CN101684051A - Production process of organic-inorganic compound fertilizer - Google Patents

Production process of organic-inorganic compound fertilizer Download PDF

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Publication number
CN101684051A
CN101684051A CN200810141473A CN200810141473A CN101684051A CN 101684051 A CN101684051 A CN 101684051A CN 200810141473 A CN200810141473 A CN 200810141473A CN 200810141473 A CN200810141473 A CN 200810141473A CN 101684051 A CN101684051 A CN 101684051A
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China
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organic
granulation
production process
compound fertilizer
drying
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CN200810141473A
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Chinese (zh)
Inventor
仵树仁
李霄锋
张献军
郝天才
丁全
田丰收
朱瑞青
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Henan Caixin Industrial Chemical Co Ltd
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Henan Caixin Industrial Chemical Co Ltd
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Priority to CN200810141473A priority Critical patent/CN101684051A/en
Publication of CN101684051A publication Critical patent/CN101684051A/en
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Abstract

A technology problem solved by the invention is to provide a production process of organic-inorganic compound fertilizer with high pelleting rate, round appearance and low moisture. The process has the steps of: fermenting organic raw materials into ecological organic fertilizer, adding inorganic raw material into a crusher; pelleting by assistantly adding water, steam and urine after crush of thematerial in the rotary drum comminutor; pelleting continuously using the material in the disk comminutor from the rotary drum comminutor; carrying out two-stage drying for the material after pelleting, and cooling the material; sieving macrobead in the cooled material; packing the sieved product after anti-blocking treatment and then delivering them out of factory. Using the technical scheme cansufficiently play the roles of the two kinds of pelleting methods, as well as solve the problems of bad appearance quality of product, and high moisture of pelleting.

