CN101706380A - Three-way sampling head device and using method thereof - Google Patents

Three-way sampling head device and using method thereof Download PDF

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Publication number
CN101706380A
CN101706380A CN200910199067A CN200910199067A CN101706380A CN 101706380 A CN101706380 A CN 101706380A CN 200910199067 A CN200910199067 A CN 200910199067A CN 200910199067 A CN200910199067 A CN 200910199067A CN 101706380 A CN101706380 A CN 101706380A
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sampling
port structure
sampling pipe
gas
head device
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CN200910199067A
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CN101706380B (en
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傅亚铁
张建杰
陆晓祖
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Shanghai Gaoqiao Sgpec Petrochemical Engineering & Construction Co Ltd
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Shanghai Gaoqiao Sgpec Petrochemical Engineering & Construction Co Ltd
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Abstract

The invention relates to a sampling head device, which comprises a three-way structure, a sample collection tube sleeved in the three-way structure, a waste gas collection tube sleeved outside the sample collection tube and a waste gas recovery tube arranged in the three-way structure, wherein one end of the sample collection tube extends to a pipeline of a sample to be collected and the other end of the sample collection tube extends into a sampling bottle; one end of the waste gas recovery tube is communicated with the waste gas collection tube and the other end of the waste gas recovery tube is communicated with a waste gas recovery system; and the gases in the sampling bottle enter the waste gas recovery system through the waste gas collection tube and the waste gas recovery tube to be treated. The invention also relates to a using method of the sampling head device, which comprises: sample collection; waste gas recovery and removal of residual sample in a sampling head. In the invention, the sampling head device has a three-way structure, so the processing of a sealing gasket at the mouth of the bottle is convenient; and in the device, the sampling head is swept by blowing to remove the residual sample liquid in the sampling head after the sampling is finished, so environmental pollution is avoided effectively and the operation is safe, simple and convenient.

