CN101693655B - 优化的液相氧化方法 - Google Patents

优化的液相氧化方法 Download PDF

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Publication number
CN101693655B
CN101693655B CN200910205021.6A CN200910205021A CN101693655B CN 101693655 B CN101693655 B CN 101693655B CN 200910205021 A CN200910205021 A CN 200910205021A CN 101693655 B CN101693655 B CN 101693655B
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CN
China
Prior art keywords
reaction medium
reaction zone
reaction
feed
oxidant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN200910205021.6A
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English (en)
Chinese (zh)
Other versions
CN101693655A (zh
Inventor
A·G·万德斯
L·R·帕丁
W·S·施特拉泽
M·德弗里德
P·古普塔
H·W·小詹金斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Grupo Petrotemex SA de CV
Original Assignee
Eastman Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/154,479 external-priority patent/US7608733B2/en
Priority claimed from US11/154,165 external-priority patent/US7381836B2/en
Application filed by Eastman Chemical Co filed Critical Eastman Chemical Co
Publication of CN101693655A publication Critical patent/CN101693655A/zh
Application granted granted Critical
Publication of CN101693655B publication Critical patent/CN101693655B/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14—Monocyclic dicarboxylic acids
    • C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/26—1,4 - Benzenedicarboxylic acid

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN200910205021.6A 2004-09-02 2005-08-29 优化的液相氧化方法 Expired - Lifetime CN101693655B (zh)

Applications Claiming Priority (12)

Application Number Priority Date Filing Date Title
US60673604P 2004-09-02 2004-09-02
US60678704P 2004-09-02 2004-09-02
US60/606736 2004-09-02
US60/606787 2004-09-02
US63139804P 2004-11-29 2004-11-29
US63135104P 2004-11-29 2004-11-29
US60/631398 2004-11-29
US60/631351 2004-11-29
US11/154479 2005-06-16
US11/154,479 US7608733B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
US11/154,165 US7381836B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
US11/154165 2005-06-16

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN2005800295416A Division CN101010277B (zh) 2004-09-02 2005-08-29 优化的液相氧化

Publications (2)

Publication Number Publication Date
CN101693655A CN101693655A (zh) 2010-04-14
CN101693655B true CN101693655B (zh) 2014-01-08

Family

ID=35825414

Family Applications (4)

Application Number Title Priority Date Filing Date
CN200910205021.6A Expired - Lifetime CN101693655B (zh) 2004-09-02 2005-08-29 优化的液相氧化方法
CN201210124407.6A Expired - Lifetime CN102698699B (zh) 2004-09-02 2005-08-29 优化的液相氧化
CN2005800295416A Expired - Lifetime CN101010277B (zh) 2004-09-02 2005-08-29 优化的液相氧化
CN2012101244697A Pending CN102701940A (zh) 2004-09-02 2005-08-29 优化的液相氧化

Family Applications After (3)

Application Number Title Priority Date Filing Date
CN201210124407.6A Expired - Lifetime CN102698699B (zh) 2004-09-02 2005-08-29 优化的液相氧化
CN2005800295416A Expired - Lifetime CN101010277B (zh) 2004-09-02 2005-08-29 优化的液相氧化
CN2012101244697A Pending CN102701940A (zh) 2004-09-02 2005-08-29 优化的液相氧化

Country Status (11)

Country Link
EP (1) EP1786751B1 (enExample)
JP (1) JP2008511648A (enExample)
KR (1) KR101281408B1 (enExample)
CN (4) CN101693655B (enExample)
BR (1) BRPI0514769A (enExample)
CA (1) CA2576341A1 (enExample)
ES (1) ES2544235T3 (enExample)
MX (1) MX2007002513A (enExample)
PL (1) PL1786751T3 (enExample)
PT (1) PT1786751E (enExample)
WO (1) WO2006031422A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102701940A (zh) * 2004-09-02 2012-10-03 奇派特石化有限公司 优化的液相氧化

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3839435A (en) * 1972-01-13 1974-10-01 Maruzen Oil Co Ltd Process for producing fiber grade terephthalic acid
US5928521A (en) * 1995-04-05 1999-07-27 Mannesmann Aktiengesellschaft Arrangement and process for oxidizing an aqueous medium
WO2003078369A1 (de) * 2002-03-18 2003-09-25 Basf Aktiengesellschaft Oxidation von o-xylol zu o-tolylsäure und anderen oxidationsprodukten durch gestaffelte zufuhr eines sauerstoffhaltigen gases
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5912096B2 (ja) * 1975-10-31 1984-03-21 三菱化学株式会社 ホウコウゾクポリカルボンサンノセイゾウホウ
JPS52111532A (en) * 1976-03-11 1977-09-19 Kuraray Yuka Kk Production of high-purity terephthalic acid
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
ID19133A (id) * 1996-12-12 1998-06-18 Praxair Technology Inc Pengisian oksigen langsung kedalam reaktor-reaktor ruang gelembung
CA2396967A1 (en) * 2000-01-21 2001-07-26 Bp Corporation North America Inc. Production of high purity aromatic carboxylic acid by oxidation in benzoic acid and water solvent
JP2001247511A (ja) * 2000-03-07 2001-09-11 Mitsubishi Chemicals Corp 芳香族カルボン酸の製造方法
US6504051B1 (en) * 2001-06-04 2003-01-07 Eastman Chemical Company Process for production of aromatic carboxylic acids with improved water removal technique
PL208869B1 (pl) * 2002-12-09 2011-06-30 Eastman Chem Co Sposób wytwarzania produktu oczyszczonego kwasu karboksylowego
CN1208301C (zh) * 2003-08-08 2005-06-29 中国纺织工业设计院 一种生产对苯二甲酸用的气升式外循环鼓泡塔氧化装置
CN2654608Y (zh) * 2003-10-12 2004-11-10 浙江大学 用于生产对苯二甲酸的鼓泡塔氧化反应装置
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
MX2007002513A (es) * 2004-09-02 2007-05-04 Eastman Chem Co Oxidacion en fase liquida optimizada.

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3839435A (en) * 1972-01-13 1974-10-01 Maruzen Oil Co Ltd Process for producing fiber grade terephthalic acid
US5928521A (en) * 1995-04-05 1999-07-27 Mannesmann Aktiengesellschaft Arrangement and process for oxidizing an aqueous medium
WO2003078369A1 (de) * 2002-03-18 2003-09-25 Basf Aktiengesellschaft Oxidation von o-xylol zu o-tolylsäure und anderen oxidationsprodukten durch gestaffelte zufuhr eines sauerstoffhaltigen gases
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102701940A (zh) * 2004-09-02 2012-10-03 奇派特石化有限公司 优化的液相氧化

Also Published As

Publication number Publication date
WO2006031422A2 (en) 2006-03-23
ES2544235T3 (es) 2015-08-28
BRPI0514769A (pt) 2008-06-24
CN101693655A (zh) 2010-04-14
CN102698699B (zh) 2016-03-02
MX2007002513A (es) 2007-05-04
EP1786751B1 (en) 2015-06-03
CN101010277A (zh) 2007-08-01
CN101010277B (zh) 2012-06-13
PL1786751T3 (pl) 2015-12-31
CN102701940A (zh) 2012-10-03
CN102698699A (zh) 2012-10-03
CA2576341A1 (en) 2006-03-23
KR101281408B1 (ko) 2013-07-02
JP2008511648A (ja) 2008-04-17
EP1786751A2 (en) 2007-05-23
KR20070054704A (ko) 2007-05-29
PT1786751E (pt) 2015-09-24
WO2006031422A3 (en) 2006-10-12

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Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: PEMEX GROUP LLC

Free format text: FORMER OWNER: EASTMAN CHEM CO.

Effective date: 20110914

C41 Transfer of patent application or patent right or utility model
TA01 Transfer of patent application right

Effective date of registration: 20110914

Address after: Nuevo Leon, Mexico

Applicant after: GRUPO PETROTEMEX, S.A. de C.V.

Address before: Tennessee

Applicant before: EASTMAN CHEMICAL Co.

EE01 Entry into force of recordation of patent licensing contract

Assignee: JIAXING PETROCHEMICAL Co.,Ltd.

Assignor: GRUPO PETROTEMEX, S.A. de C.V.

Contract record no.: 2012990000015

Denomination of invention: Optimized liquid-phase oxidation

License type: Common License

Open date: 20100414

Record date: 20120113

C14 Grant of patent or utility model
GR01 Patent grant
CX01 Expiry of patent term

Granted publication date: 20140108

CX01 Expiry of patent term