Description

Production process of organic-inorganic compound fertilizer
Technical field
The invention belongs to a kind of compound fertilizer production technology.
Background technology
The fertilizer material used for agriculture that is absolutely necessary in agriculture production, present existing fertilizer is divided into mineral manure and organic fertilizer, mineral manure is mineral substance or inorganic chemistry reacts the fertilizer that processes, organic fertilizer is the fertilizer that the waste in natural humus matter, livestock and poultry manure, industrial production or the people's life processes, and the production technology of mineral manure, organic fertilizer is very ripe.
In China, for many years because long-term application chemical fertilizer, the fertilizer deficiency, all kinds of nutrients ratios imbalances cause farmland ecological environment, soil physical and chemical property and soil microflora to be subjected in various degree destruction, have influenced the safety of agricultural-food to a certain extent.The life-time service of chemical fertilizer or use the improper problem that may cause and have: farmland quality descends, and output descends, and quality descends, environmental pollution.Western countries' bio-feritlizers such as the U.S. are near 50% of the total consumption of fertilizer.China's organic fertilizer production is ascendant trend year after year, and market outlook are wide, becomes the new industry of a new round.State Council clearly proposes to promote " ecological agriculture " in ten big countermeasures of China's ecological environmental protection.In order to develop eco-agriculture, Development and Production is pollution-free " green food ", and the fertilizer practice in the agriculture production must be reformed, and promptly rational use of chemical fertilizer walk the development of organic-inorganic compounding application, and organic fertilizer should be advocated energetically and be developed more.
At present, China's organic fertilizer raw materials for production mainly comprise tens kinds of poultry manure, mud, stalk, the peat composed of rotten mosses, bone meal, grouts etc.These raw fibre cellulose content height, self viscosity are poor, it is big to contain moisture, cause the granulation difficulty, and the particle roundness is poor.Because product moisture content causes the storage time short greatly, the fertilizer of production will be used in very short time, otherwise can harden; The particle roundness is poor, from not accepted by the user in appearance, has limited the production and selling of fertilizer to a great extent; Production capacity is low, the cost height.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of production technique of making ball rate height, outward appearance rounding, containing the low organic-inorganic complex fertilizer of moisture.
For solving the problems of the technologies described above, the present invention by the following technical solutions: production process of organic-inorganic compound fertilizer comprises the following steps:
A, the organic raw material fermentative processing is become ecological organic fertilier, add crusher with inorganic raw material;
B, organic and inorganic raw material enter after fragmentation in the rotary drum granulator, by mending entry, steam, the auxiliary granulation of urine;
The material that c, rotary drum granulator come out enters granulating disc again, continues granulation;
D, then the material after the granulation is carried out two-stage drying, material after the granulation enters into the 1# drying machine and carries out drying, dried material is sent into the scalping sieve and is gone fine powder, other material to enter 2# drying machine continuation drying, and the material behind two-stage drying is sent into the cooler cooling;
E, cooled material enter big grain sieve, and macrobead is screened out;
F, finished product and part fine powder enter the finished product sieve and continue screening, and the finished product that sifts out can be packed after anti-caking is handled and dispatch from the factory.
Inorganic raw material described in the step a is phosphorus ammonium, general calcium, urea, Repone K;
Two sections drying processes in the steps d, bake out temperature is controlled at 60~80 ℃.
Macrobead enters tablets press among the step e after fragmentation.
Fines returns tablets press among the step f.
Adopt above technical scheme to give full play to the advantage of two kinds of prilling process, the solution product appearance is of poor quality, granulation contains the high problem of moisture.Because rotary drum granulator is long cylindrical shell; the steam, the urine that add have competent sprinkling space, and powder granulous base fertilizer is by means of water, steam, the molten adhesive aggregation granulating of fertilizer, with the rotation of tablets press; material is at the granulating of progressively reuniting in the discharge end process of flowing, and the granulation amount of water is few.The disk granulation makes the disposable balling ratio height of particle, and the returning charge multiple is little, and operation is directly perceived, because its rotating speed is higher relatively, rounding particle is not had the effect of polishing, rounding, the ropy problem of solution organic-inorganic composite fertilizer product appearance.
Production technique production capacity of the present invention obviously increases, the production technique of taking drum granulating and disk granulation to be in series, utilization replenishes required moisture and the heat of granulation in rotary drum granulator, in rotary drum granulator, realize the balling ratio more than 50%, owing to realized the heat granulation, the moisture branch of granulation material obviously reduces; Need not add water in granulating disc, the burden that makes granulating disc bear granulation reduces greatly, and granulating disc mainly is responsible for the effect of polishing, rounding.Because this tandem process has solved two big defectives of disk granulation, the oven dry load is lower, so the production capacity of this technology is higher.
