CN101564124A - Pelletizing method of pine pollen - Google Patents
Pelletizing method of pine pollen Download PDFInfo
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- CN101564124A CN101564124A CNA2009100945255A CN200910094525A CN101564124A CN 101564124 A CN101564124 A CN 101564124A CN A2009100945255 A CNA2009100945255 A CN A2009100945255A CN 200910094525 A CN200910094525 A CN 200910094525A CN 101564124 A CN101564124 A CN 101564124A
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- pine pollen
- pollen pini
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Abstract
The invention provides a pelletizing method of pine pollen, which is characterized in that: pine pollen extracting solution with the mass concentration of 3-15 percent and pine pollen are evenly mixed according to the mass ratio of 1:0.4-1.5 of pine pollen to extracting solution, and then made into soft granules; the soft granules are dried to granules with 8-15 percent of water content under the conditions that the temperature is less than 40 DEG C and the relative humidity is less than 50 percent to obtain broken wall pine pollen materials. Without adding any traditional accessories as bonding agent, the pine pollen extracting solution is directly used as the bonding agent, the pine pollen content in the product reaches up to 100 percent; and by low-temperature dehumidification and drying, the loss of enzyme active substances in the pine pollen is reduced, and the edible potency of the broken pine pollen is effectively improved.
Description
Technical field
The present invention relates to a kind of method of granulating of pollen pini, especially a kind of method of granulating that can make pollen pini in the wet granulation process, keep enzymatic activity.
Background technology
The pollen pini product is based on tablet, hard shell capsules in the market, after its main production is the pollen pini broken wall, adds auxiliary material and granulates, and makes through compressing tablet or capsule charge then.In compressing tablet or capsule charge process, the flowability of the pollen pini after the granulation, compression forming, lubricity etc. are the three big factors that directly influence its compressing tablet or capsule charge processing quality.In compressing tablet or capsule charge production process, the good fluidity of pollen pini material then can make operations such as mobile, filling carry out smoothly, and can reduce the weight differential of tablet, capsule; And compression forming is good, bad phenomenon such as sliver or loose sheet can not occur; Lubricity is good, tablet is not sticked dash, and obtains complete, bright and clean tablet.Because pollen pini is behind broken wall, its specific area increases, and the particulate agglomeration strengthens, make its flowability become very poor, and bulk density diminish, thereby, before compressing tablet or capsule charge, need broken masson pine pollen is granulated, and add a large amount of auxiliary materials, with improve liquidity, compression forming, lubricity.In adopting conventional wet granulation production, also need to add liquid adhesives such as starch, dextrin slurry, honey, dry under higher temperature after the granulation.And show through experimental study: more than 40 ℃ during temperature, along with the prolongation of drying time or the rising of temperature, the loss of enzyme activity of pollen pini can increase thereupon.On the other hand, in the dry granulation process,,, could improve the flowability of broken masson pine pollen, to satisfy compressing tablet or capsule charge production technology needs as sucrose, lactose, starch, dextrin etc. because of adding a large amount of auxiliary materials.This just makes the actual content of pollen pini in product reduce, and finally influences the edible of pollen pini and tires.
Summary of the invention
The present invention is directed to the problems referred to above that prior art exists, a kind of auxiliary material that need not to add is provided, just can keep its good flowability, compression forming and lubricity, and the little broken masson pine pollen method of granulating of loss of enzyme activity, tire to improve the edible of pollen pini.
The present invention finishes by following technical proposal: a kind of pelletizing method of pine pollen is characterized in that through following process steps:
A, be 3～15% pollen pini extract, press pollen pini mass concentration: the mass ratio of extract=1: 0.4～1.5, after extract and pollen pini mixed, make soft particle;
B, the soft particle that the A step is made are lower than 40 ℃ in temperature, and relative humidity is lower than under 50% the condition, and being dried to the particle water content is 8～15%, promptly gets pollen pini granulation powder.
Described pollen pini extract is the water extract, and perhaps alcohol extract makes through following method respectively:
Water extract: by pollen pini: the mass ratio of water=1: 15～18 adds water to carry out conventional water and carries, extract after the extraction concentrates or reverse osmosis concentration or vacuum concentrate and obtain the condensed water extract through the conventional ultrafiltration of prior art, carries out wherein that water is carried, ultrafiltration concentrates, the temperature during reverse osmosis concentration is controlled at below 20 ℃;
Alcohol extract: by pollen pini: the mass ratio of ethanolic solution=1: 14～16 adds ethanol and carries out conventional alcohol extracting, extract after the extraction concentrates or reverse osmosis concentration or the concentrated alcohol extract of the concentrated acquisition of vacuum through the conventional ultrafiltration of prior art, wherein alcohol extracting temperature is controlled at 85～90 ℃, ethanol volumetric concentration (V/V) is 40～95%, and ultrafiltration concentrates, the temperature of reverse osmosis concentration is controlled at below 20 ℃.