Description

A kind of three-way sampling head device and using method thereof
Technical field
The present invention relates to a kind of sampling head device and using method thereof, specifically, relate to a kind of sampling head device that is used for various poisonous and harmful fluids at the sampling operation of production, analytic process, be widely used in industrial circles such as medicine, chemical industry and food.
Background technology
The analytical sampling device has in chemical industry, medicine and food industry very to be used widely, and existing sampling head adopts crosspointer structure connecting tube mostly, and its operation is comparatively complicated, and the processing of sampling head is comparatively complicated, and cost is higher.And because the bottleneck of crosspointer structural requirement sampling bottle is bigger, more difficult to the packing washer of bottleneck like this; Be easy to related O-ring seal during sampling operation and be pushed in the sampling bottle, therefore causing the sampling head of present use all is the crosspointer structure sampling head of import, and just needle gage is shorter than homemade sampling head.And, the present sampling head of crosspointer structure, during collected specimens, poisonous and harmful fluid residual in sampling head is difficult to clean, and environmental pollution is serious.Therefore, be badly in need of a kind of sampling head device that can be used for the poisonous and harmful sampling fluids.
Summary of the invention
The invention provides a kind of sampling head device, this sampling head device has three-port structure, has only a syringe needle, require less to the sampling bottle bottleneck, make things convenient for the processing of the packing washer of bottleneck, and can prevent the leakage pollution on the environment of residual sample in the sampling head, simple and safe operation.
In order to achieve the above object, the invention provides a kind of sampling head device with three-port structure, this sampling head device comprises:
Three-port structure, this three-port structure have the first one-tenth end, the second one-tenth end and the three one-tenth ends;
Be set in the sampling pipe in the described three-port structure, the first one-tenth end of an end and the three-port structure of this sampling pipe is fixing, and extend on the pipeline of wanting collected specimens; The other end of this collection tube passes the second one-tenth end of three-port structure, and extend in the sampling bottle by the sampling bottleneck, and the sample of collection is transferred in the sampling bottle by described sampling pipe;
Be nested with the gas sampling pipe in the sampling pipe outside, this gas sampling pipe is fixing with the second one-tenth end of three-port structure, and this gas sampling pipe only is nested with the end at sampling pipe, is not to be nested with fully in whole sample collection tube outside; One end of this gas sampling pipe extend in the sampling bottle by the sampling bottleneck, and its other end sealing is arranged on three-port structure inside; And,
Be arranged in the three-port structure and with the three one-tenth exhaust gas recycling tube roads that end is fixing of three-port structure, one end in this exhaust gas recycling tube road is communicated with the end of gas sampling pipe, and be not communicated with the sampling pipe of gas sampling pipe inside, its other end is communicated with gas recovery system; Gas in the sampling bottle enters gas recovery system through the exhaust gas recycling tube road and recycles by the end of gas sampling pipe.
The passage that gas sampling pipe and exhaust gas recycling tube road are formed not only plays the effect of reclaiming fluid sample steam in the collecting bottle, can also make collecting bottle internal pressure and atmospheric pressure balance, the sampling difficulty of avoiding the sampling bottle internal gas pressure to rise and cause.
One end of described sampling pipe is connected and fixed with the first one-tenth end bite type of three-port structure, and an end of described gas sampling pipe is connected and fixed with the second one-tenth end bite type of three-port structure, and the three one-tenth ends adopt bite type to fixedly connected with the exhaust gas recycling tube road.
The invention still further relates to a kind of using method of sampling head device, specifically comprise:
Step 1, collected specimens, the sample that will gather by sampling pipe is transferred in the sampling bottle;
Step 2 reclaims waste gas, and the steam in the sampling bottle by the gas sampling pipe, is input to gas recovery system through the exhaust gas recycling tube road and recycles;
Step 3 is blown into nitrogen along the passage of collected specimens, and this nitrogen enters collecting bottle from sampling pipe, again through the gas sampling pipe, by the exhaust gas recycling tube road, enters into gas recovery system, removes the sample residues in described each pipeline.
Sampling head device provided by the invention has only a syringe needle, require less to the sampling bottle bottleneck, make things convenient for the processing of the packing washer of bottleneck, and use this sampling head device with three-port structure, after sampling finishes, can feed nitrogen sampling head is purged, remove the sample raffinate of sampling head inside fully, can effectively avoid environmental pollution, simple and safe operation.
Description of drawings
Accompanying drawing 1 is the structural representation of three-way sampling head device of the present invention.
Embodiment
As shown in Figure 1, the present invention adopts a kind of sampling head device with three-port structure, and this sampling head device comprises:
Three-port structure 1, this three-port structure have the first one-tenth end 11, the second one-tenth end 12 and the three one-tenth ends 13;
Be set in the sampling pipe 2 in the three-port structure, the first one-tenth end of these collection tube 2 one ends 21 and three-port structure, 11 bite types are fixedly connected, and extend on the pipeline of sample to be collected, in order to collected specimens; The other end 22 of this collection tube 2 passes the second one-tenth of three-port structure 1 and holds 12, extend in the sampling bottle 5 by the sampling bottleneck; The sample of gathering is transferred in the sampling bottle 5 by described sampling pipe 2;
Be nested with gas sampling pipe 3 in sampling pipe 2 outsides, this gas sampling pipe 3 only is set in 22 those ends of collection tube 2, be not set in the outside of whole collection tube 2, this gas sampling pipe 3 is fixedly connected with the second one-tenth end 12 bite type of three-port structure 1, and an end 31 of this gas sampling pipe 3 extend in the sampling bottle 5 by the sampling bottleneck; The other end 32 sealings of this gas sampling pipe 3 are arranged on the inside of three-port structure 1, make its pipeline through hole be in closed state with the first one-tenth end 11 of three-port structure; And,
Be arranged in the three-port structure 1 and with the three one-tenth fixedly connected exhaust gas recycling tube roads 4 of end 13 bite types of three-port structure 1, one end 41 in this exhaust gas recycling tube road 4 is communicated with the end 32 of gas sampling pipe 3, and be not communicated with the sampling pipe 2 of gas sampling pipe 3 inside, its other end 42 is communicated with gas recovery system; Gas in the sampling bottle 5 enters gas recovery system through exhaust gas recycling tube road 4 and recycles by the end 31 of gas sampling pipe 3.
Sampling bottle 5 by the packing washer of bottleneck, with the gas sampling pipe 3 that stretches in the sampling bottle 5, seals in the bottleneck junction; When gathering fluid sample, the fluid sample of being gathered enters into sampling bottle 5 by sampling pipe 2; When gathering, the fluid steam in the sampling bottle 5 enters into gas sampling pipe 3 by the through hole of the end 31 of gas sampling pipe 3, then, is connected with gas recovery system through exhaust gas recycling tube road 4, and waste gas is recycled; And the air in the collecting bottle 5 also is connected with atmosphere by this passage, in order to avoid pressure rises in the collecting bottle, influence is gathered; After collection finishes, feed each pipeline in the purging with nitrogen gas three-port structures 1, comprise sampling pipe 2, gas sampling pipe 3 and exhaust gas recycling tube road 4 from the port 21 of sampling pipe 2; Can avoid the residual of interior solvent of above-mentioned pipeline and steam thereof, contaminated environment, harmful to human.
Because the present invention adopts the sampling head device with three-port structure, need only a syringe needle and both can finish, lower to the bottleneck seal request, and collected specimens finishes, and also can feed nitrogen and purge, and removes the residual sample in the pipeline, make that this device is environmentally friendly, safe.
Although content of the present invention has been done detailed introduction by above preferred embodiment; but will be appreciated that above-mentioned description should not be considered to limitation of the present invention. after those skilled in the art have read foregoing; for multiple modification of the present invention with to substitute all will be conspicuous. therefore, protection scope of the present invention should be limited to the appended claims.

