CN101684000B - Device for microwave drying germanium dioxide - Google Patents
Device for microwave drying germanium dioxide Download PDFInfo
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- CN101684000B CN101684000B CN2008102230619A CN200810223061A CN101684000B CN 101684000 B CN101684000 B CN 101684000B CN 2008102230619 A CN2008102230619 A CN 2008102230619A CN 200810223061 A CN200810223061 A CN 200810223061A CN 101684000 B CN101684000 B CN 101684000B
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Abstract
The invention belongs to the technical field of microwave drying, particularly relates to a device for microwave drying germanium dioxide. The invention improves a household microwave oven which is used as the main body; the top plate of the microwave oven is changed into a metal mesh structure, and an exhaust fan is arranged at the top of the microwave oven; a temperature control system is arranged in the microwave oven; a high-temperature automatic alarm system is arranged on the circuit connected with a transformer; the rotating shaft of a rotating disk is composed of a plurality of blades; and both cover plates of internal and external baffles of the microwave oven are coated with nanometer protective paints. When the device is used for drying germanium dioxide, the overall drying time is short, the water content of the dried germanium dioxide achieves the national standard, and the crystalline form of the germanium dioxide does not change. The invention has the advantage of low energy consumption, avoids high environment temperature, reduces working labor intensity and can be used in other dehydration and drying fields for reference.
Description
Technical field
The invention belongs to technical field of microwave drying, particularly a kind of equipment of microwave drying germanium dioxide.
Background technology
Germanium dioxide is a kind of germanium compound that important use is arranged in fields such as chemical metallurgy, generally gets by the high-purity germanium tetrachloride preparation of hydrolysis.But because hydrolysis GeCl
4Prepared GeO
2Still certain water and crystal water can be contained through behind the centrifuge dripping, therefore these water and crystal water must be removed earlier.Traditions of the past process using baking oven is dried it, but has the energy consumption height with baking oven, and baking cycle is long, and GeO
2Easy shortcoming such as caking in bake process.Therefore our company adopts the method for microwave drying to dry now, microwave drying is under the high frequency electromagnetic field effect, the material absorption of electromagnetic energy, the impellent that is converted into the heat mass transfer in material inside is the inner pressure gradient that produces rapidly of material, liquid can pressure gradient effect under from material, discharge rapidly.Therefore, contrast traditional drying means, microwave drying has that rate of heating is fast, homogeneous heating, effectively utilize advantage such as energy.But it is excessive to buy the special-purpose fund that microwave oven spent, and, industrial microwave oven and household microwave oven on some key element (as magnetron) model substantially, consider the production problems of the germanium dioxide of maintenance issues and our company, can use household microwave oven to realize drying effect.
Household microwave oven microwave output power 700w, the microwave transmitting frequency is 2450MHZ, comprise equipment such as magnetron, waveguide mouth, the time relay, rotating disk, consider the inventory of every batch of germanium dioxide, adopt household microwave oven can finish the microwave drying task of germanium dioxide substantially.But have the following disadvantages when being to use household microwave oven: the inner no exhaust fan of cavity of household microwave oven is unfavorable for the water vapour evaporation; Anhydrous minute means of detection of domestic microwave furnace interior, can't know whether inner germanium dioxide dries, and when the germanium dioxide internal moisture was dried, dry material-germanium dioxide became main energy absorption person, under the effect of frequency electromagnetic waves, make germanium dioxide produce other chemical transformation easily; Supply transformer can burn transformer easily because of self power consumption heating when household microwave oven used for a long time; The household microwave oven supporting capacity is limited, and the rotating shaft position of rotating disk is fragile; When producing germanium dioxide, because the hydrolysis germanium tetrachloride can produce hydrochloric acid, so household microwave oven easily is corroded when using in the production scene.
Summary of the invention
The present invention is directed to the deficiency of household microwave oven when dry germanium dioxide, a kind of equipment of microwave drying germanium dioxide is provided,, has made the top board 5 of microwave oven 1 into wire netting poroid structure based on microwave oven 1, play the effect of electromagnetic shielding, avoid microwave leakage; And the vent fan system 2 of taking out is set at the top of microwave oven 1, to improve the volatilization of water vapour; Temperature control system 3 is installed in microwave oven 1; On the circuit that connects transformer, the high temperature automatic alarm system is set; The rotating shaft 7 of rotating disk 6 is made of 4～10 flabellums.
The metal mesh opening of described top board 5 adopts copper mesh as shielding material, and thickness is 0.5～3mm, and mesh diameter is 1.5～4.5mm.
