CN101497764B - Formula and production process of polyethersulfone water soluble paint - Google Patents
Formula and production process of polyethersulfone water soluble paint Download PDFInfo
- Publication number
- CN101497764B CN101497764B CN200810006647XA CN200810006647A CN101497764B CN 101497764 B CN101497764 B CN 101497764B CN 200810006647X A CN200810006647X A CN 200810006647XA CN 200810006647 A CN200810006647 A CN 200810006647A CN 101497764 B CN101497764 B CN 101497764B
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- CN
- China
- Prior art keywords
- pes
- polyethersulfone
- water soluble
- soluble paint
- ultra
- Prior art date
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- 239000004695 Polyether sulfone Substances 0.000 title claims abstract description 35
- 229920006393 polyether sulfone Polymers 0.000 title claims abstract description 35
- 239000003973 paint Substances 0.000 title claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 238000009472 formulation Methods 0.000 title abstract description 4
- 239000011347 resin Substances 0.000 claims abstract description 10
- 229920005989 resin Polymers 0.000 claims abstract description 10
- 229910021642 ultra pure water Inorganic materials 0.000 claims abstract description 9
- 239000012498 ultrapure water Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 4
- 238000002360 preparation method Methods 0.000 claims abstract 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000004809 Teflon Substances 0.000 claims description 5
- 229920006362 Teflon® Polymers 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 239000012046 mixed solvent Substances 0.000 claims description 3
- JSPLKZUTYZBBKA-UHFFFAOYSA-N trioxidane Chemical compound OOO JSPLKZUTYZBBKA-UHFFFAOYSA-N 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 238000000576 coating method Methods 0.000 abstract description 19
- 239000011248 coating agent Substances 0.000 abstract description 18
- 239000002904 solvent Substances 0.000 abstract description 8
- 239000003513 alkali Substances 0.000 abstract description 7
- 239000000203 mixture Substances 0.000 abstract description 6
- 238000005299 abrasion Methods 0.000 abstract description 5
- 239000011882 ultra-fine particle Substances 0.000 abstract 4
- 229920012266 Poly(ether sulfone) PES Polymers 0.000 abstract 1
- 239000006072 paste Substances 0.000 abstract 1
- 238000002474 experimental method Methods 0.000 description 9
- 239000007787 solid Substances 0.000 description 6
- 239000002585 base Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 238000002791 soaking Methods 0.000 description 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- 239000012267 brine Substances 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention relates to the formulation and the preparation process of polyether sulfone (PES) solution coating. The PES solution coating contains PES ultra-fine particles, polyfluortetraethylene resin, color paste, ultrapure water and solvent. The preparation process of the PES solution coating comprises the steps of putting the PES ultra-fine particles, the color paste, the ultrapure water and the solvent into a container according to a certain proportion, dispersing the PES ultra-fine particles, the color paste, the ultrapure water and the solvent with a high-speed dispersing machine, adding the polyfluortetraethylene resin into the filtered mixture of the PES ultra-fine particles, the color paste, the ultrapure water and the solvent, and stirring the polyfluortetraethylene resin and the filtered mixture for about 20 minutes. The PES solution coating is cheap, has high alkali resistance and abrasion resistance, can be independently coated into a finished product, and can be used as double-layer fluororesin nonstick coating.
Description
Technical field
The present invention relates to a kind of prescription and production technique of polyethersulfone water soluble paint.
Background technology
Alkaline-resisting, wear-resisting is one of the important indicator of non-stick pan, and used in the past non-stick pan coating mainly is polyamidoimide coating, this coating price costliness, and alkali resistance, hardness and wear resistance are not high enough.
Summary of the invention
Purpose of the present invention just provides a kind of alkaline-resisting, hardness high abrasion, and the low non-stick pan coating of cost value.
For achieving the above object, the present invention adopts following technical scheme:
This coating is made by following materials of weight proportions:
A: tackiness agent: polyethersulfone ultra-fine micropowder (PES) solid content: 3-20%
B: antisticking agent: teflon resin solid content: 5-30%
C: filler: mill base solid content: 5-20%
D: ultrapure water content: 50-70%
E: solvent: keto-alcohol ether mixed solvent content: 15-30%
The content percentage ratio sum of above each component equals 100%.
Described polyethersulfone water soluble paint, comprise following production technique: polyethersulfone ultra-fine micropowder (PES), mill base, ultrapure water, solvent are put into container in proportion, after disperseing 30 minutes with high speed dispersor (800-960 rev/min), filter through the 200-400 order, add teflon resin more in proportion, low speed (60-100 rev/min) stir about can obtain polyethersulfone water soluble paint in 20 minutes.
Because the character of the raw material polyethersulfone ultra-fine micropowder (PES) of this prescription tamanori itself has determined alkali resistance and hardness to be higher than the polyamidoimide of tamanori in the conventional formulation (PAI), this has just determined the alkali resistance of institute's coatings formulated and the increase of hardness.The market value of polyamidoimide (PAI) is very high, and generally more than 500 yuan/kilogram, polyethersulfone ultra-fine micropowder (PES) then is about 170 yuan/kilogram, the price variance like this 3 times emphasis place that this prescription cost is lower just.
Embodiment
Press column weight amount proportion raw material and make this coating:
A: tackiness agent: polyethersulfone ultra-fine micropowder (PES) solid content: 5%
B: antisticking agent: teflon resin solid content: 10%
C: filler: mill base solid content: 11%
D: ultrapure water content: 58%
E: solvent: keto-alcohol ether mixed solvent content: 16%
This polyethersulfone water soluble paint, comprise following production technique: polyethersulfone ultra-fine micropowder (PES), mill base, ultrapure water, solvent are put into container in proportion, after disperseing 30 minutes with (800-960 rev/min) high speed dispersor, filter through the 200-400 order, add teflon resin more in proportion, low speed (60-100 rev/min) stirs and can obtain polyethersulfone water soluble paint in 20 minutes.
