be used in edible film of food internal packing and preparation method thereof.
Background technology
Edible packaging film is mainly used in food fresh-keeping in transportation, storage and shelf storage process, need mould material in the biodegradable while of safety non-toxic, also have good gas-barrier properties, fragrance protectiveness, the vapour perviousness that blocks water, dubbin perviousness, stability and a mechanical property preferably.
Protein has the characteristics of originate abundant, biodegradable and safety non-toxic, is widely used in edible packaging film as the film forming substrate.Collagen is a kind of natural protein, extensively is present in skin, bone, muscle, heel string, ligament and the blood vessel of animal, and be structural protein important in reticular tissue, the cartilaginous tissue.The molecular weight of collagen is big, and solvability is little, has good film-forming properties.And the triple helix structure that collagen is natural and self be fibrous texture closely, makes collagenic material demonstrate very strong toughness and intensity, is applicable to the preparation mould material.
The barrier property of simple collagen film and mechanical property are all limited.Force of cohesion increase between the protein peptide chain is the important factor that improves the film barrier property, can come the stable of induced protein by the formation of hydrogen bond, electrostatic interaction and covalent linkage.In the research often by proteinic chemically crosslinked, enzyme is crosslinked or physical treatment improves its barrier property and mechanical property.Pycnogenols is a kind of plant polyphenol that is widespread in nature, and has stronger antibacterial, anti-oxidant and capability of resistance to radiation, is mainly used in food, beverage, healthcare products and cosmetic field.Contain more phenolic hydroxyl group, alcoholic extract hydroxyl group and ether in the pycnogenols molecule, easily with collagen on hydroxyl, amino and carboxyl form hydrogen bond, thereby produce crosslinked, the barrier property and the mechanical property of raising collagem membrane.Therefore, pycnogenols is a kind of collagen crosslinking agent of effective safety non-toxic.
At present, there have been some patents that collagen base edible film is disclosed.Disclose a kind of edible film and production method thereof that contains collagen of fish skin as CN101341977.Patents such as CN1547434, CN1154797, CN1337179, CN1228922 are to being that the method that main raw material is made casing discloses with collagen.CN1723803 discloses a kind of natural membrane forming preservation agent used for crystal-like delicious meat that contains tea-polyphenol and collagen protein, but just a kind of additive of tea-polyphenol as preservation agent used, do not use, and what wherein adopt is not the collagen that the triple helix structure remains intact as main component.The mechanical property of these edible films, swelling behavior, barrier property and anti-Oxidation of Fat and Oils ability are still waiting to improve, and are that the edible film of matrix does not also have document and patent report with the taking proanthocyanidins crosslinked with collagen with good resistance of oxidation.
The invention provides a kind of taking proanthocyanidins crosslinked with collagen is edible film of matrix and preparation method thereof.This edible film is the biodegradable natural fresh-keeping film of a kind of safety non-toxic, have good anti-Oxidation of Fat and Oils, germ resistance and barrier property, and the preparation method is simple, and profit margin is big.In addition, this edible film use range is wider, can be applied to the internal packing of lipid food, frozen product, medicine instant and ready-to-eat, has good market application prospect.
Summary of the invention
The object of the present invention is to provide a kind of taking proanthocyanidins crosslinked with collagen is edible film of matrix and preparation method thereof, consumable film is reached have the effect of bacteriostasis, anti-Oxidation of Fat and Oils ability by add pycnogenols in collagen.
For reaching above purpose, the present invention is by the following technical solutions: prepare mass concentration at first respectively and be the pycnogenols aqueous solution of (0.1-0.5) ‰ and the mass concentration collagenic aqueous solution for (1-5) ‰, under whipped state pycnogenols and collagen solution are pressed dry weight than 1 then: 50-4: 50 mix, stir and form film forming liquid, and after the system film obtain.Above described film-forming method for film forming liquid pour into the system film die in, natural air drying or in 20-35 ℃ of baking oven the oven dry after take off film.
Edible film of the present invention can be applied to the internal packing of lipid food, frozen product, medicine instant and ready-to-eat.
Compare with existing edible film, adopt the material of the present invention's preparation to have the following advantages:
(1) it is little that the collagen that remains intact for the triple helix structure of the raw material that adopts of the present invention, the edible film of preparation have a swelling ratio, the characteristics that water preventing ability is good;
(2) edible film of the present invention's preparation has good anti-Oxidation of Fat and Oils and germ resistance, is the biodegradable natural fresh-keeping film of a kind of safety non-toxic;
(3) the edible film use range of the present invention's preparation is extensive, can be applied to the internal packing of lipid food, frozen product, medicine instant and ready-to-eat;
(4) preparation method of edible film disclosed by the invention, easy handling, with short production cycle, have bigger application and popularization value.
Embodiment
Providing 5 embodiment of the present invention below, is edible film of matrix and preparation method thereof to specify a kind of taking proanthocyanidins crosslinked with collagen.
Embodiment 1
Prepare mass concentration respectively and be 0.1 ‰ the pycnogenols aqueous solution and mass concentration and be 5 ‰ collagenic aqueous solution, under whipped state, pycnogenols and collagen solution are mixed than 1: 50 by dry weight then, stir and form film forming liquid, then get 40mL film forming liquid and pour in the tetrafluoroethylene mould that diameter is 10cm, put into 30 ℃ of dry 36h of baking oven and get final product film forming.
Embodiment 2
Prepare mass concentration respectively and be 0.2 ‰ the pycnogenols aqueous solution and mass concentration and be 5 ‰ collagenic aqueous solution, under whipped state, pycnogenols and collagen solution are mixed than 2: 50 by dry weight then, stir and form film forming liquid, then get 40mL film forming liquid and pour in the tetrafluoroethylene mould that diameter is 10cm, put into 30 ℃ of dry 36h of baking oven and get final product film forming.
Embodiment 3
Prepare mass concentration respectively and be 0.2 ‰ the pycnogenols aqueous solution and mass concentration and be 3 ‰ collagenic aqueous solution, under whipped state, pycnogenols and collagen solution are mixed than 1: 50 by dry weight then, stir and form film forming liquid, then get 40mL film forming liquid and pour on the sheet glass of 50cm * 50cm the natural air drying film forming into.
Embodiment 4
Prepare mass concentration respectively and be 0.4 ‰ the pycnogenols aqueous solution and mass concentration and be 4 ‰ collagenic aqueous solution, under whipped state, pycnogenols and collagen solution are mixed than 4: 50 by dry weight then, stir and form film forming liquid, then get 40mL film forming liquid and pour on the sheet glass of 50cm * 50cm the natural air drying film forming into.。
Embodiment 5
Prepare mass concentration respectively and be 0.2 ‰ the pycnogenols aqueous solution and mass concentration and be 2 ‰ collagenic aqueous solution, under whipped state, pycnogenols and collagen solution are mixed than 1: 50 by dry weight then, stir and form film forming liquid, then get 40mL film forming liquid and pour on the sheet glass of 50cm * 50cm the natural air drying film forming into.
Claims (3)
1. taking proanthocyanidins crosslinked with collagen edible film that is matrix and preparation method thereof, it is characterized in that the preparation method is as follows: preparing the pycnogenols aqueous solution and the mass concentration that mass concentration is (0.1-0.5) ‰ at first respectively is the collagenic aqueous solution of (1-5) ‰, under whipped state pycnogenols and collagen solution are pressed dry weight than 1 then: 50-4: 50 mix, stir and form film forming liquid, and after the system film obtain.
2. method according to claim 1 is characterized in that described film-forming method is that film forming liquid is poured in the system film die, takes off film after the oven dry in natural air drying or the 20-35 ℃ baking oven.