Production process of organic-inorganic compound fertilizer of the present invention; granulating working procedure adopts drum granulating to add the disk granulation; in rotary drum granulator, mend required moisture and the heat of granulation; in granulating disc, improve balling ratio, improve the particle roundness; take two-stage granulation tandem process to make the granulation balling ratio improve 20%, give full play to the advantage of two kinds of prilling process again, the product water content is low; solve the second-rate problem of organic and inorganic fertilizer product appearance, improve production capacity.
Description of drawings
Accompanying drawing is a production process of organic-inorganic compound fertilizer schema of the present invention.
Embodiment
Embodiment 1
As shown in drawings, organic raw material becomes ecological organic fertilier after fermentative processing, distinguishes after metering with inorganic raw materials such as phosphorus ammonium, general calcium, urea, Repone K, and incoming stock e Foerderanlage, various raw materials all should have good physical property and certain fineness; Comprise organic raw material, the raw material that enters system is less than 1mm 〉=60%; Behind crusher, crusher outlet material granularity reaches: less than 2mm 〉=95%; Enter bucket elevator then, send into rotary drum granulator by bucket elevator again, by water, steam, the auxiliary granulation of urine, material in tablets press by the rotation of body, form the thermopnore of mechanical type solid materials, in the Flow of Goods and Materials process the extruding, frictional force effect under, be agglomerated into spheroidal particle, rotary drum granulator outlet material diameter 1~4mm accounts for more than 50%, the material that rotary drum granulator comes out enters granulating disc through e Foerderanlage and material guiding device, continue granulation, granulating disc outlet material diameter 1~4mm accounts for more than 70%; The granulation temperature of charge is 50 ℃, and the granulation material contains moisture and is controlled at 7%; Material after the granulation is delivered to the import of 1# drying machine by e Foerderanlage, is sent into the charging flight section of drying machine by elephant trunk.Material is by the volution flight, and the wet pellet that will have thermo-sensitivity moves apart high-temperature area, is thrown into heating zone; By elevate a turnable ladder formula flight, the pellet elevate a turnable ladder is shed space at drying machine, pellet is fully contacted with hot furnace gas, quicken to conduct heat, finish the process that dehydrates of granular material.The hot gas flow that drying process is required, the high-temperature furnace gas by coal is produced in roasting kiln with the hot and cold air thorough mixing, is made into the working heat air-flow of institute's air demand and temperature with an injection air inducing device, sends into drying machine; Hot gas becomes the concurrent drying operation of equidirectional with material.This device adopts two-stage drying, by the dried material of 1# drying machine, sends into the scalping sieve and removes fine powder, and other material enters 2# drying machine continuation drying through e Foerderanlage and bucket elevator, and the material behind two-stage drying is sent into the cooler cooling by bucket elevator.
The finished product process of cooling mainly is that the moisture that removes is not spread on the particle top layer as yet, by the air of the bed that flows steam is taken away, and reaches the cooling purpose simultaneously.The controlled chilling air quantity is cooled to below 45 degree temperature of charge.
Cooled material enters big grain sieve through bucket elevator, will screen out greater than the macrobead of 4.75mm, and macrobead enters tablets press by raw material conveying device after fragmentation.Finished product and part fine powder enter the finished product sieve and continue screening, and it is 3% of output that the finished product that sifts out is handled the applying medicinal powder add-on through anti-caking; The anti-hard caking agent add-on is 2% of an output.Can pack then and dispatch from the factory, fines then returns raw material conveying device and enters tablets press.
Because the organic-inorganic complex fertilizer production process requires the standard height to bake out temperature, adopt two sections drying processes in this technological design, bake out temperature reduces, and controls 70 ℃, realizes reducing the purpose of moisture by prolonging drying time.
Thereby reach produce the particle appearance rounding, evenly, contain the low organic-inorganic complex fertilizer of being convenient to store of moisture.
In screening system, can adopt following configuration:
One, at " screening 1 " configuration macrobead sieve and small-particle sieve, at " screening 2 " configuration small-particle sieve;
Two, at " screening 1 " configuration small-particle sieve, at " screening 2 " configuration macrobead sieve and small-particle sieve;
Three, at " screening 1 " configuration macrobead sieve, at " screening 2 " configuration macrobead sieve and small-particle sieve;
Embodiment 2
Prilling temperature is 40 ℃ in the present embodiment, and the granulation material contains moisture and is controlled at 10%, and bake out temperature is controlled to be 60 ℃.Other steps are identical with embodiment 1.
Embodiment 3
Prilling temperature is 60 ℃ in the present embodiment, and the granulation material contains moisture and is controlled at 5%, and bake out temperature is controlled to be 80 ℃.Other steps are identical with embodiment 1.
Embodiment 4
Prilling temperature is 55 ℃ in the present embodiment, and the granulation material contains moisture and is controlled at 8%, and bake out temperature is controlled to be 65 ℃.Other steps are identical with embodiment 1.