This polyethersulfone water soluble paint alkali resistance is apparently higher than traditional polyamidoimide (PAI) coating.Coating with conventional formulation and present new prescription, mix same face and be coated with separate application, wait to solidify to form membranaceous after experiment of 5%NACL aqueous solution soaking and resistance to abrasion experiment susceptible of proof: old prescription polyamidoimide (PAI) coating reaches as high as at alkali resistance experiment, brine soaking experiment: 5-7 days.Resistance to abrasion experiment in experiment of hardness can reach about 300 commentaries on classics; New prescription polyethersulfone water soluble paint (PES) can reach 15 days at alkali resistance experiment, brine soaking experiment.Resistance to abrasion experiment in hardness can reach more than 1000 commentaries on classics, this shows that its over-all properties of polyethersulfone water soluble paint of new prescription all is higher than traditional non-stick pan coating, and price reduces greatly.
This coating can be produced the individual layer non-viscous paint according to proportioning, promptly films separately to be finished product, also can produce the primary coat of double-deck fluor resin non-stick paint, promptly behind this coating of Workpiece painting drying and forming-film, is coated with fluorine resin coating again.
Claims (2)
1. polyethersulfone water soluble paint is characterized in that it is that following materials of weight proportions is made:
2. a kind of polyethersulfone water soluble paint according to claim 1, it is characterized in that described polyethersulfone water soluble paint adopts following production technique preparation: polyethersulfone ultra-fine micropowder, mill base, ultrapure water, keto-alcohol ether mixed solvent are put into container in proportion, after disperseing 30 minutes with high speed dispersor with 800-960 rev/min speed, filter through the 200-400 order, proportionally add teflon resin again, stir with 60-100 rev/min speed and can obtain polyethersulfone water soluble paint in 20 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810006647XA CN101497764B (en) | 2008-01-30 | 2008-01-30 | Formula and production process of polyethersulfone water soluble paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810006647XA CN101497764B (en) | 2008-01-30 | 2008-01-30 | Formula and production process of polyethersulfone water soluble paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101497764A CN101497764A (en) | 2009-08-05 |
| CN101497764B true CN101497764B (en) | 2011-12-21 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200810006647XA Active CN101497764B (en) | 2008-01-30 | 2008-01-30 | Formula and production process of polyethersulfone water soluble paint |
Country Status (1)
| Country | Link |
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| CN (1) | CN101497764B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102373009A (en) * | 2011-10-18 | 2012-03-14 | 曾志玲 | Anti-adhesion paint |
| CN104974661B (en) * | 2014-04-03 | 2016-04-27 | 曾志玲 | Polyethersulfone ultra-fine micropowder, its purposes and the coating containing polyethersulfone ultra-fine micropowder and their preparation method |
| CN105086660A (en) * | 2014-06-03 | 2015-11-25 | 曾志玲 | Aqueous anti-adhesion coating for iron substrate |
| CN110194819A (en) * | 2019-06-19 | 2019-09-03 | 连云港泰科复合材料有限公司 | A kind of glass fiber net cloth coating modified acrylate emulsion and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168403A (en) * | 1997-05-20 | 1997-12-24 | 吉林大学 | Preparation of sintered PES non-stickness paint for kitchenware and household appliance |
| CN1304431A (en) * | 1998-06-05 | 2001-07-18 | 大金工业株式会社 | Water-based primer composition for fluororesin coating |
| US20070232732A1 (en) * | 2006-04-04 | 2007-10-04 | Adams Jerome T | Non-stick finish composition |
-
2008
- 2008-01-30 CN CN200810006647XA patent/CN101497764B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168403A (en) * | 1997-05-20 | 1997-12-24 | 吉林大学 | Preparation of sintered PES non-stickness paint for kitchenware and household appliance |
| CN1304431A (en) * | 1998-06-05 | 2001-07-18 | 大金工业株式会社 | Water-based primer composition for fluororesin coating |
| US20070232732A1 (en) * | 2006-04-04 | 2007-10-04 | Adams Jerome T | Non-stick finish composition |
Non-Patent Citations (1)
| Title |
|---|
| JP昭61-111352A 1986.05.29 |
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| Publication number | Publication date |
|---|---|
| CN101497764A (en) | 2009-08-05 |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: FOSHAN POLYMER ADVANCED TECHNOLOGY + SUPPLIES CO., Free format text: FORMER OWNER: CENG ZHILING Effective date: 20140109 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20140109 Address after: 528300 Guangdong province Foshan city Shunde District Daliang Street five sand Xinyue Road No. 10 Patentee after: FOSHAN POLIMA ADVANCED TECHNOLOGY & SUPPLIES Co.,Ltd. Address before: 528300, No. 1, No. 101, Foshan Road, Ronggui street, Shunde District, Guangdong, China Patentee before: Zeng Zhiling |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Formula and production process of polyethersulfone water soluble paint Effective date of registration: 20170802 Granted publication date: 20111221 Pledgee: Shunde Guangdong rural commercial bank Limited by Share Ltd. Daliang branch Pledgor: FOSHAN POLIMA ADVANCED TECHNOLOGY & SUPPLIES Co.,Ltd. Registration number: 2017440000059 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230103 Granted publication date: 20111221 Pledgee: Shunde Guangdong rural commercial bank Limited by Share Ltd. Daliang branch Pledgor: FOSHAN POLIMA ADVANCED TECHNOLOGY & SUPPLIES Co.,Ltd. Registration number: 2017440000059 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |