CN101612486A - Rotary steam distillation equipment - Google Patents
Rotary steam distillation equipment Download PDFInfo
- Publication number
- CN101612486A CN101612486A CN200810047493A CN200810047493A CN101612486A CN 101612486 A CN101612486 A CN 101612486A CN 200810047493 A CN200810047493 A CN 200810047493A CN 200810047493 A CN200810047493 A CN 200810047493A CN 101612486 A CN101612486 A CN 101612486A
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- Prior art keywords
- funnel
- shell
- form cone
- cone shell
- steam distillation
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- 238000001256 steam distillation Methods 0.000 title claims abstract description 22
- 241000237942 Conidae Species 0.000 claims abstract description 30
- 239000000463 material Substances 0.000 claims abstract description 30
- 239000003205 fragrance Substances 0.000 abstract description 15
- 239000000796 flavoring agent Substances 0.000 abstract description 8
- 235000019634 flavors Nutrition 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 5
- 239000000284 extract Substances 0.000 description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
- 238000004821 distillation Methods 0.000 description 16
- 244000269722 Thea sinensis Species 0.000 description 15
- 235000006468 Thea sinensis Nutrition 0.000 description 15
- 235000020279 black tea Nutrition 0.000 description 15
- 238000009835 boiling Methods 0.000 description 13
- 239000007789 gas Substances 0.000 description 11
- 238000010586 diagram Methods 0.000 description 10
- 238000000605 extraction Methods 0.000 description 7
- 239000002304 perfume Substances 0.000 description 7
- 235000013599 spices Nutrition 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 5
- 241000208125 Nicotiana Species 0.000 description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 210000000214 mouth Anatomy 0.000 description 4
- 238000011084 recovery Methods 0.000 description 4
- 235000019504 cigarettes Nutrition 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 2
- 238000000998 batch distillation Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000009834 vaporization Methods 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- 235000012984 Aspalathus linearis Nutrition 0.000 description 1
- 240000006914 Aspalathus linearis Species 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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Abstract
The invention discloses a kind of rotary steam distillation equipment, belong to the steam distillation equipment technical field.Rotary steam distillation equipment is upright cylindrical shell, and its shell center is provided with vertical column spinner, and column spinner is provided with multilayer funnel-form cone shell, is fitted with the funnel-form cone shell that is connected with shell between the funnel-form cone shell.The number of plies of funnel-form cone shell is 7～35 layers.Rotating speed of motor is 0～10000 rev/min.Angle between funnel-form cone shell and the column spinner is 30-75 °.Be parallel to each other between the multilayer funnel-form cone shell.Be parallel to each other between funnel-form cone shell that is connected with column spinner and the funnel-form cone shell that is connected with housing.Have following advantage: raw material can be realized continuous supply, has improved production efficiency; The efficient height; Can keep the natural flavour mountaineous of material, obtain high-quality fragrance; The fragrance component loss is few; The selecting range of fragrant matter is big.
Description
Technical field
The invention belongs to the water vapor distillation apparatus technical field, be specifically related to a kind of rotary steam distillation equipment that is used for extracting natural plants volatility and half volatile flavor component.
Background technology
In the prior art, increasing people extracts volatility and half volatile flavor component from natural plants and Chinese herbal medicine, but the equipment that uses is the water vapor distillation apparatus and the conventional method of routine.That is: material and water are mixed in the adding distillation equipment, by heating, make the water boiling, water vapour is taken volatility and the half volatile flavor component in these materials out of, and condensation then obtains reclaiming fragrant after the cooling.There are following problem in the said equipment and method: material can not be supplied with continuously, carries out the production of next group after can only a collection ofly finishing, and production efficiency is not high; Extraction efficiency is lower, relies on the vaporization of water self to take volatility and half volatile flavor component out of, wants at least just can reach suitable productive rate more than 1 hour, and the production time is longer; In the process of solvent refluxing heat time heating time longer, extract is in the condition of high temperature for a long time, active ingredient is easy to take place cracking or side reaction, causes destructurized; Low boiling or mid-boiling point flavor component lose easily, are difficult to obtain reflecting the extract of this note of natural plants.
Summary of the invention
At the above-mentioned deficiency of prior art, the technical problem to be solved in the present invention provides a kind of rotary steam distillation equipment, and it can be produced continuously, and material fully contacts with steam, and the reaction time is short, can fully be reflected this fragrant extract of natural plants.
Technical scheme of the present invention is: rotary steam distillation equipment is upright cylindrical shell, its shell center is provided with vertical column spinner, column spinner is provided with multilayer funnel-form cone shell, is fitted with the funnel-form cone shell that is connected with shell between the funnel-form cone shell.The number of plies of funnel-form cone shell is 7～35 layers.The column spinner bottom is connected with motor.Rotating speed of motor is 0～10000 rev/min, and is adjustable continuously.Angle between funnel-form cone shell and the column spinner is 30-75 °.Cover top portion is provided with charging aperture and gaseous state material outlet.Outer casing bottom is provided with steam-gas inlet and material outlet.Be parallel to each other between the multilayer funnel-form cone shell.Be parallel to each other between funnel-form cone shell that is connected with column spinner and the funnel-form cone shell that is connected with housing.
Equipment of the present invention is compared with conventional batch distillation method equipment has following advantage:
(1) this equipment raw material can be realized continuous supply, has improved production efficiency;
(2) contact area of raw material and steam increases greatly, can obtain distilling effect efficiently in the short time, the extraction efficiency height;
(3) the raw material heated time of this equipment is short, and the active ingredient deterioration of being heated is few, can keep material natural flavour mountaineous, obtain high-quality fragrance; And batch distillation method raw material will be under the high temperature for a long time, the fragrance component deterioration of easily being heated, and fragrance component easily loses, and therefore is difficult to obtain high-quality recovery perfume (or spice).
(4) loss of the fragrance component of this equipment is few, can obtain the recovery perfume (or spice) that contains the high intensity fragrance composition;
(5) this equipment can be set arbitrarily under the various conditions from low temperature (decompression) to high temperature (normal pressure) and carry out, and the selecting range of fragrant matter is big.
Description of drawings
Accompanying drawing 1 is the present invention and associated external equipment connection structure schematic diagram;
Accompanying drawing 2 is one embodiment of the invention structural representations;
Accompanying drawing 3 is funnel-form conical shell structure schematic diagrames in the accompanying drawing 2;
Accompanying drawing 4 is that material moves towards schematic diagram;
Accompanying drawing 5 is that steam moves towards schematic diagram;
Accompanying drawing 6 is the black tea extract gas chromatograms that obtain with this equipment;
Accompanying drawing 7 is the black tea extract gas chromatograms that obtain with prior art equipment;
Accompanying drawing 8 is comparison diagrams of the black tea extract different boiling component content that obtains of two kinds of equipment;
Accompanying drawing 9 is the coffee-extract gas chromatograms that obtain with this equipment;
Accompanying drawing 10 is the coffee-extract gas chromatograms that obtain with prior art equipment;
Accompanying drawing 11 is comparison diagrams of the coffee-extract different boiling component content that obtains of two kinds of equipment;
Accompanying drawing acceptance of the bid keep the score state as follows: 1-material storage tank; 2-storage tank material charging aperture; The 3-agitator; The 4-pump; The 5-housing; The 6-charging aperture; The 7-rotating shaft; 8-funnel-form cone shell; 9-funnel-form cone shell; The outlet of 10-gaseous material; The 11-steam inlet; The 12-material outlet; The 13-motor; The 14-condenser; The 15-collecting tank; The 16-liquid outlet.
The specific embodiment
Below in conjunction with accompanying drawing the specific embodiment of the present invention is described in further detail.When Rotary Water steam distillation equipment of the present invention uses with the logotype mutually of external equipment charging (feeding) equipment, condensing plant and collecting device.Material joins material storage tank 1 by storage tank material charging aperture 2, after agitator 3 stirs material, distill in distillation equipment charging aperture 6 enters Rotary Water steam distillation equipment housing 5 by pump 4, steam and fragrance matter mixture enter condenser 14 condensations from gaseous material outlet 10, and the recovery perfume (or spice) that obtains is stored in the collecting tank 15.The material that adds can be a solid, also can be liquid.Solid material can be crushed to behind the 60-80 order and add material storage tanks 1 from charging aperture 2, adds an amount of running water then, and agitator 3 stirs material.Material passes through pump 4 in distillation equipment material charging aperture 6 adds Rotary Water steam distillation equipment housings 5 continuously.Because the electric rotating machine 13 that rotating speed is adjustable drives funnel-form cone shell 8 rotation at a high speed on the centre rotational axis 7, material is formed very thin film, and owing to centrifugal force makes progress away along cone, fall on the funnel-form cone shell 9, and owing to gravity is walked downwards, fall down on one deck funnel-form cone shell 8, the material of adding constantly descends along each layer funnel-form cone shell.Water vapour is fed by steam inlet 11, material Continuous Contact with the film shape, the water vapour that the flavor component of volatility in the material or half volatile is made progress is effectively vaporized, the fragrance component of vaporization and steam import condenser 14 from gaseous material outlet 10 together, and the cooling back forms the recovery perfume (or spice) that contains the high intensity fragrance composition.
The applicant has carried out the contrast test of this distillation equipment and the extraction of conventional water vapor distillation apparatus.The black tea and the coffee of equivalent weight are pulverized, sieved, obtain 60-80 order powder, on above-mentioned two kinds of distinct devices, distill extraction respectively.
Accompanying drawing 6 is black tea extract gas chromatograms that present device obtains; Accompanying drawing 7 is black tea extract gas chromatograms that prior art equipment obtains; Accompanying drawing 8 is comparison diagrams of the black tea extract different boiling component content that obtains of two kinds of equipment.Diagram is the result show, in the black tea extract that Rotary Water steam distillation equipment of the present invention obtains, embody the black tea extract that this fragrant low boiling of black tea and mid-boiling point fragrance component partly obtains apparently higher than prior art equipment, can cause that the composition of the high-boiling fration that the oral cavity is residual then is starkly lower than the black tea extract that the prior art wetting system obtains.Illustrate that black tea extract that this equipment of utilization obtains more can embody this perfume (or spice) of black tea, fragrance is full, and the oral cavity is clean.
Accompanying drawing 9 is coffee-extract gas chromatograms that present device obtains; Accompanying drawing 10 is coffee-extract gas chromatograms that prior art equipment obtains; Accompanying drawing 11 is comparison diagrams of the coffee-extract different boiling component content that obtains of two kinds of distinct devices.Diagram is the result show, in the coffee-extract that rotation water vapor distillation apparatus of the present invention obtains, embody the coffee-extract that this fragrant low boiling of coffee fragrance component partly obtains apparently higher than the prior art water vapor distillation apparatus, the coffee-extract that the mid-boiling point of embodiment coffee solid sense obtains a little less than the prior art water vapor distillation apparatus can cause that the composition of the high-boiling fration that the oral cavity is residual then is starkly lower than the coffee-extract that the prior art water vapor distillation apparatus obtains.The coffee-extract that the The above results explanation utilizes this equipment to obtain more can embody this perfume (or spice) of coffee, and the oral cavity is clean.
The applicant has also carried out black tea and the coffee-extract application in the cigarette contrast of smokeing panel test, the extract of above-mentioned two kinds of distinct devices preparation is joined in the same pipe tobacco in same ratio, black tea extract adds the high-grade cigarette pipe tobacco, and coffee-extract adds middle-grade cigarette shreds.Allow 2 national judging panels and 5 provincial judging panels in Hubei smoke panel test, found that, the obvious flue gas perfume quantity of extract that more conventional distillation equipment obtains behind the extract adding pipe tobacco that rotary steam distillation equipment of the present invention obtains improves, and pleasant impression is clean, and overall assessment is better than the latter.Contrast effect sees Table 1 and table 2.
Table 1 Different Red tea extraction is added to smoking result comparison in the pipe tobacco in same ratio
| Extraction process | Gloss 5 | Fragrance 32 | Coordinate 6 | Assorted |
|
Pleasant impression 25 | Add up to |
| Conventional distillation equipment extracts | ??4 | ??28 | ??5 | ??10 | ??18 | ??23 | ??88 |
| Rotary distillation equipment extracts | ??4 | ??29.5 | ??5 | ??10 | ??18 | ??24 | ??90.5 |
The different coffee-extracts of table 2 are added to smoking result comparison in the pipe tobacco in same ratio
| Extraction process | Gloss 5 | Fragrance 32 | Coordinate 6 | Assorted |
|
Pleasant impression 25 | Add up to |
| Conventional distillation equipment extracts | ??4 | ??26 | ??5 | ??10 | ??17 | ??22 | ??84 |
| Rotary distillation equipment extracts | ??4 | ??27.5 | ??5.5 | ??10 | ??18 | ??23 | ??87 |
Claims (9)
1, a kind of rotary steam distillation equipment, it is characterized in that: described equipment is upright cylindrical shell, its shell (5) center is provided with vertical column spinner (7), column spinner (7) is provided with multilayer funnel-form cone shell (8), is fitted with the funnel-form cone shell (9) that is connected with shell (5) between the funnel-form cone shell (8).
2, rotary steam distillation equipment according to claim 1 is characterized in that: the number of plies of described funnel-form cone shell (8) is 7～35 layers.
3, rotary steam distillation equipment according to claim 1 is characterized in that: described column spinner (7) bottom is connected with motor (13).
4, rotary steam distillation equipment according to claim 3 is characterized in that: the rotating speed of described motor (13) is 0～10000 rev/min, and is adjustable continuously.
5, rotary steam distillation equipment according to claim 1 is characterized in that: the angle between described funnel-form cone shell (8) and the column spinner (7) is 30-75 °.
6, rotary steam distillation equipment according to claim 1 is characterized in that: described shell (5) top is provided with charging aperture (6) and gaseous state material outlet (10).
7, rotary steam distillation equipment according to claim 1 is characterized in that: described shell (5) bottom is provided with steam-gas inlet (11) and material outlet (12).
8, rotary steam distillation equipment according to claim 1 is characterized in that: be parallel to each other between the described multilayer funnel-form cone shell (8).
9, rotary steam distillation equipment according to claim 1 is characterized in that: be parallel to each other between described funnel-form cone shell (8) and the funnel-form cone shell (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810047493A CN101612486A (en) | 2008-06-26 | 2008-06-26 | Rotary steam distillation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810047493A CN101612486A (en) | 2008-06-26 | 2008-06-26 | Rotary steam distillation equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101612486A true CN101612486A (en) | 2009-12-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200810047493A Pending CN101612486A (en) | 2008-06-26 | 2008-06-26 | Rotary steam distillation equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101612486A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104870071A (en) * | 2013-07-18 | 2015-08-26 | Lg化学株式会社 | Gas-liquid separation apparatus |
| CN104884157A (en) * | 2013-07-19 | 2015-09-02 | Lg化学株式会社 | Gas-liquid separation apparatus |
| CN105251225A (en) * | 2015-10-31 | 2016-01-20 | 武汉纽威晨创科技发展股份有限公司 | Multilayer disc type centrifugation and gravity film forming microwave evaporation device |
| CN105251227A (en) * | 2015-10-31 | 2016-01-20 | 武汉纽威制药机械有限公司 | Multilayer disc type centrifugation and gravity film forming and differential speed pressure reduction low-temperature evaporation device |