Described temperature control system 3 adopts long-range inductive probe that the microwave oven internal temperature is surveyed.
All scribble the nanometer protective paint on the cover plate of the interior outer baffle of described microwave oven 1 and the blower fan, play erosion-resisting effect.
Beneficial effect of the present invention is: adopt equipment of the present invention that germanium dioxide is carried out drying, overall drying time is about 2 hours, shortened drying time, and oven dry back germanium dioxide water content is up to state standards discovery germanium dioxide crystalline form no change behind the process electron-microscope scanning; Can cut down the consumption of energy behind the equipment after the improvement, avoid high ambient temperature, reduce labor intensity, and can use for reference other dewatered drying field.
Description of drawings
Fig. 1 is a microwave oven synoptic diagram of the present invention;
Fig. 2 is a microwave oven schematic perspective view of the present invention;
Fig. 3 is the vertical view of microwave oven cavity upper plate wire netting;
Fig. 4 is the pivot structure comparison diagram after improving preceding rotating shaft in the embodiment of the invention and improving.
Number in the figure:
The 1-microwave oven; 2-takes out the vent fan system; The 3-temperature control system; The 4-control panel of microwave oven;
The 5-top board; The 6-rotating disk; The 7-rotating shaft; The 8-microwave generating apparatus.
Embodiment
The invention provides a kind of equipment of microwave drying germanium dioxide, the invention will be further described below in conjunction with description of drawings and embodiment:
Fig. 1 is a microwave oven synoptic diagram of the present invention; Fig. 2 is a microwave oven schematic perspective view of the present invention.Use household microwave oven, and make improvements:
(1) Fig. 3 is the vertical view of microwave oven cavity upper plate wire netting; Make the top board 5 of microwave oven 1 into wire netting poroid structure, adopt copper mesh as shielding material, thickness is 1mm, and the aperture is 3mm, and the poroid structure of wire netting can play the effect of electromagnetic shielding, avoid microwave leakage, the vent fan system of taking out is installed at microwave oven 1 top,, takes out the FZ560B0000 type interchange aerofoil fan that vent fan system 2 adopts FANS-TECH company to produce to improve the volatilization of water vapour, power 420W, rotating speed 880RPM;
(2) add temperature control system 3 in microwave oven 1, temperature control system 3 adopts the Luxtron Luxtron FOT Lab Kit of company type optical fiber temperature-measurement meters as temperature measuring equipment (adopt the long-range inductive probe of STR type, range-25～330 ℃); Temp controlled meter adopts the Japanese SHIMAX MAC50A of company type temperature control instrument; When washiness, microwave energy is mainly absorbed by water, temperature can remain on a general constant temp in the stove, when moisture in the few or material substantially anhydrous the time, dry material one germanium dioxide becomes main energy absorption person, at this moment temperature will raise, and when temperature is elevated to a certain degree, can make microwave oven 1 stop heating automatically by temperature control system 3;
(3) installing the high temperature automatic alarm system additional on the circuit that connects transformer avoids transformer to burn out;
(4) Fig. 4 is the pivot structure comparison diagram after improving preceding rotating shaft in the embodiment of the invention and improving; In the family expenses microwave oven, the rotating shaft of rotating disk is made of 3 flabellums, the limited and easy damage of weight capacity, the structure of 6 flabellums is used in rotating shaft in the present invention 7, angle between each flabellum is 60 °, and material is the bakelite material, Y font and the M shape of concrete structure such as Fig. 4;
(5) coat the nanometer protective paint on microwave oven 1 inside and outside baffle plate cover plate, nano-paint adopts the German KLB-AC 2055M of Krupp type bicomponent epoxy resin antifouling paste, avoids the corrosion of on-the-spot sour environment to equipment.
By control panel of microwave oven 4 is provided with, realize the drying to germanous chloride, overall drying time is about 2 hours, has shortened drying time, and oven dry back germanium dioxide water content is up to state standards, through finding germanium dioxide crystalline form no change behind the electron-microscope scanning.
Claims (3)
1. the equipment of a microwave drying germanium dioxide based on microwave oven (1), is characterized in that, makes the top board (5) of microwave oven (1) into wire netting poroid structure, plays the effect of electromagnetic shielding, avoids microwave leakage; And the vent fan system (2) of taking out is set at the top of microwave oven (1), to improve the volatilization of water vapour; Temperature control system (3) is installed in microwave oven (1); On the circuit that connects transformer, the high temperature automatic alarm system is set; The rotating shaft (7) of rotating disk (6) is made of 4～10 flabellums; All scribble the bicomponent epoxy resin antifouling paste on the cover plate of the interior outer baffle of described microwave oven (1) and the blower fan, play erosion-resisting effect.
2. the equipment of a kind of microwave drying germanium dioxide according to claim 1 is characterized in that, the metal mesh opening of described top board (5) adopts copper mesh as shielding material, and thickness is 0.5～3mm, and mesh diameter is 1.5～4.5mm.
3. the equipment of a kind of microwave drying germanium dioxide according to claim 1 is characterized in that, described temperature control system (3) adopts long-range inductive probe that the microwave oven internal temperature is surveyed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102230619A CN101684000B (en) | 2008-09-26 | 2008-09-26 | Device for microwave drying germanium dioxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102230619A CN101684000B (en) | 2008-09-26 | 2008-09-26 | Device for microwave drying germanium dioxide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101684000A CN101684000A (en) | 2010-03-31 |
| CN101684000B true CN101684000B (en) | 2011-12-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008102230619A Active CN101684000B (en) | 2008-09-26 | 2008-09-26 | Device for microwave drying germanium dioxide |
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| CN (1) | CN101684000B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499474B (en) * | 2011-10-31 | 2014-03-12 | 益阳科嘉轻工机械制造有限公司 | Cigarette filter tip firming method |
| CN105277676A (en) * | 2015-11-17 | 2016-01-27 | 山东交通学院 | Movable test device and method for measuring road surface microwave deicing performance |
| US11629409B2 (en) * | 2019-05-28 | 2023-04-18 | Applied Materials, Inc. | Inline microwave batch degas chamber |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20020029892A (en) * | 2002-04-02 | 2002-04-20 | 권순목 | Microwave oven using program controller |
| CN2656915Y (en) * | 2003-09-04 | 2004-11-17 | 胡爱军 | Microwave sterilizing drying equipment |
| CN101071036A (en) * | 2007-06-11 | 2007-11-14 | 吴健辉 | Microwave cocoon-drying method and equipment |
| CN101210771A (en) * | 2006-12-29 | 2008-07-02 | 河南农业大学 | Microwave drying device |
-
2008
- 2008-09-26 CN CN2008102230619A patent/CN101684000B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20020029892A (en) * | 2002-04-02 | 2002-04-20 | 권순목 | Microwave oven using program controller |
| CN2656915Y (en) * | 2003-09-04 | 2004-11-17 | 胡爱军 | Microwave sterilizing drying equipment |
| CN101210771A (en) * | 2006-12-29 | 2008-07-02 | 河南农业大学 | Microwave drying device |
| CN101071036A (en) * | 2007-06-11 | 2007-11-14 | 吴健辉 | Microwave cocoon-drying method and equipment |
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|---|---|
| CN101684000A (en) | 2010-03-31 |
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Free format text: FORMER OWNER: BEIJING GUOJING INFRARED OPTICAL TECHNOLOGY CO., LTD. Effective date: 20130820 Owner name: BEIJING GUOJING INFRARED OPTICAL TECHNOLOGY CO., L Free format text: FORMER OWNER: BEIJING CENTRAL INST.OF THE NONFERROUS METAL Effective date: 20130820 |
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Effective date of registration: 20130820 Address after: 100088, No. two, No. 43 middle third ring road, Haidian District, Beijing Patentee after: Beijing Guojing Infrared Optical Technology Co., Ltd. Address before: 100088, 2, Xinjie street, Haidian District, Beijing Patentee before: General Research Institute for Nonferrous Metals Patentee before: Beijing Guojing Infrared Optical Technology Co., Ltd. |
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Effective date of registration: 20151208 Address after: Langfang City, Hebei Province, Sanhe Yanjiao 065201 Star Village South Patentee after: GRINM GUOJING ADVANCED MATERIALS CO., LTD. Address before: 100088, No. two, No. 43 middle third ring road, Haidian District, Beijing Patentee before: Beijing Guojing Infrared Optical Technology Co., Ltd. |
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Address after: 065201 Langfang city of Hebei province Sanhe Yanjiao Hing Village South Patentee after: GRINM GUOJING ADVANCED MATERIALS CO., LTD. Address before: Langfang City, Hebei Province, Sanhe Yanjiao 065201 Star Village South Patentee before: GRINM GUOJING ADVANCED MATERIALS CO., LTD. |