Claims (6)

1. a three-way sampling head device is characterized in that, this sampling head device comprises:
Three-port structure (1), this three-port structure (1) have the first one-tenth end (11), the second one-tenth end (12) and the three one-tenth ends (13);
Be set in the sampling pipe (2) in the described three-port structure (1), the first one-tenth end of one end (21) and three-port structure (11) of this sampling pipe (2) is fixing, and extend on the pipeline of sample to be collected, its other end (22) passes the second one-tenth end (12) of three-port structure (1), extend in the sampling bottle (5);
Be nested with at the outside gas sampling pipe (3) of sampling pipe (2), one end (31) of this gas sampling pipe (3) is fixing with the second one-tenth end (12) of three-port structure, and extend in the sampling bottle (5), its other end (32) sealing is arranged on the inside of three-port structure (1); And,
Be arranged in the three-port structure (1) and with the fixing exhaust gas recycling tube road (4) of the three one-tenth ends (13) of three-port structure (1), one end (41) in this exhaust gas recycling tube road (4) is communicated with the end (32) of gas sampling pipe, and its other end (42) is communicated with gas recovery system.
2. three-way sampling head device as claimed in claim 1 is characterized in that, an end (21) of described sampling pipe (2) is connected and fixed with the first one-tenth end (11) bite type of three-port structure (1).
3. three-way sampling head device as claimed in claim 1 is characterized in that, an end (3 1) of described gas sampling pipe (3) is connected and fixed with the second one-tenth end (12) bite type of three-port structure (1).
4. three-way sampling head device as claimed in claim 1 is characterized in that, the three one-tenth ends (13) of three-port structure (1) adopt bite type to be connected and fixed with exhaust gas recycling tube road (4).
5. three-way sampling head device as claimed in claim 1 is characterized in that, described exhaust gas recycling tube road (4) sampling pipe (1) inner with being arranged on gas sampling pipe (3) is not communicated with.
6. the using method of a three-way sampling head device is characterized in that, this method may further comprise the steps:
Step 1, collected specimens, the sample that will gather by sampling pipe (2) is transferred in the sampling bottle;
Step 2 reclaims waste gas, and the waste gas in the sampling bottle by gas sampling pipe (3), is input to gas recovery system through exhaust gas recycling tube road (4) and recycles;
Step 3 is blown into nitrogen along the passage of collected specimens, and this nitrogen enters collecting bottle (5) from sampling pipe (2), again through gas sampling pipe (3), by exhaust gas recycling tube road (4), enter into gas recovery system, remove the sample residues in described each pipeline.
CN2009101990671A 2009-11-19 2009-11-19 Three-way sampling head device and using method thereof Active CN101706380B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009101990671A CN101706380B (en) 2009-11-19 2009-11-19 Three-way sampling head device and using method thereof

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Application Number Priority Date Filing Date Title
CN2009101990671A CN101706380B (en) 2009-11-19 2009-11-19 Three-way sampling head device and using method thereof

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CN101706380A true CN101706380A (en) 2010-05-12
CN101706380B CN101706380B (en) 2011-08-31

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109406814A (en) * 2018-12-24 2019-03-01 江苏科维仪表控制工程有限公司 A kind of sample retrieval system
CN113447321A (en) * 2021-08-17 2021-09-28 古海燕 Oil refining chemical industry enterprise safety ring protects gaseous sampling device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109406814A (en) * 2018-12-24 2019-03-01 江苏科维仪表控制工程有限公司 A kind of sample retrieval system
CN109406814B (en) * 2018-12-24 2024-04-12 江苏科维仪表控制工程有限公司 Sample recovery system
CN113447321A (en) * 2021-08-17 2021-09-28 古海燕 Oil refining chemical industry enterprise safety ring protects gaseous sampling device

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