| CN105289023A (en) * | 2015-10-31 | 2016-02-03 | 武汉纽威制药机械有限公司 | Method for extracting effective ingredients of traditional Chinese medicine by water jet crushing and decompressing low-temperature distilling through centrifugal membrane |
| CN105381628A (en) * | 2015-10-31 | 2016-03-09 | 武汉纽威晨创科技发展股份有限公司 | Method for extracting effective ingredients of traditional Chinese medicine through water jet smashing and centrifugal film microwave distilling |
| CN108499151A (en) * | 2017-12-27 | 2018-09-07 | 温州市日中轻工机械有限公司 | A kind of centrifugal thin-film Distallation systm |
| CN109045737A (en) * | 2018-08-17 | 2018-12-21 | 无锡科技职业学院 | A kind of falling bowl stirring plate distillation column |
| CN110772827A (en) * | 2019-11-14 | 2020-02-11 | 安徽徽柏环保科技有限公司 | High-temperature combustible tar gas rotary type cooling and recycling device |
| CN113893568A (en) * | 2021-10-15 | 2022-01-07 | 付雪玲 | Acrylic acid purification lightness-removing tower |
-
2008
- 2008-06-26 CN CN200810047493A patent/CN101612486A/en active Pending
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|---|---|---|---|---|
| US9446332B2 (en) | 2013-07-18 | 2016-09-20 | Lg Chem, Ltd. | Apparatus for separating gas and liquid |
| CN104870071B (en) * | 2013-07-18 | 2017-03-15 | Lg化学株式会社 | For separating the device of gas and liquid |
| CN104870071A (en) * | 2013-07-18 | 2015-08-26 | Lg化学株式会社 | Gas-liquid separation apparatus |
| CN104884157A (en) * | 2013-07-19 | 2015-09-02 | Lg化学株式会社 | Gas-liquid separation apparatus |
| CN104884157B (en) * | 2013-07-19 | 2018-02-06 | Lg化学株式会社 | For separating the device of gas and liquid |
| EP3023142A4 (en) * | 2013-07-19 | 2017-01-25 | LG Chem, Ltd. | Gas-liquid separation apparatus |
| CN105289023A (en) * | 2015-10-31 | 2016-02-03 | 武汉纽威制药机械有限公司 | Method for extracting effective ingredients of traditional Chinese medicine by water jet crushing and decompressing low-temperature distilling through centrifugal membrane |
| CN105381628A (en) * | 2015-10-31 | 2016-03-09 | 武汉纽威晨创科技发展股份有限公司 | Method for extracting effective ingredients of traditional Chinese medicine through water jet smashing and centrifugal film microwave distilling |
| CN105251227A (en) * | 2015-10-31 | 2016-01-20 | 武汉纽威制药机械有限公司 | Multilayer disc type centrifugation and gravity film forming and differential speed pressure reduction low-temperature evaporation device |
| CN105289023B (en) * | 2015-10-31 | 2017-08-01 | 武汉纽威制药机械有限公司 | A kind of method that nappe flip length and centrifugation film decompression low temperature distillation extract effective component of chinese medicine |
| CN105251225B (en) * | 2015-10-31 | 2017-10-27 | 武汉纽威晨创科技发展股份有限公司 | A kind of multilayer disc-stack centrifuge and gravity film forming microwave evaporation device |
| CN105251225A (en) * | 2015-10-31 | 2016-01-20 | 武汉纽威晨创科技发展股份有限公司 | Multilayer disc type centrifugation and gravity film forming microwave evaporation device |
| CN108499151A (en) * | 2017-12-27 | 2018-09-07 | 温州市日中轻工机械有限公司 | A kind of centrifugal thin-film Distallation systm |
| CN109045737A (en) * | 2018-08-17 | 2018-12-21 | 无锡科技职业学院 | A kind of falling bowl stirring plate distillation column |
| CN110772827A (en) * | 2019-11-14 | 2020-02-11 | 安徽徽柏环保科技有限公司 | High-temperature combustible tar gas rotary type cooling and recycling device |
| CN110772827B (en) * | 2019-11-14 | 2021-12-31 | 安徽徽柏环保科技有限公司 | High-temperature combustible tar gas rotary type cooling and recycling device |
| CN113893568A (en) * | 2021-10-15 | 2022-01-07 | 付雪玲 | Acrylic acid purification lightness-removing tower |
| CN113893568B (en) * | 2021-10-15 | 2024-01-05 | 徐州合谷生命科技有限公司 | Acrylic acid purification light component removing tower |
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Open date: 20091230 |