Claims (5)

1, a kind of production process of organic-inorganic compound fertilizer is characterized in that: comprise the following steps:
A, the organic raw material fermentative processing is become ecological organic fertilier, add crusher with inorganic raw material;
B, organic and inorganic raw material enter after fragmentation in the rotary drum granulator, by mending entry, steam, the auxiliary granulation of urine;
The material that c, rotary drum granulator come out enters granulating disc again, continues granulation;
D, then the material after the granulation is carried out two-stage drying, material after the granulation enters into the 1# drying machine and carries out drying, dried material is sent into the scalping sieve and is gone fine powder, other material to enter 2# drying machine continuation drying, and the material behind two-stage drying is sent into the cooler cooling;
E, cooled material enter big grain sieve, and macrobead is screened out;
F, finished product and part fine powder enter the finished product sieve and continue screening, and the finished product that sifts out can be packed after anti-caking is handled and dispatch from the factory.
2, according to the described production process of organic-inorganic compound fertilizer of claim 1, it is characterized in that: inorganic raw material described in the step a is phosphorus ammonium, general calcium, urea, Repone K;
3, according to the described production process of organic-inorganic compound fertilizer of claim 1, it is characterized in that: two sections drying processes in the steps d, bake out temperature is controlled at 60~80 ℃.
4, according to the described production process of organic-inorganic compound fertilizer of claim 1, it is characterized in that: macrobead enters tablets press among the step e after fragmentation.
5, according to the described production process of organic-inorganic compound fertilizer of claim 1, it is characterized in that: fines returns tablets press among the step f.
CN200810141473A 2008-09-27 2008-09-27 Production process of organic-inorganic compound fertilizer Pending CN101684051A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101921149A (en) * 2010-08-24 2010-12-22 中盐安徽红四方股份有限公司 Filler-free synergistic compound fertilizer produced by urine syrup ammonia-acid method and production method thereof
CN102173940A (en) * 2011-02-02 2011-09-07 安徽国祯生物质发电有限责任公司 Carbon black as anticaking agent of compound fertilizer and production process of carbon black
CN102285822A (en) * 2010-06-18 2011-12-21 河南财鑫实业化工有限责任公司 Method for preparing environmental-friendly slow-release fertilizer
CN102408263A (en) * 2011-08-19 2012-04-11 安徽统益生物科技有限公司 Preparation method of organic inorganic compound fertilizer
CN104326830A (en) * 2014-11-13 2015-02-04 中国科学院亚热带农业生态研究所 Organic-inorganic compound fertilizer and preparation method thereof
CN105198537A (en) * 2015-10-25 2015-12-30 金乡蒜乡肥业化工有限公司 Multi-speed tail-drying-type mixed fertilizer granulation production process and special production equipment thereof
CN105985160A (en) * 2015-01-30 2016-10-05 山东省农业可持续发展研究所 Organic inorganic composite slow-release fertilizer and preparation method thereof
CN109851453A (en) * 2019-02-18 2019-06-07 黑龙江金合康肥业有限公司 Organic and inorganic environmental protection and public nuisance free compound fertilizer

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102285822A (en) * 2010-06-18 2011-12-21 河南财鑫实业化工有限责任公司 Method for preparing environmental-friendly slow-release fertilizer
CN101921149A (en) * 2010-08-24 2010-12-22 中盐安徽红四方股份有限公司 Filler-free synergistic compound fertilizer produced by urine syrup ammonia-acid method and production method thereof
CN101921149B (en) * 2010-08-24 2013-08-07 中盐安徽红四方股份有限公司 Filler-free synergistic compound fertilizer produced by urine syrup ammonia-acid method and production method thereof
CN102173940A (en) * 2011-02-02 2011-09-07 安徽国祯生物质发电有限责任公司 Carbon black as anticaking agent of compound fertilizer and production process of carbon black
CN102408263A (en) * 2011-08-19 2012-04-11 安徽统益生物科技有限公司 Preparation method of organic inorganic compound fertilizer
CN104326830A (en) * 2014-11-13 2015-02-04 中国科学院亚热带农业生态研究所 Organic-inorganic compound fertilizer and preparation method thereof
CN104326830B (en) * 2014-11-13 2016-11-02 中国科学院亚热带农业生态研究所 A kind of compound organic and inorganic fertilizer and preparation method
CN105985160A (en) * 2015-01-30 2016-10-05 山东省农业可持续发展研究所 Organic inorganic composite slow-release fertilizer and preparation method thereof
CN105198537A (en) * 2015-10-25 2015-12-30 金乡蒜乡肥业化工有限公司 Multi-speed tail-drying-type mixed fertilizer granulation production process and special production equipment thereof
CN105198537B (en) * 2015-10-25 2018-05-04 金乡蒜乡肥业化工有限公司 Multi-change speed tail dries formula mixed fertilizer and is granulated production technology and its production equipment special
CN109851453A (en) * 2019-02-18 2019-06-07 黑龙江金合康肥业有限公司 Organic and inorganic environmental protection and public nuisance free compound fertilizer

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