3. according to claim 1, it is characterized in that this edible film can be applied to the internal packing of lipid food, frozen product, medicine instant and ready-to-eat.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010119040XA CN101787214B (en) | 2010-03-08 | 2010-03-08 | Edible membrane by taking proanthocyanidins crosslinked with collagen as matrix and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010119040XA CN101787214B (en) | 2010-03-08 | 2010-03-08 | Edible membrane by taking proanthocyanidins crosslinked with collagen as matrix and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101787214A true CN101787214A (en) | 2010-07-28 |
| CN101787214B CN101787214B (en) | 2012-04-25 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010119040XA Active CN101787214B (en) | 2010-03-08 | 2010-03-08 | Edible membrane by taking proanthocyanidins crosslinked with collagen as matrix and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN101787214B (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102250368A (en) * | 2011-05-19 | 2011-11-23 | 四川大学 | Edible collagen-based food packaging film and preparation method thereof |
| CN102633054A (en) * | 2012-04-23 | 2012-08-15 | 福州大学 | Antioxidation collagen active membrane containing plant extract and preparation method for antioxidation collagen active membrane |
| CN104558642A (en) * | 2014-12-31 | 2015-04-29 | 中国海洋大学 | Plant extract and method for cross-linking collagen by using plant extract as biological cross-linker |
| CN105288734A (en) * | 2015-11-23 | 2016-02-03 | 四川大学 | Composite crosslinked type I collagen membrane and preparation method thereof |
| WO2017158041A1 (en) * | 2016-03-18 | 2017-09-21 | Indena S.P.A. | Compositions useful in the prevention and/or treatment of disorders of the oral cavity, upper airways and esophagus |
| CN111700205A (en) * | 2020-06-16 | 2020-09-25 | 绥化学院 | Method for preparing hyaluronic acid cyclodextrin embedded collagen-anthocyanin pH indicating gel |
| CN113150561A (en) * | 2021-04-06 | 2021-07-23 | 暨南大学 | Collagen-based biological ink for 3D biological printing and preparation method and application thereof |
| CN113197242A (en) * | 2020-09-23 | 2021-08-03 | 四川大学 | Continuous water bath fixing treatment process for preparing collagen casing by wet method |
| CN115197453A (en) * | 2022-07-01 | 2022-10-18 | 陕西科技大学 | Intelligent slow-release active packaging film and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1760247A (en) * | 2005-09-30 | 2006-04-19 | 四川师范大学 | Food wrap film of collagen and preparation method |
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2010
- 2010-03-08 CN CN201010119040XA patent/CN101787214B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1760247A (en) * | 2005-09-30 | 2006-04-19 | 四川师范大学 | Food wrap film of collagen and preparation method |
Non-Patent Citations (2)
| Title |
|---|
| 《眼科新进展》 20070430 林旭明等 原花青素交联的支架材料的生物相容性研究 第262-265页 1-3 第27卷, 第4期 2 * |
| 《贵州农业科学》 20031231 罗爱平等 可食性胶原蛋白成膜技术初探 第44-46页 1-3 第31卷, 第4期 2 * |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102250368A (en) * | 2011-05-19 | 2011-11-23 | 四川大学 | Edible collagen-based food packaging film and preparation method thereof |
| CN102633054A (en) * | 2012-04-23 | 2012-08-15 | 福州大学 | Antioxidation collagen active membrane containing plant extract and preparation method for antioxidation collagen active membrane |
| CN104558642A (en) * | 2014-12-31 | 2015-04-29 | 中国海洋大学 | Plant extract and method for cross-linking collagen by using plant extract as biological cross-linker |
| CN104558642B (en) * | 2014-12-31 | 2017-12-29 | 中国海洋大学 | One Plant Extracts and its method as Biological cross-linker cross-linked collagen |
| CN105288734A (en) * | 2015-11-23 | 2016-02-03 | 四川大学 | Composite crosslinked type I collagen membrane and preparation method thereof |
| WO2017158041A1 (en) * | 2016-03-18 | 2017-09-21 | Indena S.P.A. | Compositions useful in the prevention and/or treatment of disorders of the oral cavity, upper airways and esophagus |
| CN111700205A (en) * | 2020-06-16 | 2020-09-25 | 绥化学院 | Method for preparing hyaluronic acid cyclodextrin embedded collagen-anthocyanin pH indicating gel |
| CN111700205B (en) * | 2020-06-16 | 2022-11-25 | 绥化学院 | Method for preparing hyaluronic acid cyclodextrin embedded collagen-anthocyanin pH indicating gel |
| CN113197242A (en) * | 2020-09-23 | 2021-08-03 | 四川大学 | Continuous water bath fixing treatment process for preparing collagen casing by wet method |
| CN113150561A (en) * | 2021-04-06 | 2021-07-23 | 暨南大学 | Collagen-based biological ink for 3D biological printing and preparation method and application thereof |
| CN115197453A (en) * | 2022-07-01 | 2022-10-18 | 陕西科技大学 | Intelligent slow-release active packaging film and preparation method and application thereof |
| CN115197453B (en) * | 2022-07-01 | 2023-05-16 | 陕西科技大学 | Intelligent slow-release type active packaging film and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101787214B (en) | 2012-04-25 |
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