Be the mixing of described extract and pollen pini to adopt the conventional spray method of prior art to mix.
Described granulation is to adopt the conventional method of granulating of prior art to make.
Preferred 20～30 ℃ of described baking temperature is to keep the enzymatic activity of pollen pini as far as possible.
Described relative humidity is preferred 20～30%, and relative humidity is to control by the air freezing drying of prior art or air conditioner dehumidification to realize.
Described pollen pini is the pollen pini that carries out broken wall treatment through the conventional method of prior art.
The present invention compared with prior art has following advantage and effect: when adopting such scheme to granulate, need not add any auxiliary material as binder, but directly use the pollen pini extract as binder, make the pollen pini content in the product reach 100%, again by the low temperature dehumidification drying, reduced the loss of enzymatic activity material in the pollen pini, effectively improved the edible of pollen pini and tired.
The specific embodiment
Below by specific embodiment the present invention is described further.
Embodiment 1
Pollen pini water extract obtains through following method: pollen pini is pressed pollen pini behind broken wall: the mass ratio of water=1: 18, in 15 ℃ of lixiviates 2 times, each 2 hours, centrifugation, the gained clear liquid in 15 ℃ by ultrafiltration, reverse osmosis concentration to solid content 3%, it is standby to make water extracting liquid.
Embodiment 2
The pollen pini alcohol extract obtains through following method: behind the pollen pini broken wall, press pollen pini: the mass ratio of ethanolic solution=1: 14 is 70% food grade ethanolic solution with volumetric concentration (V/V), in 90 ℃ of heating and refluxing extraction 2 times, each 2 hours, filter to get filtrate while hot; Gained filtrate is concentrated into the Pollen Pini extract solid content through vacuum is 10%, standby.
Embodiment 3
Capsule charge is granulated with broken masson pine pollen: be 3% broken masson pine pollen water extract with the concentration of embodiment 1 gained, press pollen pini: the mass ratio of water extract=1: 0.4, be sprayed in the broken masson pine pollen, after stirring and making soft particle, mat formation on basin, the thickness of spreading is 0.5 centimetre, put into drying shed, start air conditioner dehumidification equipment, keep 25 ℃ of air themperatures, relative humidity 30%, dry pollen pini to water content drops to 10%, promptly get broken masson pine pollen granulation powder, be filled in the hard shell capsules, get the pollen pini capsule.
Embodiment 4
Compressing tablet broken masson pine pollen granulation: be 10% broken masson pine pollen alcohol extract with the concentration of embodiment 2 gained, press pollen pini: the mass ratio of alcohol extract=1: 0.7, be sprayed in the broken masson pine pollen, after stirring and making soft particle, place fluidized bed drying equipment, feeding temperature is 30 ℃, relative humidity is 30% dry air, and dry pollen pini to water content drops to 15%, promptly gets broken masson pine pollen granulation powder, through conventional method tablet forming, get the pollen pini sheet.
Claims (6)
1, a kind of pelletizing method of pine pollen is characterized in that through following process steps:
A, be 3～15% pollen pini extract, press pollen pini mass concentration: the mass ratio of extract=1: 0.4～1.5, after extract and pollen pini mixed, make soft particle;
B, the soft particle that the A step is made are lower than 40 ℃ in temperature, and relative humidity is lower than under 50% the condition, and being dried to the particle water content is 8～15%, promptly gets broken masson pine pollen granulation powder.
2, pelletizing method of pine pollen according to claim 1 is characterized in that described pollen pini extract is the water extract, and perhaps alcohol extract makes through following method respectively:
Water extract: by pollen pini: the mass ratio of water=1: 15～18 adds water to carry out conventional water and carries, extract after the extraction concentrates or reverse osmosis concentration or vacuum concentrate and obtain the condensed water extract through the conventional ultrafiltration of prior art, carries out wherein that water is carried, ultrafiltration concentrates, the temperature during reverse osmosis concentration is controlled at below 20 ℃;
Alcohol extract: by pollen pini: the mass ratio of ethanolic solution=1: 14～16 adds ethanol and carries out conventional alcohol extracting, extract after the extraction concentrates or reverse osmosis concentration or the concentrated alcohol extract of the concentrated acquisition of vacuum through the conventional ultrafiltration of prior art, wherein alcohol extracting temperature is controlled at 85～90 ℃, ethanol volumetric concentration (V/V) is 40～95%, and ultrafiltration concentrates, the temperature of reverse osmosis concentration is controlled at below 20 ℃.
3, pelletizing method of pine pollen according to claim 1 is characterized in that being mixing of described extract and pollen pini adopting the conventional spray method of prior art to mix.
4, pelletizing method of pine pollen according to claim 1 is characterized in that described granulation is to adopt the conventional method of granulating of prior art to make.
5, pelletizing method of pine pollen according to claim 1 is characterized in that preferred 20～30 ℃ of described baking temperature, to keep the enzymatic activity of pollen pini as far as possible.
6, pelletizing method of pine pollen according to claim 1 is characterized in that described relative humidity is preferred 20～30%, and relative humidity is to control by the air freezing drying of prior art or air conditioner dehumidification to realize.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100945255A CN101564124B (en) | 2009-05-27 | 2009-05-27 | Pelletizing method of pine pollen |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2009100945255A CN101564124B (en) | 2009-05-27 | 2009-05-27 | Pelletizing method of pine pollen |
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| CN101564124A true CN101564124A (en) | 2009-10-28 |
| CN101564124B CN101564124B (en) | 2012-05-23 |
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| CN2009100945255A Expired - Fee Related CN101564124B (en) | 2009-05-27 | 2009-05-27 | Pelletizing method of pine pollen |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101703249A (en) * | 2009-11-12 | 2010-05-12 | 西安斯强实业有限公司 | Health care product with functions of regulating incretion and increasing immunity and preparation method thereof |
| CN105309855A (en) * | 2014-07-18 | 2016-02-10 | 武汉蜂之宝蜂业有限公司 | Processing method for selenium-rich pollen sheet |
| CN108851054A (en) * | 2018-07-05 | 2018-11-23 | 广元亿明生物科技有限公司 | A kind of eucommia Bark male flower chewable tablets and preparation method thereof |
| CN108926581A (en) * | 2017-05-24 | 2018-12-04 | 严芳 | A kind of preparation method of pure pine pollen tablet |
| CN108938683A (en) * | 2017-05-24 | 2018-12-07 | 严芳 | A kind of pure pelletizing method of pine pollen |
| CN113679070A (en) * | 2021-08-23 | 2021-11-23 | 浙江亚林生物科技股份有限公司 | Dry method granulation method for pine pollen |
| CN114868943A (en) * | 2022-05-24 | 2022-08-09 | 张卫 | Novel bee pollen tabletting process without adding auxiliary materials |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101380101B (en) * | 2008-06-27 | 2012-05-23 | 吉林农业大学 | Health food new preparation of common fig |
| CN101411727B (en) * | 2008-12-01 | 2011-09-28 | 浙江亚林生物科技股份有限公司 | Formula of pine pollen essence tablet and preparation technique thereof |
-
2009
- 2009-05-27 CN CN2009100945255A patent/CN101564124B/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101703249A (en) * | 2009-11-12 | 2010-05-12 | 西安斯强实业有限公司 | Health care product with functions of regulating incretion and increasing immunity and preparation method thereof |
| CN105309855A (en) * | 2014-07-18 | 2016-02-10 | 武汉蜂之宝蜂业有限公司 | Processing method for selenium-rich pollen sheet |
| CN108926581A (en) * | 2017-05-24 | 2018-12-04 | 严芳 | A kind of preparation method of pure pine pollen tablet |
| CN108938683A (en) * | 2017-05-24 | 2018-12-07 | 严芳 | A kind of pure pelletizing method of pine pollen |
| CN108851054A (en) * | 2018-07-05 | 2018-11-23 | 广元亿明生物科技有限公司 | A kind of eucommia Bark male flower chewable tablets and preparation method thereof |
| CN113679070A (en) * | 2021-08-23 | 2021-11-23 | 浙江亚林生物科技股份有限公司 | Dry method granulation method for pine pollen |
| CN114868943A (en) * | 2022-05-24 | 2022-08-09 | 张卫 | Novel bee pollen tabletting process without adding auxiliary materials |
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| Publication number | Publication date |
|---|---|
| CN101564124B (en) | 2012-05-23 |
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